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ASTM D629-99

(Test Method)

Standard Test Methods for Quantitative Analysis of Textiles

Standard Test Methods for Quantitative Analysis of Textiles

SCOPE
1.1 These test methods cover procedures for the determination of the fiber blend composition of mixtures of the fibers listed in 1.2. Procedures for quantitative estimation of the amount of moisture and certain nonfibrous materials in textiles are also described, for use in the analysis of mixtures, but these are not the primary methods for the determination of moisture content for commercial weights.  
1.2 These test methods cover procedures for the following fiber types:  
1.2.1 Natural Fibers:  
1.2.1.1 Cellulose-Base Fibers: Cotton Hemp Flax Ramie  
1.2.1.2 Protein-Base Fibers: Animal hairs (other than wool) Silk, cultivated Silk, Tussah Wool  
1.2.2 Man-Made Fibers:  
1.2.2.1 Cellulose-Base Fibers: Acetate (secondary) Rayon, viscose or cuprammonium Triacetate  
1.2.2.2 Synthetic-Base Fibers: Acrylic Aramid Modacrylic Nylon 6, Nylon 6-6, others Olefin Polyester Spandex  
1.3 These test methods include the following sections and tables:  Section Referenced Documents 2 Terminology 3 Summary of Methods 4 Uses and Significance 5 Sampling 6 Purity of Reagents 7 Moisture Content or Moisture Regain 8 Nonfibrous Materials 9 Mechanical Separation or Dissection 10 Chemical Test Methods: Summary of Methods 11 Specimens and Symbols 12 No. 1 Acetate Mixed With Other Fibers 13 No. 2 Modacrylic Mixed With Cellulosic Fiber or Wool 14 No. 3 Nylon 6 or Nylon 6-6 Mixed With Natural Fibers or Rayon 15 No. 4 Rayon Mixed With Cotton 16 No. 5 Wool or Polyester Mixed With Cellulosic Fibers or Silk 17 No. 6 Polyester or Acrylic Mixed With Wool 18 No. 7 Natural Cellulosic Material and Rayon Mixed With Acrylic, Modacrylic, and Polyester 19 Referenced Documents 2 No. 8 Polyester Mixed With Olefin 20 No. 9 Polyester Mixed With Acetate or Nylon 6,6-6 21 No. 10 Acrylic Fiber or Linear Spandex Mixed With Nylon or Polyester 22 Microspical Analysis Scope 23 Summary of Method 24 Sampling 25 Apparatus 26 Procedure 27 Indexing Term 28 Table Chemical Methods for Analysis of Fiber Mixtures 1 Solubilities of Various Fibers in Solvents Used in Chemical Methods 2 Comparative Scale for Fineness of Various Textile Fibers 3 Fineness Ranges and Fiber Diameters of Various Textile Fibers 4 Specific Gravity of Various Textile Fibers 5
1.4 The analytical procedures described in the test methods are applicable to the fibers listed in 1.2. The test methods are not satisfactory for the separation of mixtures containing fibers that fall within the same generic class but differ somewhat, either physically or chemically, from each other. These test methods are not satisfactory for the determination of bicomponent fibers.  Note 1-For other methods of analysis covering specific determinations, refer to: Test Methods D461, Test Method D584, Methods D885, Test Method D1113, Test Method D1334, and Test Method D2130. Methods for moisture are covered in Methods D885, Test Method D1576, Test Method D2462, Test Method D2495 and Test Methods D2654. For the determination of commercial weight, refer to Test Method D2494.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Sep-1999
ICS
59.080.01 - Textiles in general
Technical Committee
D13 - Textiles
Drafting Committee
D13.51 - Conditioning, Chemical and Thermal Properties
Current Stage
Ref Project

