Paints and varnishes - Coating materials and coating systems for exterior wood - Part 9: Determination of pull-off strength

This Technical Specification specifies a method for assessing the resistance of a coating system on wet wood to separation from the substrate by measuring the force necessary to detach or rupture the coating system by a normal tensile strain applied through an attached stud (dolly). Additional information is gained by noting the type and locus of failure. The force required for detachment will depend on several factors including the adhesion of the coating to the substrate and between intermediate coating layers. The procedure is not regarded as a direct means of measuring adhesion but an indicator of adhesive performance (adherence) under wet conditions.
A procedure for wetting the wood substrate is described. The test method is only suitable for wood and wood based substrates.
For dry adhesion the test method is allowed to be carried out without wetting in which case it will differ very little from EN ISO 4624.

Beschichtungsstoffe - Beschichtungsstoffe und Beschichtungssysteme für Holz im Außenbereich - Teil 9: Bestimmung der Abreißfestigkeit

Dieses Dokument legt ein Verfahren zum Beurteilen der Beständigkeit eines Beschichtungssystems auf nassem Holz gegen seine Entfernung vom Substrat fest; dies geschieht durch Messen der Kraft, die zum Lösen oder Brechen des Beschichtungssystems mithilfe einer normalen Zugbelastung erforderlich ist, die über einen verbundenen Bolzen (Stempel) angewandt wird. Weitere Informationen ergeben sich durch Notieren von Fehlerart und -ort. Die zum Lösen erforderliche Kraft hängt von mehreren Faktoren ab, einschließlich der Haftfestigkeit der Beschichtung auf dem Substrat und innerhalb von Zwischenbe¬schichtungen. Das Verfahren wird nicht als direktes Mittel zur Messung der Haftfestigkeit betrachtet, sondern als Indikator für die Klebeleistung (Haftfähigkeit) bei Nässe.
Ein Verfahren zum Benetzen des Holzsubstrates wird beschrieben. Das Prüfverfahren eignet sich nur für Holz und auf Holz basierende Substrate.
Für Trockenhaftfestigkeit kann das Prüfverfahren ohne Benetzen durchgeführt werden; in diesem Fall weicht es nur geringfügig von EN ISO 4624 ab.

Peintures et vernis - Produits de peinture et systèmes de peinture pour le bois extérieur - Partie 9 : Détermination de la résistance à l’arrachement

Le présent document spécifie une méthode d'évaluation de la résistance d'un système de peinture sur
bois humide à la séparation du subjectile en mesurant la force nécessaire pour détacher ou rompre le
système de peinture par une contrainte de traction normale appliquée au moyen d'un goujon (plot). Des
informations supplémentaires sont obtenues en notant le type et l'emplacement de la rupture. La force
requise pour le décollement dépendra de plusieurs facteurs, notamment de l'adhérence du revêtement
au subjectile et entre les couches intermédiaires du revêtement. Le mode opératoire n'est pas considéré
comme un moyen direct de mesure de l'adhésion, mais comme un indicateur de la performance adhésive
(adhérence) dans des conditions humides.
Une méthode de mouillage du subjectile en bois est décrite. La méthode d'essai convient uniquement aux
subjectiles en bois et en matériaux dérivés du bois.
Pour l'adhérence en condition sèche, la méthode d'essai peut être utilisée sans mouillage, auquel cas elle
diffèrera très peu de l'EN ISO 4624.

Barve in laki - Premazi in premazni sistemi za zaščito lesa za zunanjo uporabo - 9. del: Ugotavljanje razslojne trdnostii

Ta tehnična specifikacija določa metodo za ocenjevanje odpornosti premaznih sistemov na mokrem lesu proti ločevanju od podlage z merjenjem sile, ki je potrebna, da se premazni sistem odtrga ali pretrga z uporabo normalnega natega prek pritrjenega podpornika. Dodatne informacije se lahko pridobijo z zapisom vrste in lokacije okvare. Sila, potrebna za odtrganje, bo odvisna od različnih dejavnikov, vključno s sprijemnostjo premaza s podlago in med vmesnimi plastmi premaza. Postopek ni mišljen kot neposredno sredstvo za merjenje sprijemnosti, temveč kot kazalnik sprijemne učinkovitosti (sprijetosti) v mokrih pogojih.
Opisan je postopek za močenje lesnega substrata. Preskusna metoda je primerna samo za lesne substrate in substrate na osnovi lesa.
Preskusno metodo je za suho sprijemnost dovoljeno izvesti brez močenja, pri čemer se nekoliko razlikuje od standarda EN ISO 4624.

