Durability of wood and wood-based products - Performance criteria for curative wood preservatives as determined by biological tests

This standard specifies the minimum performance requirements for curative products and processes in biological tests, for each class of wood attacking organism. It specifies the biological tests required together with the performance criteria to be achieved in each test.

Dauerhaftigkeit von Holz und Holzprodukten - Anforderungen an bekämpfend wirkende Holzschutzmittel, wie sie durch biologische Prüfungen ermittelt werden

Durabilité du bois et des matériaux dérivés du bois - Criteres de performances des produits curatifs de préservation du bois établis par des essais biologiques

Trajnost lesa in lesnih proizvodov – Merila za kakovost farmakoloških zaščitnih sredstev za les, ugotovljeno z biološkimi preskusi

General Information

Status
Withdrawn
Publication Date
31-Aug-2004
Withdrawal Date
17-May-2020
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
18-May-2020
Due Date
10-Jun-2020
Completion Date
18-May-2020

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EN 14128:2004
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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Dauerhaftigkeit von Holz und Holzprodukten - Anforderungen an bekämpfend wirkende Holzschutzmittel, wie sie durch biologische Prüfungen ermittelt werdenDurabilité du bois et des matériaux dérivés du bois - Criteres de performances des produits curatifs de préservation du bois établis par des essais biologiquesDurability of wood and wood-based products - Performance criteria for curative wood preservatives as determined by biological tests79.040Les, hlodovina in žagan lesWood, sawlogs and sawn timber71.100.50Wood-protecting chemicalsICS:Ta slovenski standard je istoveten z:EN 14128:2003SIST EN 14128:2004en01-september-2004SIST EN 14128:2004SLOVENSKI
STANDARD



SIST EN 14128:2004



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 14128December 2003ICS 71.100.50; 79.040English versionDurability of wood and wood-based products - Performancecriteria for curative wood preservatives as determined bybiological testsDurabilité du bois et des matériaux dérivés du bois -Critères de performances des produits curatifs depréservation du bois établis par des essais biologiquesDauerhaftigkeit von Holz und Holzprodukten -Anforderungen an bekämpfend wirkende Holzschutzmittel,wie sie durch biologische Prüfungen ermittelt werdenThis European Standard was approved by CEN on 1 October 2003.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and UnitedKingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2003 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 14128:2003 ESIST EN 14128:2004



EN 14128:2003 (E)2ContentspageForeword.3Introduction.41Scope.52Normative references.53Terms and definitions.64Wood destroying organisms.75Performance requirements for products against beetles (see Table 1).86Performance requirements for barrier treatments against dry rot fungus.97Derivation of effective values.98Product identification and labelling.9Annex A (informative)
Guidance on re-testing after making variations in product formulation.13Annex B (normative)
Test requirements for curative products against Xestobium rufovillosum.18Annex C (normative)
Test requirements for curative products against Hesperophanes cinnereus.19Annex D (informative)
Recommended system for the classification of the effectiveness of curativewood preservatives.20Annex E (informative)
Guidance for physical chemical properties.21Annex F (informative)
Example of a system to describe the effectiveness of a curative woodpreservatives against beetles.22Bibliography.23SIST EN 14128:2004



EN 14128:2003 (E)3ForewordThis document (EN 14128:2003) has been prepared by Technical Committee CEN/TC 38 “Durability of wood andwood-based products”, the secretariat of which is held by AFNOR.This European Standard shall be given the status of a national standard, either by publication of an identical text orby endorsement, at the latest by June 2004, and conflicting national standards shall be withdrawn at the latest byJune 2004.This European Standard gives the performance criteria for curative wood preservatives as determined by biologicaltests. A further European Standard (at present still in preparation) is concerned with criteria for hot air processes forcurative uses against wood destroying organisms.This European Standard is valid for products to eradicate beetles in infested wood and for products to be used inthe course of curative actions against the dry rot fungus to prevent its growth through masonry and beyond.The annexes B and C are normative.The annexes A, D, E and F are informative.According to the CEN/CENELEC Internal Regulations, the national standards organizations of the followingcountries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal,Slovakia, Spain, Sweden, Switzerland and the United Kingdom.SIST EN 14128:2004



