Bitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method

This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions.
WARNING  The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Bitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit Feinmineralstoff

Diese Europäische Norm legt ein Verfahren zur Bestimmung des Brechwertes kationischer Bitumenemulsio-nen fest.
WARNUNG - Die Anwendung dieser Norm kann den Umgang mit gefährlichen Substanzen und Aus¬rüstungsteilen und die Ausführung gefährlicher Arbeitsgänge einschließen. Diese Norm erhebt nicht den Anspruch, alle mit ihrer Anwendung verbundenen Sicherheitsprobleme anzusprechen. Es liegt in der Verantwortung des Anwenders dieser Norm, geeignete Verhaltensregeln für den Arbeits- und Gesundheitsschutz festzulegen und vor der Anwendung zu klären, ob einschränkende Vorschriften zu berücksichtigen sind.

Bitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minérales

La présente Nome européenne décrit une méthode de détermination de l’indice de rupture des émulsions
cationiques de bitume.
AVERTISSEMENT - L’utilisation de la présente Norme européenne implique l'intervention de produits,
d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n'a pas la prétention
d'aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité de
l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer
l'applicabilité des restrictions réglementaires avant utilisation.

Bitumen in bitumenska veziva - Določevanje stopnje stabilnosti - 1. del: Določevanje hitrosti razpada kationskih bitumenskih emulzij, metoda z mineralnim polnilom

General Information

Status
Withdrawn
Public Enquiry End Date
04-Jan-2009
Publication Date
11-Jun-2009
Withdrawal Date
01-Aug-2012
Technical Committee
Current Stage
9900 - Withdrawal (Adopted Project)
Start Date
02-Aug-2012
Due Date
25-Aug-2012
Completion Date
02-Aug-2012

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.SROQLORPBitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit FeinmineralstoffBitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minéralesBitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13075-1:2009SIST EN 13075-1:2009en,fr,de01-julij-2009SIST EN 13075-1:2009SLOVENSKI
STANDARDSIST EN 13075-1:20031DGRPHãþD



SIST EN 13075-1:2009



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13075-1March 2009ICS 75.140; 91.100.50Supersedes EN 13075-1:2002
English VersionBitumen and bituminous binders - Determination of breakingbehaviour - Part 1: Determination of breaking value of cationicbituminous emulsions, mineral filler methodBitumes et liants bitumineux - Détermination ducomportement à la rupture - Partie 1 : Détermination del'indice de rupture des émulsions cationiques de bitume,méthode des fines minéralesBitumen und bitumenhaltige Bindemittel - Bestimmung desBrechverhaltens - Teil 1: Bestimmung des Brechwerteskationischer Bitumenemulsionen, Verfahren mitFeinmineralstoffThis European Standard was approved by CEN on 10 February 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre:
Avenue Marnix 17,
B-1000 Brussels© 2009 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13075-1:2009: ESIST EN 13075-1:2009



EN 13075-1:2009 (E) 2 Contents Page Foreword .3 1 Scope .4 2 Normative references .4 3 Terms and definitions .4 4 Principle .4 5 Reagents and materials .4 6 Apparatus .5 7 Sampling .6 8 Procedure .6 9 Calculation .7 10 Expression of results .7 11 Precision .7 12 Test report .8 Annex A (normative)
Characteristics of the Sikaisol filler . 13 Bibliography . 14
SIST EN 13075-1:2009



EN 13075-1:2009 (E) 3 Foreword This document (EN 13075-1:2009) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2009, and conflicting national standards shall be withdrawn at the latest by September 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 13075-1:2002. This European Standard, EN 13075, consists of the following parts under the general title Bitumen and bituminous binders – Determination of breaking behaviour: Part 1 – Determination of breaking value of cationic bituminous emulsions, mineral filler method; Part 2 – Determination of fines mixing time of cationic bituminous emulsions. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom.
SIST EN 13075-1:2009



EN 13075-1:2009 (E) 4 1 Scope This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders – Sampling bituminous binders EN 12594, Bitumen and bituminous binders – Preparation of test samples 3 Terms and definitions For the purposes of this document, the following term and definition applies. 3.1 breaking value dimensionless number corresponding to the amount of reference filler, in grams, needed to coagulate 100 g of bitumen emulsion 4 Principle A reference filler is added at a uniform rate to a specified quantity of stirred cationic bitumen emulsion. When the emulsion has broken completely, the amount of added filler is determined by weighing. The mass of filler (in grams) multiplied by 100 and divided by the amount of emulsion (in grams) is the breaking value. NOTE The cationic or anionic nature of an emulsion can be determined with EN 1430 [1]. 5 Reagents and materials 5.1 Reference filler The Sikaisol filler1 (characteristics are given in Annex A) shall be used as the reference filler. Other filler such as the Forshammer filler may be used as an alternative to the Sikaisol filler. In the event of dispute, the Sikaisol filler shall be used. 5.2 Cleaning agents, as used conventionally in laboratories.
1 This information is given for the convenience of users of this European Standard and does not constitute an endorsement by CEN of the product name. Equivalent products may be used if they can be shown to lead to the same results, or if a correlation between the products has been established. SIST EN 13075-1:2009



EN 13075-1:2009 (E) 5 6 Apparatus 6.1 General
Usual laboratory apparatus and glassware, together with specific equipment that is described below depending on the used procedure (semi-automatic or manual). An explanatory sketch of the equipment set-up is shown in Figure 1 for the semi-automatic procedure.
6.2 Equipment for semi-automatic procedure 6.2.1 Stirrer motor, as shown in Figure 1, with
...