Relations

Replaced By
ASTM D629-08 - Standard Test Methods for Quantitative Analysis of Textiles
Effective Date
01-Aug-2008
Referred By
ASTM D5034-21 - Standard Test Method for Breaking Strength and Elongation of Textile Fabrics (Grab Test)
Effective Date
10-Sep-1999
Referred By
ASTM D1059-17(2022) - Standard Test Method for Yarn Number Based on Short-Length Specimens
Effective Date
10-Sep-1999
Referred By
ASTM D5587-15(2019) - Standard Test Method for Tearing Strength of Fabrics by Trapezoid Procedure
Effective Date
10-Sep-1999
Referred By
ASTM F2368-04(2018) - Standard Specification for Labeling for Wet Mops for Consumer and Institutional Use
Effective Date
10-Sep-1999
Referred By
ASTM D2817-18 - Standard Specification for Maximum Cashmere Coarse-Hair Content in Cashmere
Effective Date
10-Sep-1999
Referred By
ASTM D7268-23 - Standard Performance Specification for Seamless Knit Garments Including Intimates and Swimwear
Effective Date
10-Sep-1999
Referred By
ASTM D1577-07(2018) - Standard Test Methods for Linear Density of Textile Fibers
Effective Date
10-Sep-1999
Referred By
ASTM D2494-13(2020) - Standard Test Method for Commercial Mass of a Shipment of Yarn or Manufactured Staple Fiber or Tow
Effective Date
10-Sep-1999
Referred By
ASTM D1795-13(2021) - Standard Test Method for Intrinsic Viscosity of Cellulose
Effective Date
10-Sep-1999
Referred By
ASTM D2816-18 - Standard Test Method for Cashmere Coarse-Hair Content in Cashmere
Effective Date
10-Sep-1999
Referred By
ASTM D5035-11(2019) - Standard Test Method for Breaking Force and Elongation of Textile Fabrics (Strip Method)
Effective Date
10-Sep-1999
Referred By
ASTM D1424-21 - Standard Test Method for Tearing Strength of Fabrics by Falling-Pendulum (Elmendorf-Type) Apparatus
Effective Date
10-Sep-1999
Referred By
ASTM D6719-22e1 - Standard Guide for Standard Test Methods and Practices for Evaluating Pile Yarn Floor Covering
Effective Date
10-Sep-1999
Referred By
ASTM D2402-07(2018) - Standard Test Method for Water Retention of Textile Fibers (Centrifuge Procedure)
Effective Date
10-Sep-1999

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ASTM D629-99 - Standard Test Methods for Quantitative Analysis of TextilesASTM D629-99 - Standard Test Methods for Quantitative Analysis of Textiles
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ASTM D629-99 - Standard Test Methods for Quantitative Analysis of Textiles
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 629 – 99
Standard Test Methods for
1
Quantitative Analysis of Textiles
This standard is issued under the fixed designation D629; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
INTRODUCTION
Methods D629-59 T, Quantitative Analysis of Textiles, were discontinued in 1969 because the
responsible subcommittee failed to recommend their adoption as a standard after several years of
publication as a tentative. The subcommittee action was based on the members’ knowledge that the
standard did not include several fiber types introduced to the textile trade after the method was
published, and that the techniques required for their identification were lacking in the text, allowing
it to become out of date. The procedures included in the text, however, are believed to be reliable for
the fiber types named and the techniques described are currently being used in the trade and are
referenced by other standards sponsored by Committee D-13 onTextiles. Reinstatement as a standard
using the previously assigned number was requested since the listed procedures were reliable and the
text considered to be the best available, though not all inclusive. Extensive editorial changes were
made in various sections in 1972, and the methods were reinstated as D629-72. Editorial changes
have again been made throughout the text, and statements on precision and bias and suitability for
acceptance testing have been added.
The text of Methods D629-59 T was published by the American Association of Textile Chemists
and Colorists in that society’sTechnical Manual as “Test Method20A-1959” issued in the years 1959
through 1974. The AATCC Method was revised completely in 1975 and since published as “Test
Method20A-1975.”
1. Scope Animal hairs (other than wool)
Silk, cultivated
1.1 These test methods cover procedures for the determina-
Silk, Tussah
tion of the fiber blend composition of mixtures of the fibers
Wool
listed in 1.2. Procedures for quantitative estimation of the
1.2.2 Man-Made Fibers:
amount of moisture and certain nonfibrous materials in textiles
1.2.2.1 Cellulose-Base Fibers:
arealsodescribed,foruseintheanalysisofmixtures,butthese
Acetate (secondary)
are not the primary methods for the determination of moisture
Rayon, viscose or cuprammonium
content for commercial weights.
Triacetate
1.2 These test methods cover procedures for the following
1.2.2.2 Synthetic-Base Fibers:
fiber types:
Acrylic
1.2.1 Natural Fibers:
Aramid
1.2.1.1 Cellulose-Base Fibers:
Modacrylic
Cotton
Nylon 6, Nylon 6-6, others
Hemp
Olefin
Flax
Polyester
Ramie
Spandex
1.2.1.2 Protein-Base Fibers:
1.3 These test methods include the following sections and
tables:
1
These test methods are under the jurisdiction of ASTM Committee D13 on
Section
Textiles and are the direct responsibility of Subcommittee D13.51 on Conditioning
and, Chemical and Thermal Properties.
Referenced Documents 2
Current edition approved Sept. 10, 1999. Published January 2000. Originally
published as D629–41T. Last previous edition D629–88. Withdrawn 1969 and
reinstated 1972 as D629 – 72(1999)
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D629–99
2
D461 Test Methods for Felt
Section
D584 Test Method for Wool Content of Raw Wool—
Terminology 3
2
Laboratory Scale
Summary of Methods 4
D885 Methods of Testing Tire Cords, Tire Cord Fabrics,
Uses and Significance 5
Sampling 7
and Industrial Filament Yarns Made From Man-Made
Purity of Reagents 6
2
Organic Base Fibers
Moisture Content or Moisture Regain 9
D 1113 TestMethodforVegetableMatterandOtherAlkali-
Nonfibrous Materials 8
2
Mechanical Separation or Dissection 10
Insoluble Impurities in Scoured Wool
Chemical Test Methods:
3
D1193 Specification for Reagent Water
Summary of Methods 11
Specimens and Symbols 12 D1334 Test Method for Wool Content of Raw Wool—
2
No. 1 Acetate Mixed With Other Fibers 13
Commercial Scale
No. 2 Modacrylic Mixed With Cellulosic Fiber or Wool 14
2
D1576 TestMethodforMoistureinWoolbyOvenDrying
No. 3 Nylon 6 or Nylon 6-6 Mixed With Natural Fibers or
Rayon 15 D1909 Table of Commercial Moisture Regains for Textile
2
No. 4 Rayon Mixed With Cotton 16
Fibers
No. 5 Wool or Polyester Mixed With Cellulosic Fibers or Silk 17
D2130 Test Method for Diameter of Wool and Other
No. 6 Polyester or Acrylic Mixed With Wool 18
2
No. 7 Natural Cellulosic Material and Rayon Mixed With Animal Fiber by Microprojection
Acrylic, Modacrylic
...