General Information

Status
Published
Public Enquiry End Date
02-Nov-2022
Publication Date
05-Apr-2023
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
08-Mar-2023
Due Date
13-May-2023
Completion Date
06-Apr-2023

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SLOVENSKI STANDARD
SIST-TS CEN/TS 927-9:2023
01-maj-2023
Nadomešča:
SIST-TS CEN/TS 927-9:2019
Barve in laki - Premazi in premazni sistemi za zaščito lesa za zunanjo uporabo - 9.
del: Ugotavljanje razslojne trdnostii
Paints and varnishes - Coating materials and coating systems for exterior wood - Part 9:
Determination of pull-off strength
Beschichtungsstoffe - Beschichtungsstoffe und Beschichtungssysteme für Holz im
Außenbereich - Teil 9: Bestimmung der Abreißfestigkeit
Peintures et vernis - Produits de peinture et systèmes de peinture pour le bois extérieur -
Partie 9 : Détermination de la résistance à l’arrachement
Ta slovenski standard je istoveten z: CEN/TS 927-9:2023
ICS:
71.100.50 Kemikalije za zaščito lesa Wood-protecting chemicals
87.040 Barve in laki Paints and varnishes
SIST-TS CEN/TS 927-9:2023 en,fr
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST-TS CEN/TS 927-9:2023

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SIST-TS CEN/TS 927-9:2023


CEN/TS 927-9
TECHNICAL SPECIFICATION

SPÉCIFICATION TECHNIQUE

January 2023
TECHNISCHE SPEZIFIKATION
ICS 87.040 Supersedes CEN/TS 927-9:2018
English Version

Paints and varnishes - Coating materials and coating
systems for exterior wood - Part 9: Determination of pull-
off strength
Peintures et vernis - Produits de peinture et systèmes Beschichtungsstoffe - Beschichtungsstoffe und
de peinture pour le bois extérieur - Partie 9 : Beschichtungssysteme für Holz im Außenbereich - Teil
Détermination de la résistance à l'arrachement 9: Bestimmung der Abreißfestigkeit
This Technical Specification (CEN/TS) was approved by CEN on 18 December 2022 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 927-9:2023 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
SIST-TS CEN/TS 927-9:2023
CEN/TS 927-9:2023 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 5
5 Apparatus and materials . 6
5.1 Test apparatus. 6
5.2 Test dollies . 6
5.3 Adhesives . 6
6 Test panels . 7
6.1 Wood substrate . 7
6.2 Conditioning . 7
6.3 Coating of test panels . 7
6.3.1 Coated panels not exposed to weathering . 7
6.3.2 Coated panels exposed to weathering . 7
7 Procedure. 8
7.1 Testing conditions . 8
7.2 Preparation of the samples . 8
7.3 Order of the test samples . 8
7.3.1 Non-standard panels . 8
7.3.2 Standard EN 927 exposure panels . 8
7.4 Testing procedure . 10
7.5 Evaluation of fracture . 10
8 Calculation and expression of results . 11
9 Precision statement . 11
10 Test report . 11
Annex A (informative) Interpretation of test results . 13
Bibliography . 14

2

---------------------- Page: 4 ----------------------
SIST-TS CEN/TS 927-9:2023
CEN/TS 927-9:2023 (E)
European foreword
This document (CEN/TS 927-9:2023) has been prepared by Technical Committee CEN/TC 139 “Paints
and varnishes”, the secretariat of which is held by DIN.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes CEN/TS 927-9:2018.
CEN/TS 927-9:2023 includes the following significant technical changes with respect to
CEN/TS 927-9:2018:
— the title has been modified.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN/CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
3