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.SROQLORPBitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 1: Bestimmung des Brechwertes kationischer Bitumenemulsionen, Verfahren mit FeinmineralstoffBitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 1 : Détermination de l'indice de rupture des émulsions cationiques de bitume, méthode des fines minéralesBitumen and bituminous binders - Determination of breaking behaviour - Part 1: Determination of breaking value of cationic bituminous emulsions, mineral filler method91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:prEN 13075-1kSIST prEN 13075-1:2008en,fr,de01-december-2008kSIST prEN 13075-1:2008SLOVENSKI
STANDARD



kSIST prEN 13075-1:2008



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMFINAL DRAFTprEN 13075-1October 2008ICS 75.140; 91.100.50Will supersede EN 13075-1:2002
English VersionBitumen and bituminous binders - Determination of breakingbehaviour - Part 1: Determination of breaking value of cationicbituminous emulsions, mineral filler methodBitumes et liants bitumineux - Détermination ducomportement à la rupture - Partie 1 : Détermination del'indice de rupture des émulsions cationiques de bitume,méthode des fines minéralesBitumen und bitumenhaltige Bindemittel - Bestimmung desBrechverhaltens - Teil 1: Bestimmung des Brechwerteskationischer Bitumenemulsionen, Verfahren mitFeinmineralsotoffThis draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the TechnicalCommittee CEN/TC 336.If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations whichstipulate the conditions for giving this European Standard the status of a national standard without any alteration.This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other languagemade by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has thesame status as the official versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice andshall not be referred to as a European Standard.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2008 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. prEN 13075-1:2008: EkSIST prEN 13075-1:2008



prEN 13075-1:2008 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Normative references.4 3 Terms and definitions.4 4 Principle.4 5 Reagents and materials.4 6 Apparatus.5 7 Sampling.6 8 Procedure.6 9 Calculation.7 10 Expression of results.7 11 Precision.7 12 Test report.8 Annex A (normative)
Characteristics of the Sikaisol filler.13 Bibliography.14
kSIST prEN 13075-1:2008



prEN 13075-1:2008 (E) 3 Foreword This document (prEN 13075-1:2008) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This document is currently submitted to the Unique Acceptance Procedure. This document will supersede EN 13075-1:2002. This European Standard, EN 13075, consists of the following parts under the general title Bitumen and bituminous binders – Determination of breaking behaviour: Part 1 – Determination of breaking value of cationic bituminous emulsions, mineral filler method; Part 2 – Determination of fines mixing time of cationic bituminous emulsions. kSIST prEN 13075-1:2008



prEN 13075-1:2008 (E) 4 1 Scope This European Standard specifies a method for the determination of the breaking value of cationic bituminous emulsions. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders – Sampling bituminous binders EN 12594, Bitumen and bituminous binders – Preparation of test samples 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 breaking value dimensionless number corresponding to the amount of reference filler, in grams, needed to coagulate 100 g of bitumen emulsion 4 Principle A reference filler is added at a uniform rate to a specified quantity of stirred cationic bitumen emulsion. When the emulsion has broken completely, the amount of added filler is determined by weighing. The mass of filler (in grams) multiplied by 100 and divided by the amount of emulsion (in grams) is the breaking value. NOTE The cationic or anionic nature of an emulsion can be determined with EN 1430 [1]. 5 Reagents and materials 5.1 Reference filler The Sikaisol filler1 (characteristics are given in Annex A) shall be used as the reference filler. Other filler such as the Forshammer filler may be used as an alternative to the Sikaisol filler. In the event of dispute, the Sikaisol filler shall be used. 5.2 Cleaning agents, as used conventionally in laboratories.
1 This information is given for the convenience of users of this European Standard and does not constitute an endorsement by CEN of the product name. Equivalent products may be used if they can be shown to lead to the same results, or if a correlation between the products has been established. kSIST prEN 13075-1:2008



prEN 13075-1:2008 (E) 5 6 Apparatus Usual laboratory apparatus and glassware, together with specific equipments which are described hereafter depending on the used procedure (semi-automatic or manual). An explanatory sketch of the equipment set-up is shown in Figure 1 in the case of the semi-automatic procedure.
6.1 Equipment for semi-automatic procedure 6.1.1 Stirrer motor, as shown in Figure 1, with an output power of a
...

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