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ASTM D1488-00(2018)

(Test Method)

Standard Test Method for Amylaceous Matter in Adhesives

Standard Test Method for Amylaceous Matter in Adhesives

SIGNIFICANCE AND USE
5.1 This test method is used to determine if a melamine resin, a phenol, or a resorcinol adhesive contains any starch-like filler, the presence of which could affect water resistance or strength, or both.
SCOPE
1.1 This test method covers the determination of the presence or absence of amylaceous (starch-like) material in phenol-, resorcinol-, and melamine-resin adhesives.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jul-2018
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.30 - Wood Adhesives
Current Stage
Ref Project

Relations

Replaces
ASTM D1488-00(2013) - Standard Test Method for Amylaceous Matter in Adhesives
Effective Date
01-Aug-2018
Refers
ASTM D907-12a - Standard Terminology of Adhesives
Effective Date
01-Jul-2012
Refers
ASTM D907-12 - Standard Terminology of Adhesives
Effective Date
01-May-2012
Refers
ASTM D907-11a - Standard Terminology of Adhesives
Effective Date
01-Dec-2011
Refers
ASTM D907-11 - Standard Terminology of Adhesives
Effective Date
01-Jan-2011
Refers
ASTM D907-08b - Standard Terminology of Adhesives
Effective Date
01-Oct-2008
Refers
ASTM D907-08a - Standard Terminology of Adhesives
Effective Date
15-Aug-2008
Refers
ASTM D907-08 - Standard Terminology of Adhesives
Effective Date
01-Mar-2008
Refers
ASTM D907-06 - Standard Terminology of Adhesives
Effective Date
01-Dec-2006
Refers
ASTM D907-05e1 - Standard Terminology of Adhesives
Effective Date
01-Apr-2005
Refers
ASTM D907-05 - Standard Terminology of Adhesives
Effective Date
01-Apr-2005
Refers
ASTM D907-04a - Standard Terminology of Adhesives
Effective Date
01-Dec-2004
Refers
ASTM D907-04 - Standard Terminology of Adhesives
Effective Date
01-Apr-2004
Refers
ASTM D907-03 - Standard Terminology of Adhesives
Effective Date
10-May-2003
Refers
ASTM D907-00 - Standard Terminology of Adhesives
Effective Date
10-Oct-2000

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ASTM D1488-00(2018) - Standard Test Method for Amylaceous Matter in AdhesivesASTM D1488-00(2018) - Standard Test Method for Amylaceous Matter in Adhesives
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ASTM D1488-00(2018) - Standard Test Method for Amylaceous Matter in Adhesives
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1488 − 00 (Reapproved 2018)
Standard Test Method for
Amylaceous Matter in Adhesives
This standard is issued under the fixed designation D1488; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 5. Significance and Use
1.1 This test method covers the determination of the pres- 5.1 This test method is used to determine if a melamine
ence or absence of amylaceous (starch-like) material in resin, a phenol, or a resorcinol adhesive contains any starch-
phenol-, resorcinol-, and melamine-resin adhesives. like filler, the presence of which could affect water resistance
or strength, or both.
1.2 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
6. Reagents
only.
6.1 Iodine Test Solution—Add 5 g (0.18 oz) of iodine and 5
1.3 This standard does not purport to address all of the
g of potassium iodide to 100 mL (3 oz) of distilled water.
safety concerns, if any, associated with its use. It is the
6.2 Acetic Acid—Ethyl Alcohol Solution—Add 20 parts of
responsibility of the user of this standard to establish appro-
glacial acetic acid and 20 parts of 95 % ethyl alcohol to 60
priate safety, health, and environmental practices and deter-
parts of distilled water by volume.
mine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accor-
7. Sampling
dance with internationally recognized principles on standard-
7.1 Except in special cases, take a composite of the sample
ization established in the Decision on Principles for the
of the adhesive when possible, from three or more separate
Development of International Standards, Guides and Recom-
containers, chosen at random. Also, take samples from con-
mendations issued by the World Trade Organization Technical
tainers that appear to be nonrepresentative, and test such
Barriers to Trade (TBT) Committee.
samples separately. Before a sample is taken, thoroughly mix
the contents of the container if there is a tendency for the
2. Referenced Documents
materials to separate. Place the samples immediately in airtight
2.1 ASTM Standards:
containers and transport to the testing laboratory in these
D907 Terminology of Adhesives
containers.Take precautions to reduce evaporation or drying to
a minimum.
3. Terminology
3.1 Definitions—Many terms in this test method are defined
8. Procedure
in Terminology D907.
8.1 Phenol and Resorcinol Adhesives—Weigh 0.5 g (0.018
oz) of thoroughly mixed adhesive into a small-diameter test
4. Summary of Test Method
tube. Add 5 mL (0.15 oz) of 95 % ethyl alcohol. Shake
4.1 A reagent solution is added to the adhesive in question
thoroughly, allow the insoluble matter to settle, and decant the
which causes any starch-like material to become insoluble.The
supernatant liquid. Re
...

