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ASTM D5953M-23

(Test Method)

Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection

Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection

SIGNIFICANCE AND USE
5.1 Many regulators, industrial processes, and other stakeholders require determination of NMOC in atmospheres.  
5.2 Accurate measurements of ambient NMOC concentrations are critical in devising air pollution control strategies and in assessing control effectiveness because NMOCs are primary precursors of atmospheric ozone and other oxidants (7, 8).  
5.2.1 The NMOC concentrations typically found at urban sites may range up to 1 ppm C to 3 ppm C or higher. In order to determine transport of precursors into an area monitoring site, measurement of NMOC upwind of the site may be necessary. Rural NMOC concentrations originating from areas free from NMOC sources are likely to be less than a few tenths of 1 ppm C.  
5.3 Conventional test methods based upon gas chromatography and qualitative and quantitative species evaluation are relatively time consuming, sometimes difficult and expensive in staff time and resources, and are not needed when only a measurement of NMOC is desired. The test method described requires only a simple, cryogenic pre-concentration procedure followed by direct detection with an FID. This test method provides a sensitive and accurate measurement of ambient total NMOC concentrations where speciated data are not required. Typical uses of this standard test method are as follows.  
5.4 An application of the test method is the monitoring of the cleanliness of canisters.  
5.5 Another use of the test method is the screening of canister samples prior to analysis.  
5.6 Collection of ambient air samples in pressurized canisters provides the following advantages:  
5.6.1 Convenient collection of integrated ambient samples over a specific time period,  
5.6.2 Capability of remote sampling with subsequent central laboratory analysis,  
5.6.3 Ability to ship and store samples, if necessary,  
5.6.4 Unattended sample collection,  
5.6.5 Analysis of samples from multiple sites with one analytical system,  
5.6.6 Collection of replicate samples for ...
SCOPE
1.1 This test method2 presents a procedure for sampling and determination of non-methane organic compounds (NMOC) in ambient, indoor, or workplace atmospheres.  
1.2 This test method describes the collection of integrated whole air samples in silanized or other passivated stainless steel canisters, and their subsequent laboratory analysis.  
1.2.1 This test method describes a procedure for sampling in canisters at final pressures above atmospheric pressure (pressurized sampling).  
1.3 This test method employs a cryogenic trapping procedure for concentration of the NMOC prior to analysis.  
1.4 This test method describes the determination of the NMOC by the flame ionization detection (FID), without the use of gas chromatographic columns and other procedures necessary for species separation.  
1.5 The range of this test method is from 20 ppb C to 10 000 ppb C (1, 2).3  
1.6 This test method has a larger uncertainty for some halogenated or oxygenated hydrocarbons than for simple hydrocarbons or aromatic compounds. This is especially true if there are high concentrations of chlorocarbons or chlorofluorocarbons present.  
1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.  
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.9 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Techn...

General Information

Status
Published
Publication Date
28-Feb-2023
ICS
13.040.01 - Air quality in general
71.040.50 - Physicochemical methods of analysis
Technical Committee
D22 - Air Quality
Drafting Committee
D22.03 - Ambient Atmospheres and Source Emissions
Current Stage
Ref Project

Relations

Refers
ASTM D1356-20a - Standard Terminology Relating to Sampling and Analysis of Atmospheres
Effective Date
01-Sep-2020
Refers
ASTM D1356-20 - Standard Terminology Relating to Sampling and Analysis of Atmospheres
Effective Date
15-Mar-2020

