Paints and varnishes - Determination of non-volatile-matter content and spreading rate of coil coating materials

The method specifies the gravimetric procedure for determining the non-volatile-matter content as a percentage by mass of the majority of thermally cured coil coatings and subsequently for determining the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.

Beschichtungsstoffe - Bestimmung des Gehaltes an nichtflüchtigen Anteilen und der Ergiebigkeit von Bandbeschichtungsstoffen

Die Norm legt die gravimetrische Bestimmung des Gehaltes an nichtflüchtigen Anteilen als Massenanteil in Prozent der Mehrzahl von wärmehärtenden Bandbeschichtungsstoffen mit nachfolgender Bestimmung der theoretischen Ergiebigkeit fest. Das Verfahren ist nicht geeignet für Bandbeschichtungsstoffe, die reine Epoxidharze als Bindemittel enthalten.

Peintures et vernis - Détermination de la teneur en matière non volatile et du rendement superficiel spécifique de revêtements pour prélaquage

La présente méthode décrit le mode opératoire permettant de déterminer par gravimétrie la teneur en matière non volatile en pourcentage en masse de la majorité des revêtements pour prélaquage durcis par traitement thermique, et par conséquent de déterminer le rendement d’application théorique. Cette méthode ne convient pas aux revêtements pour prélaquage en époxy pur.

Barve in laki - Določevanje nehlapnih snovi in razlivnosti premazov za kovine, ki se navijajo

Metoda določa gravimetrični postopek za določanje masnega odstotka nehlapnih snovi večine toplotno strjenih premazov za kovine, ki se navijajo, in nato za teoretično določanje njihove razlivnosti. Metoda ni primerna za čiste epoksi premaze.

General Information

Status
Published
Public Enquiry End Date
04-Jan-2019
Publication Date
09-Oct-2019
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
20-Sep-2019
Due Date
25-Nov-2019
Completion Date
10-Oct-2019

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SLOVENSKI STANDARD
SIST EN 16074:2019
01-november-2019
Nadomešča:
SIST EN 16074:2011
Barve in laki - Določevanje nehlapnih snovi in razlivnosti premazov za kovine, ki
se navijajo
Paints and varnishes - Determination of non-volatile-matter content and spreading rate of
coil coating materials
Beschichtungsstoffe - Bestimmung des Gehaltes an nichtflüchtigen Anteilen und der
Ergiebigkeit von Bandbeschichtungsstoffen
Peintures et vernis - Détermination de la teneur en matière non volatile et du rendement
superficiel spécifique de revêtements pour prélaquage
Ta slovenski standard je istoveten z: EN 16074:2019
ICS:
87.040 Barve in laki Paints and varnishes
SIST EN 16074:2019 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN 16074:2019

---------------------- Page: 2 ----------------------
SIST EN 16074:2019


EN 16074
EUROPEAN STANDARD

NORME EUROPÉENNE

September 2019
EUROPÄISCHE NORM
ICS 87.040 Supersedes EN 16074:2011
English Version

Paints and varnishes - Determination of non-volatile-
matter content and spreading rate of coil coating materials
Peintures et vernis - Détermination de la teneur en Beschichtungsstoffe - Bestimmung des Gehaltes an
matière non volatile et du rendement superficiel nichtflüchtigen Anteilen und der Ergiebigkeit von
spécifique de revêtements pour prélaquage Bandbeschichtungsstoffen
This European Standard was approved by CEN on 1 July 2019.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2019 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 16074:2019 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
SIST EN 16074:2019
EN 16074:2019 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 5
5 Apparatus and materials . 5
6 Sampling . 6
7 Test procedure . 6
7.1 Accuracy of weighing . 6
7.2 Procedure for coatings with the exception of PVC plastisols and pure epoxy . 6
7.2.1 Pan method. 6
7.2.2 Drawdown method . 6
7.3 Procedure for PVC plastisol . 7
7.3.1 Pan method. 7
7.3.2 Drawdown method . 8
8 Determination of the density . 8
9 Calculation of spreading rate of the paint . 8
10 Validation of test results . 9
11 Precision . 9
12 Test report . 9
Bibliography . 10

