Standard Specification for Perfluoroalkoxy (PFA)-Fluoropolymer Tubing

ABSTRACT
This specification covers tubing produced from PFA fluoropolymer resins which are cited in another specification. This document specifies tubing dimensional tolerances, tensile properties and related electrical properties as noted in the appropriate tables when tested in accordance with the methods cited. Different tests shall be performed in order to determine the following properties of resins: inside diameter, wall thickness, specific gravity, tensile strength, elongation, and dimensional stability.
SCOPE
1.1 This specification covers tubing produced from PFA Fluoropolymer resins which are cited in Specification D 3307. This document specifies tubing dimensional tolerances, tensile properties and related electrical properties as noted in the appropriate tables when tested in accordance with the methods cited in this specification. This specification is for virgin material only and does not address recycled material, as it is not appropriate for PFA tubing.
Note 1—Abbreviations are in accordance with Terminology D 1600.
Note 2—There is no known ISO equivalent to this specification.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.3 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D6867 −03(Reapproved 2009)
Standard Specification for
Perfluoroalkoxy (PFA)-Fluoropolymer Tubing
This standard is issued under the fixed designation D6867; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D4894 Specification for Polytetrafluoroethylene (PTFE)
Granular Molding and Ram Extrusion Materials
1.1 This specification covers tubing produced from PFA
IEEE/ASTM SI 10 Standard for Use of the International
Fluoropolymer resins which are cited in Specification D3307.
System of Units (SI): The Modern Metric System
This document specifies tubing dimensional tolerances, tensile
properties and related electrical properties as noted in the
3. Terminology
appropriate tables when tested in accordance with the methods
cited in this specification. This specification is for virgin 3.1 Definitions:
material only and does not address recycled material, as it is
3.1.1 Definitions are in accordance with Terminology D883
not appropriate for PFA tubing.
unless otherwise specified.
NOTE 1—Abbreviations are in accordance with Terminology D1600.
3.1.2 lot, n—one continuous production run or a uniform
NOTE 2—There is no known ISO equivalent to this specification.
blend of two or more production runs of one size sheet or
1.2 The values stated in SI units are to be regarded as
molded basic shape.
standard. The values given in parentheses are for information
only.
4. Physical Requirements
1.3 The following safety hazards caveat pertains only to the
4.1 The tubing shall be made of PFA-fluoropolymer resin
test methods portion, Section 7, of this specification. This
meeting the requirements of Specification D3307.
standard does not purport to address all of the safety concerns,
4.2 Theinsidediameterandwallthicknessandtolerancesof
if any, associated with its use. It is the responsibility of the user
the tubing shall be as shown in Table 1, when determined in
of this standard to establish appropriate safety and health
accordance with 7.1.3.1 and 7.1.3.2.
practices and determine the applicability of regulatory require-
4.3 The specific gravity of the tubing shall be between 2.12
ments prior to use.
and 2.17 inclusive when determined in accordance with 7.1.4.
2. Referenced Documents
4.4 The tubing shall have a minimum tensile strength of
2.1 ASTM Standards: 10.0 MPa (1500 psi) and a minimum elongation of 200 %
when determined in accordance with 7.1.5.
D618 Practice for Conditioning Plastics for Testing
D792 Test Methods for Density and Specific Gravity (Rela-
4.5 The tubing shall remain free from cracks and exhibit no
tive Density) of Plastics by Displacement
splitting when tested for dimensional stability in accordance
D883 Terminology Relating to Plastics
with 7.1.6.
D1600 Terminology forAbbreviatedTerms Relating to Plas-
tics
5. Sampling
D1675 Test Methods for Polytetrafluoroethylene Tubing
5.1 Sampling shall be statistically adequate to satisfy the
D3307 Specification for Perfluoroalkoxy (PFA)-
requirements of 8.2.