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ASTM D5953M-23 - Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization DetectionASTM D5953M-23 - Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection
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ASTM D5953M-23 - Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection
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REDLINE ASTM D5953M-23 - Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization DetectionREDLINE ASTM D5953M-23 - Standard Test Method for Determination of Non-methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic Preconcentration and Direct Flame Ionization Detection
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5953M − 23
Standard Test Method for
Determination of Non-methane Organic Compounds (NMOC)
in Ambient Air Using Cryogenic Preconcentration and Direct
1
Flame Ionization Detection
This standard is issued under the fixed designation D5953M; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope conversions to inch-pound units that are provided for informa-
tion only and are not considered standard.
2
1.1 This test method presents a procedure for sampling and
1.8 This standard does not purport to address all of the
determination of non-methane organic compounds (NMOC) in
safety concerns, if any, associated with its use. It is the
ambient, indoor, or workplace atmospheres.
responsibility of the user of this standard to establish appro-
1.2 This test method describes the collection of integrated
priate safety, health, and environmental practices and deter-
whole air samples in silanized or other passivated stainless
mine the applicability of regulatory limitations prior to use.
steel canisters, and their subsequent laboratory analysis.
1.9 This international standard was developed in accor-
1.2.1 This test method describes a procedure for sampling in
dance with internationally recognized principles on standard-
canisters at final pressures above atmospheric pressure (pres-
ization established in the Decision on Principles for the
surized sampling).
Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
1.3 This test method employs a cryogenic trapping proce-
dure for concentration of the NMOC prior to analysis. Barriers to Trade (TBT) Committee.
1.4 This test method describes the determination of the
2. Referenced Documents
NMOC by the flame ionization detection (FID), without the
4
2.1 ASTM Standards:
use of gas chromatographic columns and other procedures
D1193 Specification for Reagent Water
necessary for species separation.
D1356 Terminology Relating to Sampling and Analysis of
1.5 The range of this test method is from 20 ppb C to
Atmospheres
3
10 000 ppb C (1, 2).
D1357 Practice for Planning the Sampling of the Ambient
Atmosphere
1.6 This test method has a larger uncertainty for some
halogenated or oxygenated hydrocarbons than for simple D5466 Test Method for Determination of Volatile Organic
Compounds in Atmospheres (Canister Sampling, Mass
hydrocarbons or aromatic compounds. This is especially true if
there are high concentrations of chlorocarbons or chlorofluo- Spectrometry Analysis Methodology)
rocarbons present.
2.2 Other References:
EPA Method TO-12 Determination of Non-Methane Organic
1.7 The values stated in SI units are to be regarded as
Compounds (NMOC) in Ambient Air Using Cryogenic
standard. The values given in parentheses are mathematical
Pre-Concentration and Direct Flame Ionization Detection
5
(PDFID)
1
This test method is under the jurisdiction of ASTM Committee D22 on Air
3. Terminology
Quality and is the direct responsibility of Subcommittee D22.03 on Ambient
Atmospheres and Source Emissions. 3.1 Definitions—For definitions of terms used in this test
Current edition approved March 1, 2023. Published March 2023. Originally
method, refer to Terminology D1356.
approved in 1996. Last previous edition approved in 2016 as D5953M – 16. DOI:
10.1520/D5953M-23.
2
This test method is based on EPA Compendium Method TO-12: “Determination
4
of Non-Methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Pre-Concentration and Direct Flame Ionization Detection (PDFID),” Compendium contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