2

---------------------- Page: 4 ----------------------
SIST EN 16074:2019
EN 16074:2019 (E)
European foreword
This document (EN 16074:2019) has been prepared by Technical Committee CEN/TC 139 “Paints and
varnishes”, the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by March 2020, and conflicting national standards shall
be withdrawn at the latest by March 2020.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 16074:2011.
The main changes compared to EN 16074:2011 are:
a) the symbols have been aligned with current standards [ISO 3251 and ISO 3233 (all parts)], i.e. m for
mass, s for spreading rate, NV for non-volatile matter and ρ for density;
b) Clause 8 on "Determination of the density" has been added;
c) the text has been editorially revised and the normative references have been updated.
According to the CEN-CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
3

---------------------- Page: 5 ----------------------
SIST EN 16074:2019
EN 16074:2019 (E)
1 Scope
The method specifies the gravimetric procedure for determining the non-volatile-matter content as a
percentage by mass of the majority of thermally cured coil coatings and subsequently for determining
the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 13523-0, Coil coated metals — Test methods — Part 0: General introduction
EN ISO 1513, Paints and varnishes — Examination and preparation of test samples (ISO 1513)
EN ISO 2811-1, Paints and varnishes — Determination of density — Part 1: Pycnometer method
(ISO 2811-1)
EN ISO 2811-2, Paints and varnishes — Determination of density — Part 2: Immersed body (plummet)
method (ISO 2811-2)
EN ISO 2811-3, Paints and varnishes — Determination of density — Part 3: Oscillation method (ISO 2811-
3)
EN ISO 2811-4, Paints and varnishes — Determination of density — Part 4: Pressure cup method
(ISO 2811-4)
EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling (ISO 15528)
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 13523-0 and the following
apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at http://www.iso.org/obp
3.1
spreading rate
surface area that can be covered by a given quantity of coating material to give a dried film of requisite
thickness
2 2
Note 1 to entry: It is expressed in m /l or m /kg.
Note 2 to entry: See also theoretical spreading rate.
[SOURCE: EN ISO 4618:2014, 2.238, modified – Application rate and practical spreading rate were
deleted in Note 2.]
4

---------------------- Page: 6 ----------------------
SIST EN 16074:2019
EN 16074:2019 (E)
3.2
non-volatile matter
NV
residue by mass obtained by evaporation under specified conditions
Note 1 to entry: Instead of the term “non-volatile matter” different terms, such as solid, dry residue, dry matter,
solid matter, stoving residue are being used commonly with the respective abbreviations. The term “non-volatile
matter” which is also applied in ISO 3251 should be used together with the abbreviation “NV” instead of these
terms.
[SOURCE: EN ISO 4618:2014, 2.176]
3.3
theoretical spreading rate
spreading rate calculated solely from the volume of non-volatile matter
[SOURCE: ISO 4618:2014, 2.256]
4 Principle
The non-volatile-matter content determination is based on the mass of dry residue of a known quantity
of wet paint cured in a pan or applied on a metal panel. Th
...

SLOVENSKI STANDARD
oSIST prEN 16074:2018
01-december-2018
%DUYHLQODNL'RORþHYDQMHQHKODSQLKVQRYLLQUD]OLYQRVWLSUHPD]RY]DNRYLQHNL
VHQDYLMDMR
Paints and varnishes - Determination of non-volatile-matter content and spreading rate of
coil coating materials
Beschichtungsstoffe - Bestimmung des Gehaltes an nichtflüchtigen Anteilen und der
Ergiebigkeit von Bandbeschichtungsstoffen
Peintures et vernis - Détermination de la teneur en matière non volatile et du rendement
superficiel spécifique de revêtements pour prélaquage
Ta slovenski standard je istoveten z: prEN 16074
ICS:
87.040 Barve in laki Paints and varnishes
oSIST prEN 16074:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
oSIST prEN 16074:2018