EN 14128:2003 (E)4IntroductionThis European Standard should be used in conjunction with prEN WI 00038084 (at present still in preparation) andwith EN 599-1 which describes the performance requirements for preventive wood preservatives as determined bybiological tests.The need to use curative products against wood destroying organisms depends upon a careful diagnosis by expert,qualified specialists to determine the precise causes of the damage to be rectified. This should include the type ofwood attacking organisms involved and whether they are active, the environmental circumstances, especially thesource and nature of any wetting, the type of wood involved, the nature of the building or construction, and thestructural and physical significance of the timber which is damaged or at risk of being damaged.Curative treatment can be achieved either by chemical wood preservatives as specified in this European Standardor by specific curative processes without using chemicals, like hot air processes, as given in prEN WI 00038084.Curative wood preservative products should be used in an integrated way as part of a carefully prescribed strategyinvolving a series of actions appropriate to the particular circumstances of each case. Associated physicalmeasures involving appropriate building works to remedy ingress of moisture and to dry out any dampness can bean essential prerequisite for the use of any curative products. Expert diagnosis should take into account allregional, practical, environmental, economical, safety and any other factors which can be relevant to theprescriptive decisions to be taken.It is not the purpose of this European Standard to provide a specification, or even guidance in developingspecifications for remedial work to eradicate wood destroying organisms. This European Standard also does notgive guidance on the methods of application or the precise amounts of products that might be appropriate to applyin specific practical circumstances. It is intended to guide specifiers, users and others in selecting and specifyingproducts on the basis of their effectiveness as demonstrated in accordance with the criteria given.SIST EN 14128:2004



EN 14128:2003 (E)51 ScopeThis European Standard specifies the minimum performance requirements in biological tests for products forcurative uses against specific wood destroying organisms. It specifies the biological tests required together with theperformance criteria to be achieved in each test.Chemicals against insects can act according to their specific properties within a short time (fast acting) or only aftera long period (slow acting or with a deferred effect). Different tests and performance requirements are needed forthese various types of curative wood preservatives.This European Standard is applicable to all wood preservative products supplied for application in liquid form forcurative uses against attack by wood attacking insects, excluding termites. This European Standard is alsoapplicable for products applied to prevent growth of dry rot fungus through masonry.This European Standard is also applicable to products for curative uses supplied for application as pastes, solids orin capsule form but only where appropriate biological methods of test exist as published European Standards or asnormative annexes to this European Standard.NOTE 1The nature of the laboratory tests required in this European Standard is such that the time required to generate datais many months sometimes more than one year, depending upon the type of product and the organism(s) it is intended to beused against.Therefore, at the date of publication of this European Standard, for many products covered under its scope already placed onthe market and used lawfully in accordance with local technical traditions, the minimum data specified in this standard may notbe available. Accordingly, for a period not exceeding 3 years from the date of publication of this European Standard, nationalstandards organisations, or an organisation nominated by them may declare interim effective values for use within theirterritories, to apply to products already placed on the market and used lawfully in accordance with local traditions at the date ofuse of this European Standard.NOTE 2For re-testing after making variations in product formulation, guidance is given in annex A.This European Standard is not applicable to products used as fumigants.This European Standard is also not applicable for determining whether specific curative products, used alone or incombination, are effective in conferring long-term preventive action against attack by wood destroying organisms inthe future. Preventive effectiveness can be determined using EN 599-1 but only for products whose nature allowthem to be tested using the methods and interpretative procedures defined in EN 599-1. Amendments of existingtest methods cited in EN 599-1 may be used but only when defined in normative annexes to this EuropeanStandard.2 Normative referencesThis European Standard incorporates by dated or undated reference, provisions from other publications. Thesenormative references are cited at the appropriate places in the text, and the publications are listed hereafter. Fordated references, subsequent amendments to or revisions of any of these publications apply to this EuropeanStandard only when incorporated in it by amendment or revision. For undated references the latest edition of thepublication referred to applies (including amendments).EN 22, Wood preservatives – Determination of eradicant action against Hylotrupes bajulus (Linnaeus) larvae(Laboratory method).EN 48, Wood preservatives – Determination of the eradicant action against larvae of Anobium punctatum (DeGeer) (Laboratory method).EN 73, Wood preservatives – Accelerated ageing tests of treated wood prior to biological testing – Evaporativeageing procedure.SIST EN 14128:2004