of Methods for the Determination of Toxic Organic Compounds in Ambient Air, EPA Standards volume information, refer to the standard’s Document Summary page on
600 4-89-017, U.S. Environmental Protection Agency, Research Triangle Park, NC, the ASTM website.
5
March 1990. Available from United States Environmental Protection Agency (EPA), William
3
The boldface numbers in parentheses refer to the list of references at the end of Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
this standard. http://www.epa.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5953M − 23
3.2 Definitions of Terms
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5953M − 16 D5953M − 23
Standard Test Method for
Determination of Non-methane Organic Compounds (NMOC)
in Ambient Air Using Cryogenic Preconcentration and Direct
1
Flame Ionization Detection
This standard is issued under the fixed designation D5953M; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
2
1.1 This test method presents a procedure for sampling and determination of non-methane organic compounds (NMOC) in
ambient, indoor, or workplace atmospheres.
1.2 This test method describes the collection of integrated whole air samples in silanized or other passivated stainless steel
canisters, and their subsequent laboratory analysis.
1.2.1 This test method describes a procedure for sampling in canisters at final pressures above atmospheric pressure (pressurized
sampling).
1.3 This test method employs a cryogenic trapping procedure for concentration of the NMOC prior to analysis.
1.4 This test method describes the determination of the NMOC by the flame ionization detection (FID), without the use of gas
chromatographic columns and other procedures necessary for species separation.
1.5 The range of this test method is from 20 to 10 00020 ppb C to 10 000 ppb
3
ppb C (1, 2).
1.6 This test method has a larger uncertainty for some halogenated or oxygenated hydrocarbons than for simple hydrocarbons or
aromatic compounds. This is especially true if there are high concentrations of chlorocarbons or chlorofluorocarbons present.
1.7 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to
inch-pound units that are provided for information only and are not considered standard.
1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and healthsafety, health, and environmental practices and determine
the applicability of regulatory limitations prior to use.
1
This test method is under the jurisdiction of ASTM Committee D22 on Air Quality and is the direct responsibility of Subcommittee D22.03 on Ambient Atmospheres
and Source Emissions.
Current edition approved Oct. 1, 2016March 1, 2023. Published October 2016March 2023. Originally approved in 1996. Last previous edition approved in 20092016 as
D5953M – 96 (2009).D5953M – 16. DOI: 10.1520/D5953M-16.10.1520/D5953M-23.
2
This test method is based on EPA Compendium Method TO-12: “Determination of Non-Methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic
Pre-Concentration and Direct Flame Ionization Detection (PDFID),” Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air, EPA 600
4-89-017, U.S. Environmental Protection Agency, Research Triangle Park, NC, March 1990.
3
The boldface numbers in parentheses refer to the list of references at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5953M − 23
1.9 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
4
2.1 ASTM Standards:
D1193 Specification for Reagent Water
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D1357 Practice for Planning the Sampling of the Ambient Atmosphere
D5466 Test Method for Determination of Volatile Organic Compounds in Atmospheres (Canister Sampling, Mass Spectrometry
Analysis Methodology)
2.2 Other References:
EPA Method TO-12 Determination of Non-Methane Organic Compounds (NMOC) in Ambient Air Using Cryogenic
5
Pre-Concentration and Direct Flame Ionization Detection (PDFID)
3. Terminology
3.1 Definitions—For definitions of terms used in this test method, refer to Terminology D1356.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 cryogen—a refrigerant used to obtain very low temperatures in analytical system cryogenic traps.
3.2.1.1 Discussion—
Liquid argon (bp –185.7°C(bp –185.7 °C at standard press
...