Fluorocarbon Resin Molding and Extrusion Materials
6. Number of Tests and Retests
6.1 One set of five test specimens shall be considered
This specification is under the jurisdiction of ASTM Committee D20 on
Plastics and is the direct responsibility of Subcommittee D20.15 on Thermoplastic
sufficient for testing each batch. The average result of the
Materials.
specimens tested shall conform to the requirements of this
Current edition approved Sept. 1, 2009. Published September 2009. Originally
specification.
approved in 2003. Last previous edition approved in 2003 as D6867 - 03. DOI:
10.1520/D6867-03R09.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on Available from ASTM International Headquarters, 100 Barr Harbor Drive, PO
the ASTM website. Box C700, West Conshohocken, PA 19428–2959.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D6867−03 (2009)
TABLE 1 Dimensions and Tolerances for PFA-Fluorocarbon Tubing-Dimensions, mm (in.)
Inside Diameter Wall Thickness
Nominal Inside Diameter, Inside Diameter Tolerance, Nominal Thickness, Thickness Tolerance,
mm (in.) mm (in.) mm (in.) mm (in.)
0 to 0.25 (0.000 to 0.010) ±0.03 (0.001) 0 to 0.13 (0.000 to 0.005) ±0.030 (0.001)
0.26 to 0.50 (0.011 to 0.020) ±0.05 (0.002) 0.14 to 0.30 (0.006 to 0.012) ±0.050 (0.002)
0.51 to 0.75 (0.021 to 0.030) ±0.08 (0.003) 0.31 to 0.48 (0.013 to 0.019) ±0.080 (0.003)
0.76 to 2.54 (0.031 to 0.100) ±0.10 (0.004) 0.49 to 0.74 (0.020 to 0.029) ±0.100 (0.004)
2.55 to 4.32 (0.101 to 0.170) ±0.13 (0.005) 0.75 and >(0.030 and >) ±0.130 (0.005)
4.33 to 6.35 (0.171 to 0.250) ±0.15 (0.006)
6.36 to 19.05 (0.251 to 0.750) ±0.18 (0.007)
19.06 to 25.39 (0.751 to 0.999) ±0.25 (0.010)
25.4 and (1.000 and >) ±0.38 (0.015)
7. Test Methods 7.1.5.1 Tubing Having an Inside Diameter of 15.9 mm
(0.625 in.) and Over—Determine the tensile strength and
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D6867–03 Designation: D 6867 – 03 (Reapproved 2009)
Standard Specification for
Perfluoroalkoxy (PFA)-Fluoropolymer Tubing
This standard is issued under the fixed designation D 6867; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers tubing produced from PFA Fluoropolymer resins which are cited in Specification D 3307. This
document specifies tubing dimensional tolerances, tensile properties and related electrical properties as noted in the appropriate
tables when tested in accordance with the methods cited in this specification.This specification is for virgin material only and does
not address recycled material, as it is not appropriate for PFA tubing.
NOTE 1—Abbreviations are in accordance with Terminology D 1600.
NOTE 2—There is no similarknown ISO standard. equivalent to this specification.
1.2 The values stated in SI units are to be regarded as the standard. The values given in bracketsparentheses are for information
only.
1.3 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification. This standard
does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this
standard to establish appropriate safety and health practices and determine the applicability of regulatory requirements prior to
use.
2. Referenced Documents
2.1 ASTM Standards:
D 618 Practice for Conditioning Plastics for Testing
D 792 Test Methods for Density and Specific Gravity (Relative Density) of Plastics by Displacement
D 883 Terminology Relating to Plastics
D 1600 Terminology for Abbreviated Terms Relating to Plastics
D 1675 Test Methods for Polytetrafluoroethylene Tubing
D 3307 Specification for Perfluoroalkoxy (PFA)-Fluorocarbon Resin Molding and Extrusion Materials
D 4894 Specification for Polytetrafluoroethylene (PTFE) Granular Molding and Ram Extrusion Materials
IEEE/ASTM SI 10 Standard for Use of the International System of Units (SI): The Modern Metric System
3. Terminology
3.1 Definitions—Definitions are in accordance with Terminology D 883 unless otherwise specified.
3.1.1 lot, n—onecontinuousproductionrunorauniformblendoftwoormoreproductionrunsofonesizesheetormoldedbasic
shape.
