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ASTM D2893-04(2009)

(Test Method)

Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils

Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils

SIGNIFICANCE AND USE
These test methods have been widely used to measure the oxidation stability of extreme pressure lubricating fluids, gear oils, and mineral oils.
SCOPE
1.1 These test methods (A and B) cover the determination of the oxidation characteristics of extreme-pressure fluid lubricants, gear oils, or mineral oils.
Note 1—The changes in the lubricant resulting from these test methods are not always necessarily associated with oxidation of the lubricant. Some changes may be due to thermal degradation.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Sep-2009
ICS
75.100 - Lubricants, industrial oils and related products
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.09.0D - Oxidation of Lubricants
Current Stage
Ref Project

Relations

Replaces
ASTM D2893-04 - Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils
Effective Date
01-Oct-2009
Replaced By
ASTM D2893-04(2014)e1 - Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils
Effective Date
01-Jun-2014
Referred By
ASTM D5763-22a - Standard Test Method for Oxidation and Thermal Stability Characteristics of Gear Oils Using Universal Glassware
Effective Date
01-Oct-2009
Referred By
ASTM D8324-21 - Standard Guide for Selection of Environmentally Acceptable Lubricants for the U.S. Environmental Protection Agency (EPA) Vessel General Permit
Effective Date
01-Oct-2009

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ASTM D2893-04(2009) - Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication OilsASTM D2893-04(2009) - Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils
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ASTM D2893-04(2009) - Standard Test Method for Oxidation Characteristics of Extreme-Pressure Lubrication Oils
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D2893 − 04(Reapproved 2009)
Standard Test Methods for
Oxidation Characteristics of Extreme-Pressure Lubrication
1
Oils
This standard is issued under the fixed designation D2893; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3.2 The oil is then tested for precipitation number and
increase in kinematic viscosity.
1.1 Thesetestmethods(AandB)coverthedeterminationof
the oxidation characteristics of extreme-pressure fluid
4. Significance and Use
lubricants, gear oils, or mineral oils.
4.1 These test methods have been widely used to measure
NOTE1—Thechangesinthelubricantresultingfromthesetestmethods the oxidation stability of extreme pressure lubricating fluids,
are not always necessarily associated with oxidation of the lubricant.
gear oils, and mineral oils.
Some changes may be due to thermal degradation.
5. Apparatus
1.2 The values stated in SI units are to be regarded as
5.1 Heating Bath or Block, thermostatically controlled,
standard. No other units of measurement are included in this
capable of maintaining the oil sample in the test tube at a
standard.
temperature of 95 6 0.2°C (Test Method A), or 121 6 1.0°C
1.3 This standard does not purport to address all of the
(Test Method B) and large enough to hold the desired number
safety concerns, if any, associated with its use. It is the
of oxidation cells immersed in the heating bath or block to a
responsibility of the user of this standard to establish appro-
depth of approximately 350 mm. The liquid heating bath shall
priate safety and health practices and determine the applica-
be fitted with a suitable stirring device to provide a uniform
bility of regulatory limitations prior to use.
temperature throughout the bath.
5.2 Test Tubes, of borosilicate glass, 41 6 0.5 mm inside
2. Referenced Documents
diameter and 600 mm in length are required, each fitted with a
2
2.1 ASTM Standards:
slotted cork (Note 2) stopper into which shall be inserted a
D91 Test Method for Precipitation Number of Lubricating
glass air delivery tube of 4 to 5 mm of inside diameter. The
Oils
length of the air delivery tube shall be such that one end
D445 Test Method for Kinematic Viscosity of Transparent
reaches to within 6 mm of the bottom of the tube and the other
and Opaque Liquids (and Calculation of Dynamic Viscos-
end projects 60 to 80 mm from the cork stopper.
ity)
NOTE 2—New corks should be used for each run.
D943 Test Method for Oxidation Characteristics of Inhibited
Mineral Oils
5.3 Flowmeter, one to each test tube, capable of measuring
E1 Specification for ASTM Liquid-in-Glass Thermometers an air flow of 10 L/h with an accuracy of 60.5 L/h.
5.4 Thermometer—ASTM Solvent Distillation Thermom-
3. Summary of Test Method
eter having a range from 76 to 126°C and conforming to the
3.1 The oil sample is subjected to a temperature of 95°C requirement for Thermometer 40C as prescribed in Specifica-
(Test Method A) or 121°C (Test Method B) in the presence of tion E1. Alternatively, calibrated thermocouples may be used.
dry air for 312 h.
5.5 Air Supply—Oil-free, dried air at constant pressure shall
be supplied to each flowmeter.
5.6 AirDryer—Before being supplied to the flowmeters, the
1
These test methods are under the jurisdiction of ASTM Committee D02 on
air shall be passed through a drying tower packed with
Petroleum Products and Lubricantsand is the direct responsibility of Subcommittee
indicating grade of anhydrous calcium sulfate or equivalent.
D02.09.0D on Oxidation of Lubricants.
The quantity of dessicant should be sufficient to last for the
Current edition approved Oct. 1, 2009. Published November 2009. Originally
approved in 1970. Last previous edition approved in 2004 as D2893–04. DOI:
entire test.
10.1520/D2893-04R09.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
6. Preparation of Apparatus
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
6.1 Cleaning of Oxidation Cells—Clean glassware with a
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. suitable cleaning solution. (Warning—Causes severe burns.A
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D2893 − 04 (2009)
recognized carcinogen. Strong oxidizer, contact with other
material may cause fire. Hygroscropic.)
NOTE 3—While other suitable cleaning solutions are now available, the
round robin used glassware cleaned with chromic acid. Other cleaning
solutions such as NoChromix and M
...