EN 14128:2003 (E)6EN 370, Wood preservatives – Determination of eradicant efficacy in preventing emergence of Anobium punctatum(De Geer).EN 599-1:1996, Durability of wood and wood-based products – Performance of preventive wood preservatives asdetermined by biological tests – Part 1: Specification according to hazard class.ENV 1390, Wood preservatives – Determination of the eradicant action against Hylotrupes bajulus (Linnaeus)larvae – Laboratory method.ENV 12404, Durability of wood and wood-based products – Assessment of the effectiveness of a masonryfungicide to prevent growth into wood of Dry Rot Serpula lacrymans (Schumacher ex Fries) S.F Gray – Laboratorymethod.3 Terms and definitionsFor the purposes of this European Standard, the following terms and definitions apply.3.1active ingredientindividual chemical compound or compounds included in the wood preservative product to give it a specific activityagainst the particular biological agencies of deterioration3.2barrier treatmenttreatment of masonry in case of dry rot fungus to avoid its growth beyond the treated zone3.3biological reference value (brv)amount in grams per square meter or kilograms per cubic meter of the wood preservative product found to beeffective in test in eradicating attack by the particular biological agency being tested3.4curative efficacyspecific property of a wood preservative to act as an eradicant in infested timber3.5deferred effect insecticidal productsinsect curative products which are not designed to have an immediate effect on the target organisms but which aredesigned to have their full eradicant effect at a later stage in the life cycle e.g. at the time of emergence from thewood3.6effective valueamount of wood preservative in millilitres per square meter obtained from all biological tests carried out inaccordance with this European Standard. It is the highest of the brvs for the curative effectiveness of the productfrom all the tests carried out to support the claimed activity of the product3.7fast acting insecticidal productsinsect curative products which achieve the required level of effectiveness within a period of three months using theappropriate standard test method3.8maximum application limitmaximum amount in millilitres per square meter of the wood preservative product permitted for application to thewood specimens in the particular biological testSIST EN 14128:2004



EN 14128:2003 (E)73.9performancebehaviour of the wood preservative product in terms of its effectiveness in the testNOTEThe term 'performance' applies also to the behaviour in terms of its effectiveness in practice against individual orcollective effects of particular biological agencies of deterioration.3.10preventive efficacyproperty of a wood preservative to avoid infestation of the wood by the particular biological agencies ofdeterioration3.11productformulated wood preservative product in the form as supplied for sale by the manufacturer3.12slow acting insecticidal productsinsect curative products which achieve the required level of effectiveness in a period longer than three months butnot more than one year using the appropriate standard test method3.13wood preservativeactive ingredient(s) or preparations containing active ingredient(s) in the form in which they are placed on themarket, which are, on the basis of the properties of their active ingredient(s), intended either to prevent wooddestroying or wood disfiguring organisms (fungi, insects and marine borers) from attacking wood and wood-basedproducts or to combat an attack by those organismsNOTE For the purpose of this European standard, the term wood preservatives includes also these products to eradicate anexisting infection.4 Wood destroying organisms4.1 InsectsAmongst the wood attacking insects considered in this European Standard the following are the most common:Beetles:Hylotrupes bajulus (house longhorn beetle) in the sapwood of softwoods;Anobium punctatum (common furniture beetle) in softwoods and hardwoods;Xestobium rufovillosum (deathwatch beetle) in hardwoods and softwoods, mainly in oak;Lyctus brunneus (powderpost beetle) in the starch containing sapwood of hardwoods;Hesperophanes cinnereus in the sapwood of hardwoods (occurs only in Mediterranean countries).4.2 Dry rot fungusThe dry rot fungus (Serpula lacrymans = true dry rot fungus) occurs in buildings, causing brown rot in timber. Thefungus can develop at relatively low wood moisture contents and is able to penetrate damp masonry over longdistances in order to infect further timber or to develop its fruit-bodies.SIST EN 14128:2004