4. Physical Requirements
4.1 The tubing shall be made of PFA-fluoropolymer resin meeting the requirements of Specification D 3307.
4.2 The inside diameter and wall thickness and tolerances of the tubing shall be as shown in Table 1, when determined in
accordance with 7.1.3.1 and 7.1.3.2.
4.3 The specific gravity of the tubing shall be between 2.12 and 2.17 inclusive when determined in accordance with 7.1.4.
4.4 The tubing shall have a minimum tensile strength of 10.0 MPa [1500 psi](1500 psi) and a minimum elongation of 200 %
when determined in accordance with 7.1.5.
This specification is under the jurisdiction of ASTM Committee D20 on Plastics and is the direct responsibility of Subcommittee D20.15 on Thermoplastic Materials.
Current edition approved July 10, 2003. Published August 2003.
Current edition approved Sept. 1, 2009. Published September 2009. Originally approved in 2003. Last previous edition approved in 2003 as D 6867 - 03.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 08.01.volume information, refer to the standard’s Document Summary page on the ASTM website.
Annual Book of ASTM Standards, Vol 10.01.
Available from ASTM International Headquarters, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428–2959.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D 6867 – 03 (2009)
TABLE 1 Dimensions and Tolerances for PFA-Fluorocarbon Tubing-Dimensions, mm [ (in.])
Inside Diameter Wall Thickness
Nominal Inside Diameter, Inside Diameter Tolerance, Nominal Thickness, Thickness Tolerance,
mm [ (in.]) mm [ (in.]) mm [ (in.]) mm [ (in.])
0 to 0.25 [0.000 to 0.010] 60.03 [0.001] 0 to 0.13 [0.000 to 0.005] 60.030 [0.001]
0 to 0.25 (0.000 to 0.010) 60.03 (0.001) 0 to 0.13 (0.000 to 0.005) 60.030 (0.001)
0.26 to 0.50 [0.011 to 0.020] 60.05 [0.002] 0.14 to 0.30 [0.006 to 0.012] 60.050 [0.002]
0.26 to 0.50 (0.011 to 0.020) 60.05 (0.002) 0.14 to 0.30 (0.006 to 0.012) 60.050 (0.002)
0.51 to 0.75 [0.021 to 0.030] 60.08 [0.003] 0.31 to 0.48 [0.013 to 0.019] 60.080 [0.003]
0.51 to 0.75 (0.021 to 0.030) 60.08 (0.003) 0.31 to 0.48 (0.013 to 0.019) 60.080 (0.003)
0.76 to 2.54 [0.031 to 0.100] 60.10 [0.004] 0.49 to 0.74 [0.020 to 0.029] 60.100 [0.004]
0.76 to 2.54 (0.031 to 0.100) 60.10 (0.004) 0.49 to 0.74 (0.020 to 0.029) 60.100 (0.004)
2.55 to 4.32 [0.101 to 0.170] 60.13 [0.005] 0.75 and[0.030 and] 60.130 [0.005]
2.55 to 4.32 (0.101 to 0.170) 60.13 (0.005) 0.75 and >(0.030 and >) 60.130 (0.005)
4.33 to 6.35 [0.171 to 0.250] 60.15 [0.006]
4.33 to 6.35 (0.171 to 0.250) 60.15 (0.006)
6.36 to 19.05 [0.251 to 0.750] 60.18 [0.007]
6.36 to 19.05 (0.251 to 0.750) 60.18 (0.007)
19.06 to 25.39 [0.751 to 0.999] 60.25 [0.010]
19.06 to 25.39 (0.751 to 0.999) 60.25 (0.010)
25.4 and [1.000 and] 60.38 [0.015]
25.4 and (1.000 and >) 60.38
...

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