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ABSTRACT
This specification covers polyvinyl acetate or polyvinyl acetate copolymer resin emulsion adhesives suitable for use on wood, wood-based substrates, or plastic laminates. This does not cover the group of polyvinyl-based adhesives suitable for bonding flexible films. Adhesives are classified on the basis of water resistance at three performance levels, namely wet-use (Type 1), intermediate use (Type 2), and dry-use (Type 3). Adhesives shall conform to test requirements as performed under the following exposure conditions and treatments: dry shear at specified temperatures; two-cycle boil; 48-hour soak; humidity exposure; freeze-thaw stability; and storage life. Materials shall also adhere to physical properties such as density, nonvolatile matter, and pH.
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1.1 This specification covers polyvinyl acetate or polyvinyl acetate copolymer resin emulsion adhesives suitable for use on wood, wood-based substrates, or plastic laminates. It does not cover the group of polyvinyl-based adhesives which are suitable for bonding flexible films.  
1.2 The adhesives are classified at three performance levels in accordance with water-resistance as shown in Table 1 and Table 2. See Section 5 for a description of the expected exposure conditions for each class of adhesive. See Table X1.1 for a classification of typical end products that are manufactured using adhesives at the three performance levels covered by this specification.    
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Section  
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Standard Test Method for Nonvolatile Content of Liquid Phenol, Resorcinol, and Melamine Adhesives

ABSTRACT
This test method covers the determination of nonvolatile content or total solids of liquid phenol, resorcinol, and melamine adhesives with or without hardener added and containing high-boiling and low-boiling volatile organic solvents or water, or both. The equipments to be used in the test shall include a petri dish, circulating-air oven, desiccator, and analytical balance. In determining the nonvolatile content of the liquid adhesives without hardener, the procedure shall include oven-drying, cooling in a desiccator, and weighing of adhesive and quartz sand . The percent nonvolatile content shall be calculated based on the amount remaining. On the other hand, the procedure for the liquid adhesives with hardener shall include oven-drying, cooling in a desiccator, and weighing of mixed adhesives. Also, the percent nonvolatile content shall be calculated based on the amount remaining.
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1.1 This test method covers the determination of nonvolatile content or total solids of liquid phenol, resorcinol, and melamine adhesives with or without hardener (Note 1) added and containing high-boiling and low-boiling volatile organic solvents or water, or both.  
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4.1 These test methods are designed to be used to determine the susceptibility of the adhesive film to biodegradation and whether the adhesive will carry into the bond line sufficient anti-fungal properties to prevent growth of fungi frequently present on the gluing equipment, on adherends, or in the adhesive as applied.  
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Note 2: The method given here using the MSA is based on Practice G21, adapted to be used with adhesives. Requirements for the use of the MSA are described in 10.2, and a mixed species of fungi is prescribed in 8.2 for the inoculum.  
4.3 The results obtained when using the procedures given in this method apply only to the species used for the testing. The test species listed in Section 8 are frequently used by laboratories to test for antifungal properties, but they are not the only ones which could be used. Selection of the fungal species to test against requires informed judgment by the testing laboratory or by the party requesting the tests. These methods are especially useful when species that have been isolated from contaminated adhesives are used as the test species (see Section 8) to aid in the selection of more effective fungicides.  
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SCOPE
1.1 These test methods test the ability of adhesive films to inhibit or support the growth of selected fungal species growing on agar plates by providing means of testing the films on two agar substrates, one which promotes microbial growth, and one which does not.  
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4.1 Creep data that are obtained over a relatively short period of time in this test method can provide a measure of an adhesive bond's ability to withstand static loading in shear over a relatively long period of time. Creep measurements are made over a range of expected service conditions, including level of stress, temperature, relative humidity, and duration of load. Creep rate, creep strain, and creep modulus are calculated at the various service conditions.  
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SCOPE
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4.1 Tension tests provide reasonably accurate information with regard to the tensile strength of adhesives. Tensile strength data may be suitable for specification acceptance, service evaluation, manufacturing control, research, and development. Tension tests are not considered significant for applications differing from the test in rate, direction, and type of loading.
SCOPE
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ASTM D3930-08(2023)(Specification)
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ABSTRACT
This specification provides the means to measure and evaluate the performance of adhesives for structural or semistructural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having woodbased surfaces at the bondline. The adhesives can be classified according to resistance to deformation: Group A or structural, and Group B or semistructural. Also, the adhesives may be designated into three types, according to their recommended use based on their resistance to water and water vapor: Type 1 for interior and exterior use, Type 2 for weather-protected interior use, and Type 3 for interior use only. Different tests shall be performed in order to determine the following properties of adhesives: shear strength, gap-filling ability, total deformation resistance, moisture and temperature limitation during fabrication, high-temperature resistance, low-temperature resistance, moisture resistance, aging, oxidation resistance, and mold resistance.
SCOPE
1.1 This specification provides the means to measure and evaluate the performance of adhesives for structural or semi-structural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having wood-based surfaces at the bondline. This specification does not cover other adhesives used in manufactured homes such as adhesives for carpet, floor tile, ceramic fixtures, plastic laminates, trim and millwork, and similar nonstructural applications.  
1.1.1 The performance of the adhesives is measured in the following tests:    
Number  
Test  
Section  
1  
Low Temperature  
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2  
Dry Lumber  
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3  
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High Temperature  
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Type 3 Qualification  
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Type 2 Qualification  
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Type 1 Qualification  
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1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
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ASTM D907-15(2023)(Terminology)
Standard Terminology of Adhesives