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5.1 The low-temperature, low-shear-rate viscosity of automatic transmission fluids, gear oils, torque and tractor fluids, and industrial and automotive hydraulic oils (see Appendix X4) are of considerable importance to the proper operation of many mechanical devices. Measurement of the viscometric properties of these oils and fluids at low temperatures is often used to specify their acceptance for service. This test method is used in a number of specifications.  
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1.1 This test method covers the determination of glycol based antifreeze for in-service engine oil by derivative headspace/gas chromatography.  
1.2 Sample is derivatized in-situ directly in a headspace sampling vial prior to vapor phase extraction and injection into a gas chromatograph.  
1.3 The chemistry of the derivatization is unique to the detection of the molecules of ethylene glycol and 1,2-propylene glycol. 1,3-propylene glycol could also be detected but is not used in any known anti-freeze at this time. Other coolant analyses are beyond the scope of this test method.  
1.4 The derivatization process does not affect glycol breakdown products such as glycolate and formate and hence the presence of these compounds in the oil will not be quantified.  
1.5 The test method concentration range is from 50 µg/g to 1000 µg/g. Lower levels are possible by method modifications. Higher levels are possible through sample dilution.  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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  • Standard
    8 pages
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ASTM
ASTM D7918-23(Test Method)
Standard Test Method for Measurement of Flow Properties and Evaluation of Wear, Contaminants, and Oxidative Properties of Lubricating Grease by Die Extrusion Method and Preparation

SIGNIFICANCE AND USE
5.1 Trending the wear, contamination, consistency, and oxidative properties of a lubricating grease is a crucial part of condition-monitoring programs. Changes in these properties or deviations from the new grease can be indicative of problems within the lubricated component, such as the mixing of incompatible thickener types, excessive wear or contaminant levels, or significant depletion of antioxidant levels. These test methods also makes it possible to develop trends that can be used to predict failures before they occur and allow for corrective action to be taken.
SCOPE
1.1 This test method covers the determination and evaluation of flow properties, wear levels, contaminants, and oxidative condition of new and in-service lubricating grease.  
1.2 This test method provides guidance on evaluating in-service grease samples, NLGI grades 00 to 3, for wear, consistency, contamination, and oxidation.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3.1 Exception—The exception to this will be where units of references were developed by the developers of the test equipment and necessary to report the results of the test.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
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  • Standard
    9 pages
    English language
    sale 15% off