---------------------- Page: 2 ----------------------
oSIST prEN 16074:2018


DRAFT
EUROPEAN STANDARD
prEN 16074
NORME EUROPÉENNE

EUROPÄISCHE NORM

October 2018
ICS 87.040 Will supersede EN 16074:2011
English Version

Paints and varnishes - Determination of non-volatile-
matter content and spreading rate of coil coating materials
Peintures et vernis - Détermination de la teneur en Beschichtungsstoffe - Bestimmung des Gehaltes an
matière non volatile et du rendement superficiel nichtflüchtigen Anteilen und der Ergiebigkeit von
spécifique de revêtements pour prélaquage Bandbeschichtungsstoffen
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 139.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 16074:2018 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
oSIST prEN 16074:2018
prEN 16074:2018 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 5
5 Apparatus and materials . 5
6 Sampling . 5
7 Test procedure . 6
7.1 Accuracy of weighing . 6
7.2 Procedure for coatings with the exception of PVC plastisols and pure epoxy . 6
7.2.1 Pan method. 6
7.2.2 Drawdown method . 6
7.3 Procedure for PVC plastisol . 7
7.3.1 Pan method. 7
7.3.2 Drawdown method . 7
8 Determination of the density . 8
9 Calculation of spreading rate of the paint . 8
10 Validation of test results . 9
11 Precision . 9
12 Test report . 9
Bibliography . 10

2

---------------------- Page: 4 ----------------------
oSIST prEN 16074:2018
prEN 16074:2018 (E)
European foreword
This document (prEN 16074:2018) has been prepared by Technical Committee CEN/TC 139 “Paints
and varnishes”, the secretariat of which is held by DIN.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 16074:2011.
The main changes are:
a) the symbols have been aligned with current standards [ISO 3251 and ISO 3233 (all parts)], i.e. m for
mass, s for spreading rate, NV for non-volatile matter and ρ for density;
b) the text has been editorially revised and the normative references have been updated.
3

---------------------- Page: 5 ----------------------
oSIST prEN 16074:2018
prEN 16074:2018 (E)
1 Scope
The method specifies the gravimetric procedure for determining the non-volatile-matter content as a
percentage by mass of the majority of thermally cured coil coatings and subsequently for determining
the theoretical spreading rate. The method is not suitable for pure epoxy coil coatings.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 13523-0, Coil coated metals — Test methods — Part 0: General introduction
EN ISO 1513, Paints and varnishes — Examination and preparation of test samples (ISO 1513)
EN ISO 2811-1, Paints and varnishes — Determination of density — Part 1: Pycnometer method (ISO
2811-1)
EN ISO 2811-2, Paints and varnishes — Determination of density — Part 2: Immersed body (plummet)
method (ISO 2811-2)
EN ISO 2811-3, Paints and varnishes — Determination of density — Part 3: Oscillation method (ISO 2811-
3)
EN ISO 2811-4, Paints and varnishes — Determination of density — Part 4: Pressure cup method (ISO
2811-4)
EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling (ISO 15528)
3 Terms and definitions
For the purposes of this document, the terms and definitions given in EN 13523-0 and the following
apply.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
— IEC Electropedia: available at http://www.electropedia.org/
— ISO Online browsing platform: available at http://www.iso.org/obp
3.1
spreading rate
surface area that can be covered by a given quantity of coating material to give a dried film of requisite
thickness
2 2
Note 1 to entry: It is expressed in m /l or m /kg.
Note 2 to entry: See also practical spreading rate and theoretical spreading rate.
[SOURCE: EN ISO 4618:2014, 2.238, modified – Application rate was deleted in Note 2.]
4

---------------------- Page: 6 ----------------------
oSIST prEN 16074:2018
prEN 16074:2018 (E)
3.2
non-volatile matter
NV
residue by mass obtained by evaporation under specified conditions
Note 1 to entry: Instead of the term “non-volatile matter” different terms, such as solid, dry residue, dry matter,
solid matter, stoving residue are being used commonly with the respective abbreviations. The term “non-volatile
matter” which is also applied in ISO 3251 should be used together with the abbreviation “NV” instead of these
terms.
[SOURCE: EN ISO 4618:2014, 2.176]
3.3
theoretical spreading rate
spreading rate calculated solely from the volume of non-volatile matter
[SOURCE: ISO 4618:2014, 2.256]
4 Principle
The non-volatile-matter content determination is based on the mass of dry residue of a known quantity
of wet paint cured in a pan or applied on a metal panel. The spreading rate is subsequently calculated
using the liquid paint density and the density of the volatile part.
5 Apparatus and materials
5.1 Analytical balance, capable of weighing to an accuracy of ± 0,000 1 g.
5.2 Flat-bottomed dish (pan), of metal or glass, inner diameter of base (75 ± 5) mm, height of the
rim at least 5 mm.
Dishes having different diameters or different rims may be used
...

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