---------------------- Page: 5 ----------------------
SIST-TS CEN/TS 927-9:2023
CEN/TS 927-9:2023 (E)
Introduction
This document is one of two methods for assessing the resistance of the coating system to removal by
external forces provided by either cross-cutting or direct pull-off, both methods carried out under wet
conditions. Two existing ISO Standards (EN ISO 2409 and EN ISO 4624) specify similar test methods for
dry substrates in general, but make no provision for wet conditions, where wood coatings are known to
be particularly vulnerable. Both of the new methods take full account of the special nature of wood as a
substrate in terms of the method of wetting and the selection of the substrate.
Most of the currently used exterior coating systems are characterized by their propensity to being
penetrated by moisture both into and out of the wood. It might therefore be difficult to achieve a good
adhesion of these coatings under high moisture conditions. In cases of an already damaged coating film
or an increased presence of moisture in the boundary zone to the wood surface, even a short-term
exposure to water can be sufficient to weaken the adhesion of a coating film either to the substrate or
within the coating system. The described method is suitable for the testing of coatings for exterior wood
or wood-based materials and applicable for testing the wet adhesion of a single coat or multi-coat system.
In this test procedure the force, which is necessary to detach or pull-off the coating perpendicular to the
substrate is measured.
Furthermore, the nature of fracture of the coating is assessed to validate or reject and assist in the
interpretation of the result.
4

---------------------- Page: 6 ----------------------
SIST-TS CEN/TS 927-9:2023
CEN/TS 927-9:2023 (E)
1 Scope
This document specifies a method for assessing the resistance of a coating system on wet wood to
separation from the substrate by measuring the force necessary to detach or rupture the coating system
by a normal tensile strain applied through an attached stud (dolly). Additional information is gained by
noting the type and locus of failure. The force required for detachment will depend on several factors
including the adhesion of the coating to the substrate and between intermediate coating layers. The
procedure is not regarded as a direct means of measuring adhesion but an indicator of adhesive
performance (adherence) under wet conditions.
A procedure for wetting the wood substrate is described. The test method is only suitable for wood and
wood-based substrates.
For dry adhesion the test method can be carried out without wetting, in which case it will differ very little
from EN ISO 4624.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 927-3, Paints and varnishes — Coating materials and coating systems for exterior wood — Part 3:
Natural weathering test
EN 927-6, Paints and varnishes — Coating materials and coating systems for exterior wood — Part 6:
Exposure of wood coatings to artificial weathering using fluorescent UV lamps and water
EN 23270, Paints and varnishes and their raw materials — Temperatures and humidities for conditioning
and testing (ISO 3270)
EN ISO 4624:2016, Paints and varnishes — Pull-off test for adhesion (ISO 4624:2016)
3 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
• ISO Online browsing platform: available at https://www.iso.org/obp
• IEC Electropedia: available at https://www.electropedia.org/
4 Principle
The product or system under test is applied at uniform thickness to flat wood-based panels of uniform
surface texture.
After drying/curing the coating system, dollies are glued directly to the surface of the coated panels.
After curing of the adhesive, a circular groove is milled or cut around the dollies. Water is deposited in
the groove for a time interval that ensures a complete wetting of the wood–coating interface beneath the
dollies.
After the complete wetting of the wood-coating interphase the bonded dolly/substrate assemblies are
placed in a suitable tensile tester. The bonded assemblies are subjected to a controlled tensile test (pull-
off test) and the force required to break is measured.
5