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1.1 This specification2 covers a group of general requirements that, unless otherwise specified in the purchase order or in an individual specification, shall apply to rolled steel plate, sheet, and strip, under each of the following specifications issued by ASTM: Specifications A240/A240M, A263, A264, A265, A666, A693, A793, and A895.  
1.2 In the case of conflict between a requirement of a product specification and a requirement of this specification, the product specification shall prevail. In the case of conflict between a requirement of the product specification or a requirement of this specification and a more stringent requirement of the purchase order, the purchase order shall prevail. The purchase order requirements shall not take precedence if they, in any way, violate the requirements of the product specification or this specification; for example, by waiving a test requirement or by making a test requirement less stringent.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The SI units are shown in brackets, except that when A480M is specified, Annex A3 shall apply for the dimensional tolerances and not the bracketed SI values in Annex A2. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This specification and the applicable material specifications are expressed in both inch-pound and SI units. However, unless the order specifies the applicable “M” specification designation [SI units], the material shall be furnished in inch-pound units.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E2552-23(Guide)
Standard Guide for Assessing the Environmental and Human Health Impacts of New Compounds for Military Use

SIGNIFICANCE AND USE
5.1 The purpose of this guide is to provide a logical, tiered approach in the development of environmental health criteria coincident with level and effort in the research, development, testing, and evaluation of new materials for military use. Various levels of uncertainty are associated with data collected from previous stages. Following the recommendation in the guide should reduce the relative uncertainty of the data collected at each developmental stage. At each stage, a general weight of evidence qualifier shall accompany each exposure/effect relationship. They may be simple (for example, low, medium, or high confidence) or sophisticated using a numerical value for each predictor as a multiplier to ascertain relative confidence in each step of risk characterization. The specific method used will depend on the stage of development, quantity and availability of data, variation in the measurement, and general knowledge of the dataset. Since specific formulations, conditions, and use scenarios may not be known until the later stages, exposure estimates can be determined when practical (for example, Engineering and Manufacturing Development; see 6.6). Exposure data can then be used with other toxicological data collected from previous stages in a quantitative risk assessment to determine the relative degree of hazard.  
5.2 Data developed from the use of this guide are designed to be consistent with criteria required in weapons and weapons system development (for example, programmatic environment, safety and occupational health evaluations, environmental assessments/environmental impact statements, toxicity clearances, and technical data sheets).  
5.3 Information shall be evaluated in a flexible manner consistent with the needs of the authorizing program. This requires proper characterization of the current problem. For example, compounds may be ranked relative to the environmental criteria of the prospective alternatives, the replacement compound, and within bo...
SCOPE
1.1 This guide is intended to determine the relative environmental influence of new substances, consistent with the research and development (R&D) level of effort and is intended to be applied in a logical, tiered manner that parallels both the available funding and the stage of research, development, testing, and evaluation. Specifically, conservative assumptions, relationships, and models are recommended early in the research stage, and as the technology is matured, empirical data will be developed and used. Munition constituents are included and may include propellants, oxidizers, explosives, binders, stabilizers, metals, dyes, and other compounds used in the formulation to produce a desired effect. Munition systems range from projectiles, grenades, rockets/missiles, training simulators, to smokes and obscurants. Given the complexity of issues involved in the assessment of environmental fate and effects and the diversity of the systems used, this guide is broad in scope and not intended to address every factor that may be important in an environmental context. Rather, it is intended to reduce uncertainty at minimal cost by considering the most important factors related to human health and environmental impacts of energetic materials. This guide provides an outline for collecting data useful in a relative ranking procedure to provide the systems scientist with a sound basis for prospectively determining a selection of candidates based on environmental and human health criteria. The general principles in this guide are applicable to substances other than energetics if intended to be used in a similar manner with similar exposure profiles.  
1.2 The scope of this guide includes:  
1.2.1 Energetic and other new/novel materials and compositions in all stages of research, development, test and evaluation.  
1.2.2 Environmental assessment, including:
1.2.2.1 Human and ecological effects of the unexploded energetics and ...

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ASTM
ASTM D8042-18(2023)(Test Method)
Test Method for Shrinkage Temperature of Wet Blue and Wet White

SIGNIFICANCE AND USE
5.1 This test method is designed to determine the temperature at which the Wet Blue or Wet White specimen experiences shrinkage. In this test method, shrinkage occurs as a result of hydrothermal denaturation of the collagen protein molecules which make up the fiber structure of the Wet Blue or Wet White. The shrinkage temperature of Wet Blue or Wet White is influenced by many different factors, most of which appear to affect the number and nature of crosslinking interactions between adjacent polypeptide chains of the collagen protein molecules. The value of the shrinkage temperature of Wet Blue or Wet White is commonly used as an indicator of the type of tannage or the degree of tannage, or both, of that particular Wet Blue or Wet White (especially for the more hydrothermally stable tannages such as chrome tannage).
SCOPE
1.1 This test method covers the determination of the shrinkage temperature of all types of Wet Blue and Wet White. The heating medium is water when the shrinkage temperature is at or below 98 °C. The heating medium is a glycerine-water solution when the shrinkage temperature is above 98 °C.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8530/D8530M-23(Guide)
Standard Guide for the Selection and Use of Waterstops

SIGNIFICANCE AND USE
4.1 This guide is intended to be used in the selection and installation of waterstops in cast-in-place concrete construction. This guide is intended to assist the building owner, owner’s representative, architect, engineer, contractor, and/or authorized inspector during the specification and installation of waterstops.  
4.2 This guide is applicable to cast-in-place concrete construction. The use of this guide may not be appropriate for installation of waterstops in other types of concrete construction, including but not limited to, pneumatically applied (that is, shotcrete) and precast concrete construction.
SCOPE
1.1 This guide covers the use of waterstops within cast-in-place concrete construction. Waterstops are generally placed within static, non-moving construction joints in concrete to close off the joint to water, which may be under significant hydrostatic pressure. They are used as part of the overall waterproofing strategy for a building or other structure. Expansion and other types of moving joints may require the use of waterstops, which can accommodate the anticipated movement of the structure and are beyond the scope of this guide.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents: therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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