EN 14128:2003 (E)85 Performance requirements for products against beetles (see Table 1)5.1 Principle requirements for curative efficacyThe curative wood preservative product shall be tested in accordance with the tests specified in Table 1, taking intoconsideration the relevant organisms and the type of insecticidal product (see 5.2.2).5.2 Supplementary requirements for curative efficacy5.2.1For Lyctus brunneus, Xestobium rufovillosum and Hesperophanes cinnereus no specific requirements arelisted, as no relevant/valid test standards exist.NOTEIn the case of Lyctus brunneus, curative treatment takes place only exceptionally so that specific preservatives areplaced only very rarely on the market. Due to economical reasons, no specific test procedure will be established. If curativetreatment against Lyctus brunneus is demanded, a curative wood preservative "for Hylotrupes and Anobium" should be applied.In the case of Xestobium rufovillosum see annex B.In the case of Hesperophanes cinnereus see annex C.5.2.2The following types of insecticidal products have to be considered:¾ fast acting products;¾ slow acting products;¾ products with deferred effect.5.2.3Tests of insecticidal activity shall be carried out against one of the following:a) "Hylotrupes bajulus (C-H)" and "Anobium punctatum (C-A)" unless b) or c) is applicable and is selected;orb) the more tolerant beetle species, if the product is based on insecticide(s) for which data on curative efficacyalready exist which show different activities against Hylotrupes bajulus and Anobium punctatum, that is theeffective value for the less tolerant species is less than 80 % of the effective amount for the more tolerantspecies;orc) against "Hylotrupes bajulus (C-H)" or "Anobium punctatum (C-A)", if the product is based on insecticide(s) forwhich data on the curative efficacy already exist which show more or less equal activity against both beetlespecies, that is the effective value of the least tolerant beetle species is equal to or greater than 80 % of theeffective value of the more tolerant beetle species.5.2.4New tests shall be carried out against Hylotrupes bajulus according to ENV 1390, however, former resultsfrom EN 22 tests shall remain valid.5.2.5At present no relevant test standards exist for deferred effect products.5.2.6The maximum application limit shall not exceed 300 ml per square meter.NOTE 1If the curative wood preservative is specified by the manufacturer to be used at a higher application in practice, themanufacturer should define how this amount is to be achieved under practical conditions.NOTE 2If the curative wood preservative is already placed on the market on the basis of results from biological testsconducted at a maximum application limit greater than 300 ml per square meter, these test results remain valid and no newtests should be demanded.SIST EN 14128:2004



EN 14128:2003 (E)95.2.7For tests according to EN 370 the duration can exceed 1 year.5.2.8If the curative wood preservative is designed to be used for the protection of items of cultural heritage forAnobium punctatum the mortality at the end of the test shall be 90 %.5.3 Requirements for preventive efficacyWhere local conditions require the curative wood preservative product to have also preventive efficacy, or tosupport the claims of manufacturers or the demands of specifiers, the product shall have its preventive efficacydemonstrated from tests in accordance with EN 599-1 at an application limit equal to or lower than that at whichtest under this curative standard were conducted.6 Performance requirements for barrier treatments against dry rot fungusIn tests according to ENV 12404 growth through mortar specimens and infection of the wood specimens shall havebeen prevented by the masonry fungicide. The application rate of the ready to use solution of the fungicide shall benot lower than 500 ml per square meter and not more than 750 ml per square meter.7 Derivation of effective values7.1 Effective value against beetlesThe effective value is derived from the results of the biological tests and shall be equal to the application rate of thewood preservative tested according to the manufacturer's recommendation (see 5.2.6).7.2 Effective value against dry rot fungusThe effective value is derived from the
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