---------------------- Page: 7 ----------------------
SIST-TS CEN/TS 927-9:2023
CEN/TS 927-9:2023 (E)
The test result is the tensile stress necessary to break the weakest interface (adhesive failure) or the
weakest component (cohesive failure) of the test assembly. Mixed adhesive/cohesive failure can also
occur and should be recorded as shown in Table 1.
5 Apparatus and materials
5.1 Test apparatus
Mobile test apparatus or tension testing machines as described in EN ISO
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 927-9:2022
01-oktober-2022
Barve in laki - Premazi in premazni sistemi za zaščito lesa za zunanjo uporabo - 9.
del: Ugotavljanje razslojne trdnosti po izpostavitvi vodi
Paints and varnishes - Coating materials and coating systems for exterior wood - Part 9:
Determination of pull-off strength after water exposure
Beschichtungsstoffe ¿ Beschichtungsstoffe und Beschichtungssysteme für Holz im
Außenbereich ¿ Teil 9: Bestimmung der Abreißfestigkeit nach Wasserbeanspruchung
Peintures et vernis - Produits de peinture et systèmes de peinture pour le bois extérieur -
Partie 9 : Détermination de la résistance à l’arrachement après exposition à l’eau
Ta slovenski standard je istoveten z: FprCEN/TS 927-9
ICS:
71.100.50 Kemikalije za zaščito lesa Wood-protecting chemicals
87.040 Barve in laki Paints and varnishes
kSIST-TS FprCEN/TS 927-9:2022 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 927-9:2022

---------------------- Page: 2 ----------------------
kSIST-TS FprCEN/TS 927-9:2022


FINAL DRAFT
TECHNICAL SPECIFICATION
FprCEN/TS 927-9
SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION

August 2022
ICS Will supersede CEN/TS 927-9:2018
English Version

Paints and varnishes - Coating materials and coating
systems for exterior wood - Part 9: Determination of pull-
off strength after water exposure
Peintures et vernis - Produits de peinture et systèmes Beschichtungsstoffe ¿ Beschichtungsstoffe und
de peinture pour le bois extérieur - Partie 9 : Beschichtungssysteme für Holz im Außenbereich ¿ Teil
Détermination de la résistance à l'arrachement après 9: Bestimmung der Abreißfestigkeit nach
exposition à l'eau Wasserbeanspruchung


This draft Technical Specification is submitted to CEN members for Vote. It has been drawn up by the Technical Committee
CEN/TC 139.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change
without notice and shall not be referred to as a Technical Specification.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 927-9:2022 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 927-9:2022
FprCEN/TS 927-9:2022 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Principle . 5
5 Apparatus and materials . 6
5.1 Test apparatus. 6
5.2 Test dollies . 6
5.3 Adhesives . 6
6 Test panels . 7
6.1 Wood substrate . 7
6.2 Conditioning . 7
6.3 Coating of test panels . 7
6.3.1 Coated panels not exposed to weathering . 7
6.3.2 Coated panels exposed to weathering . 7
7 Procedure. 8
7.1 Testing conditions . 8
7.2 Preparation of the samples . 8
7.3 Order of the test samples . 8
7.3.1 Non-standard panels . 8
7.3.2 Standard EN 927 exposure panels . 8
7.4 Testing procedure . 10
7.5 Evaluation of fracture . 10
8 Calculation and expression of results . 11
9 Precision statement . 11
10 Test report . 11
Annex A (informative) Interpretation of test results . 13
Bibliography . 14

2

---------------------- Page: 4 ----------------------
kSIST-TS FprCEN/TS 927-9:2022
FprCEN/TS 927-9:2022 (E)
European foreword
This document (FprCEN/TS 927-9:2022) has been prepared by Technical Committee CEN/TC 139
“Paints and varnishes”, the secretariat of which is held by DIN.
This document is currently submitted to the Vote on TS.
This document will supersede CEN/TS 927-9:2018.
3