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ASTM D4848-98(2018)(Terminology)
Standard Terminology Related to Force, Deformation and Related Properties of Textiles

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1.1 This terminology standard is a compilation of definitions of technical terms related to force and deformation properties when evaluating a stress-strain curve of a textile. (See Figs. X1.1 and X1.2.) A chart showing the relationship of the basic terms is shown in Table 1. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 For other terms associated with textiles, refer to Terminology D123.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D5253-04(2016)(Terminology)
Standard Terminology Relating to Floor Coverings and Textile Upholstered Furniture

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1.1 This standard is a compilation of all terminology developed by Subcommittee D13.62 on Labeling and related to refurbishing or care of floor coverings and textile upholstered furniture, excluding leather. These items cannot be refurbished by the laundering and dry cleaning methods used for apparel and other domestic textile products.  
1.2 This document defines terms for the care of textile floor coverings and textile upholstered furniture. The exact care instructions and sequence of procedures are to be determined by the manufacturer.  
1.3 The recommended terminology covers common meanings used by both textile technologists and consumers.  
1.4 This terminology is not applicable to unattached fabrics, such as slipcovers, used for covering furniture.  
1.5 When care labels are provided, a standardized terminology in a logical sequence facilitates the maximum disclosure of essential information in small label space and assists understanding of recommended care practices by the consumer.  
1.6 The use of either a permanent or a nonattached care instruction should not preclude the use of the alternative as an additional source of information to the consumer.  
1.7 The term “only” in any label term limits the procedure to the stated instruction.  
1.8 This terminology is unique to the care of textile floor coverings and upholstered furniture. Meanings of the same terms outside the industry can be found in other compilations or dictionaries of general usage.  
1.9 In addition to being a specialized dictionary, Terminology D5253 is also useful for managing the subcommittee's terminology.  
1.10 Terms listed are under the jurisdiction of SC D13.62.  
1.11 For definitions of refurbishing or care terms for apparel, textile, home furnishing, and leather products cleaned by laundering or dry cleaning methods, see Terminology D3136.  
1.12 For definitions of other textile terms, see Terminology D123.

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ASTM
ASTM D629-15(Test Method)
Standard Test Methods for Quantitative Analysis of Textiles