SCOPE
1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
1.2.1.1 In Table X1.1, the year of publication in Volume 15.06 is shown in parentheses following the term.  
1.2.2 In the text of the standard, the year of publication is shown following each definition. Also, the following codes are included after the year of publication to describe the type change that was made: (A) Addition, (R) Revision, or (E) Edited.  
1.2.3 Deletions are shown in Appendix X1, suitably footnoted. The deleted terms do not appear in the text of the standard.  
1.2.4 Any special circumstances not covered by 1.2.2 and 1.2.3 are documented in Table X1.1, suitably footnoted.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7966/D7966M-16(2023)(Test Method)
Standard Test Method for Resistance to Creep of Adhesives in Static Shear by Compression Loading (Wood-to-Wood)

SIGNIFICANCE AND USE
5.1 This test method evaluates the performance of the adhesive in laminated wood as measured by resistance to creep under static load.  
5.2 Test results from the evaluation of adhesive creep resistance, under designated environmental conditions of the test, provide a measure of the adhesive’s ability to withstand constant loading over a relatively long period of time.  
5.3 Creep measured with this test method is normally used in conjunction with specifications such as, but not limited to Specification D2559 and CSA O112.9 to confirm suitability of an adhesive to resist creep under designed loads when subjected to specific levels of stress, load duration and environmental conditions.
SCOPE
1.1 This test method covers the determination of creep properties of structural adhesives in wood-to-wood bonds when a standardized specimen is subjected to shearing stresses at various levels of static load, constant temperature, and relative humidity. Apparatus and procedures are provided for shear deformation (creep) of adhesive bonds under static load. This test method is used under the indicated conditions to evaluate resistance to creep properties of a structural wood adhesive.  
1.2 The test method is used to evaluate creep performance of adhesives suitable for the bonding of wood, including treated wood, into structural wood products for general construction, marine use, or for other uses where a high-strength general construction, creep-resistant, durable adhesive bond is required. Individual block shear specimens are prepared from adhesively bonded laminations, subjected to a constant load under various combinations of temperature and relative humidity, and the amount of creep measured.  
1.3 Creep of structural wood adhesives as measured by this test method may not be comparative to other ASTM methods and is limited to the conditions of the test and procedures contained herein.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4800-94(2023)(Guide)
Standard Guide for Classifying and Specifying Adhesives

SIGNIFICANCE AND USE
4.1 The purpose of this classification system is to provide a method of identifying adhesives in order to give industry a system that can be used universally for materials. It further provides a means for specifying these materials by the use of the standards that are developed using this guide.  
4.2 This classification system was developed to permit the addition of future adhesives.
SCOPE
1.1 This guide provides a classification system for tabulating the properties of adhesives suitable for holding parts or assemblies together. The use of this guide also provides information necessary for the development of standard specifications for adhesives.  
Note 1: This classification system may serve many of the needs of industries using adhesives. This guide is subject to revision as the need requires; therefore, the latest revision should always be used.  
1.2 Limitations—This classification system is intended to be a means of identifying adhesives. It is not intended for the selection of materials. Material selection should be made by those having expertise in the adhesives field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the attachment process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that adhesives can be arranged into broad generic families using basic properties to arrange the materials into groups, classes, and grades.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular material, the latter shall take precedence.  
1.5 The values stated in SI units, as detailed in IEEE/ASTM SI 10, are to be regarded as the standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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