---------------------- Page: 5 ----------------------
kSIST-TS FprCEN/TS 927-9:2022
FprCEN/TS 927-9:2022 (E)
Introduction
This document is one of two methods for assessing the resistance of the coating system to removal by
external forces provided by either cross-cutting or direct pull-off, both methods carried out under wet
conditions. Two existing ISO Standards (EN ISO 2409 and EN ISO 4624) specify similar test methods for
dry substrates in general, but make no provision for wet conditions, where wood coatings are known to
be particularly vulnerable. Both of the new methods take full account of the special nature of wood as a
substrate in terms of the method of wetting and the selection of the substrate.
Most of the currently used exterior coating systems are characterized by their propensity to being
penetrated by moisture both into and out of the wood. It might therefore be difficult to achieve a good
adhesion of these coatings under high moisture conditions. In cases of an already damaged coating film
or an increased presence of moisture in the boundary zone to the wood surface, even a short-term
exposure to water can be sufficient to weaken the adhesion of a coating film either to the substrate or
within the coating system. The described method is suitable for the testing of coatings for exterior wood
or wood-based materials and applicable for testing the wet adhesion of a single coat or multi-coat system.
In this test procedure the force, which is necessary to detach or pull-off the coating perpendicular to the
substrate is measured.
Furthermore, the nature of fracture of the coating is assessed to validate or reject and assist in the
interpretation of the result.
4

---------------------- Page: 6 ----------------------
kSIST-TS FprCEN/TS 927-9:2022
FprCEN/TS 927-9:2022 (E)
1 Scope
This document specifies a method for assessing the resistance of a coating system on wet wood to
separation from the substrate by measuring the force necessary to detach or rupture the coating system
by a normal tensile strain applied through an attached stud (dolly). Additional information is gained by
noting the type and locus of failure. The force required for detachment will depend on several factors
including the adhesion of the coating to the substrate and between intermediate coating layers. The
procedure is not regarded as a direct means of measuring adhesion but an indicator of adhesive
performance (adherence) under wet conditions.
A procedure for wetting the wood substrate is described. The test method is only suitable for wood and
wood-based substrates.
For dry adhesion the test method can be carried out without wetting, in which case it will differ very little
from EN ISO 4624.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
EN 927-3, Paints and varnishes - Coating materials and coating systems for exterior wood - Part 3: Natural
weathering test
EN 927-6, Paints and varnishes - Coating materials and coating systems for exterior wood - Part 6: Exposure
of wood coatings to artificial weathering using fluorescent UV lamps and water
EN 23270, Paints and varnishes and their raw materials - Temperatures and humidities for conditioning
and testing (ISO 3270)
EN ISO 4624:2016, Paints and varnishes - Pull-off test for adhesion (ISO 4624:2016)
3 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
• IEC Electropedia: available at https://www.electropedia.org/
• ISO Online browsing platform: available at https://www.iso.org/obp
4 Principle
The product or system under test is applied at uniform thickness to flat wood-based panels of uniform
surface texture.
After drying/curing the coating system, dollies are glued directly to the surface of the coated panels.
After curing of the adhesive, a circular groove is milled or cut around the dollies. Water is deposited in
the groove for a time interval that ensures a complete wetting of the wood–coating interface beneath the
dollies.
After the complete wetting of the wood-coating interphase the bonded dolly/substrate assemblies are
placed in a suitable tensile tester. The bonded assemblies are subjected to a controlled tensile test (pull-
off test) and the force required to break is measured.
5

---------------------- Page: 7 ----------------------
kSIST-TS FprCEN/TS 927-9:2022
FprCEN/TS 927-9:2022 (E)
The test result is the tensile stress necessary to break the weakest interface (adhesive failure) or the
weakest component (cohesive failure) of the test assembly. Mixed adhesive/cohesive failure can also
occur and should be recorded as shown in Table 1.
5 Apparatus and materials
5.1 Test apparatus
Mobile test apparatus or tension testing machines as described in EN ISO 4624. The tensile stress shall
be applied in a direction perpendicular to the plane of the coated substrate and shall be increased at a
substantially uniform rate, not greater than 1 MPa/s, such that failure of the test assembly occurs within
90 s. Suitable designs for applying the tensile stress are shown in EN ISO 4624:2016, 5.1 Figures 1 and 2,
or in 5.1, Figure 1 (below).
The apparatus shall permit recording of the applied force with an accuracy of ± 1 %.
It is permissible to use different types of pull
...

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