SIGNIFICANCE AND USE
5.1 Qualitative and quantitative fiber identification is actively pursued by committee RA24 (Fiber Identification) of AATCC and presented in AATCC Test Methods 20 and 20A. Since precision and bias development is also part of the AATCC test methods, both AATCC and ASTM D13 have agreed that new development will take place in RA24. However, because there is valuable information still present in the ASTM standards, D13.51 has agreed Test MethodsD276 and D629 will be maintained as active standards by ASTM.  
5.2 Test Methods D629 for the determination of quantitative analysis of textiles may be used for acceptance testing of commercial shipments but caution is advised since information on between-laboratory precision is lacking. Comparative tests as directed in 5.2.1 or in Standard Tables D1909 may be advisable.  
5.2.1 In case of a dispute arising from differences in reported test results using Test Methods D629 for acceptance testing of commercial shipments, the purchaser and the supplier should conduct comparative tests to determine if there is a statistical bias between their laboratories. Competent statistical assistance is recommended for the investigation of bias. As a minimum, the two parties should take a group of test specimens which are as homogeneous as possible and which are from a lot of material of the type in question. The test specimen should then be randomly assigned in equal numbers to each laboratory for testing. The average results from the two laboratories should be compared using Student's t-test and an acceptable probability level chosen by the two parties before the testing began. If a bias is found, either its cause must be found and corrected or the purchaser and supplier must agree to interpret future test results in the light of the known bias.  
5.3 The effects of the various reagents used in the chemical methods on the residual fibers in a blend depend upon the history of the fibers and, unless otherwise stated, are generally too small o...
SCOPE
1.1 These test methods cover procedures for the determination of the fiber blend composition of mixtures of the fibers listed in 1.2. Procedures for quantitative estimation of the amount of moisture and certain nonfibrous materials in textiles are also described, for use in the analysis of mixtures, but these are not the primary methods for the determination of moisture content for commercial weights.  
1.2 These test methods cover procedures for the following fiber types:  
1.2.1 Natural Fibers:  
1.2.1.1 Cellulose-Base Fibers:  
Cotton
Hemp
Flax
Ramie
1.2.1.2 Protein-Base Fibers:  
Animal hairs (other than wool)
Silk, cultivated
Silk, Tussah
Wool  
1.2.2 Man-Made Fibers:  
1.2.2.1 Cellulose-Base Fibers:  
Acetate (secondary)
Rayon, viscose or cuprammonium
Triacetate
1.2.2.2 Synthetic-Base Fibers:  
Acrylic
Aramid
Modacrylic
Nylon 6, Nylon 6-6, others
Olefin
Polyester
Spandex  
1.3 These test methods include the following sections and tables:    
Section  
Referenced Documents  
2  
Terminology  
3  
Summary of Methods  
4  
Uses and Significance  
5  
Sampling  
7  
Purity of Reagents  
6  
Moisture Content or Moisture Regain  
9  
Nonfibrous Materials  
8  
Mechanical Separation or Dissection  
10  
Chemical Test Methods:  
Summary of Methods  
11  
Specimens and Symbols  
12  
No. 1 Acetate Mixed With Other Fibers  
13  
No. 2 Modacrylic Mixed With Cellulosic Fiber or Wool  
14  
No. 3 Nylon 6 or Nylon 6-6 Mixed With Natural Fibers or Rayon  
15  
No. 4 Rayon Mixed With Cotton  
16  
No. 5 Wool or Polyester Mixed With Cellulosic Fibers or Silk  
17  
No. 6 Polyester or Acrylic Mixed With Wool  
18  
No. 7 Natural Cellulosic Material and Rayon Mixed With Acrylic, Modacrylic, and Polyester  
19  
No. 8 Polyester Mixed With Olefin  
20  
No. 9 Polyester Mixe...

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ASTM
ASTM D6419-00(2023)(Test Method)
Standard Test Method for Volatile Content of Sheet-Fed and Coldset Web Offset Printing Inks

SIGNIFICANCE AND USE
4.1 This test method is the procedure of choice for determining volatile content of sheet-fed and coldset web offset inks. This information is useful to the ink manufacturer and user and to environmental interests as part of the determination of the mass of volatile organic compounds emitted from the ink.
Note 3: Since these inks do not contain water or any materials currently classified by US EPA as negligibly photochemically reactive (exempt solvents), volatile organic compound content is the same as volatile content. The volatile organic compounds in these inks are high boiling hydrocarbon oils which are, according to US EPA guidelines, 95 % retained in the printed substrate or oxidized into the ink film. Therefore, the mass of volatile organic compound emitted from the ink would be calculated as only 5 % of the volatile organic compound content of the ink as derived from the results of this test method.
SCOPE
1.1 This test method describes a procedure for determination of the weight percent volatile content of sheet-fed and coldset web offset printing inks. Test specimens are heated at 110 °C ± 1 °C for 60 min.
Note 1: Coldset web offset printing is often (also) referred to as non-heatset web offset printing.  
1.2 This test method is also applicable to sheet-fed and coldset web offset printing ink vehicles.
Note 2: Vehicle is the liquid portion of the printing ink. Any substance that is dissolved in the liquid portion of the ink is a part of the vehicle.  
1.3 This test method is not applicable to ultra-violet (UV) or electron beam cured materials, which must be cured by exposure to UV light or an electron beam as part of the test for volatile content.  
1.4 This test method is based on Test Method D2369, in which the allowable ranges are ±0.1 g for specimen weight and ±5 °C for oven temperature. Interlaboratory studies have shown that specimen weight and oven temperature must both be more tightly controlled in order to improve the precision of test results for sheet-fed and coldset web-offset inks. Such inks typically contain a wide range of high-boiling hydrocarbons and often have a volatile content below 25 %.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement see 7.5.1  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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