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ASTM D3316-06(2011)

(Test Method)

Standard Test Method for Stability of Perchloroethylene with Copper

Standard Test Method for Stability of Perchloroethylene with Copper

SIGNIFICANCE AND USE
This test method is to be used as a guide in selecting or eliminating certain grades of perchloroethylene used for drycleaning fabrics or degreasing metal parts.
SCOPE
1.1 This test method covers the evaluation of the corrosiveness to copper metal by perchloroethylene.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Jul-2011
ICS
77.060 - Corrosion of metals
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.04 - Test Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D3316-06 - Standard Test Method for Stability of Perchloroethylene with Copper
Effective Date
01-Aug-2011

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ASTM D3316-06(2011) - Standard Test Method for Stability of Perchloroethylene with CopperASTM D3316-06(2011) - Standard Test Method for Stability of Perchloroethylene with Copper
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ASTM D3316-06(2011) - Standard Test Method for Stability of Perchloroethylene with Copper
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D3316 − 06(Reapproved 2011)
Standard Test Method for
Stability of Perchloroethylene with Copper
This standard is issued under the fixed designation D3316; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 5.3 Allihn Condenser, bulb type, 34/45 standard-taper bot-
tom joint.
1.1 This test method covers the evaluation of the corrosive-
ness to copper metal by perchloroethylene.
5.4 Bottle, wide-mouth, 8 oz.
1.2 The values stated in SI units are to be regarded as
5.5 Funnel, 8-mm outside diameter stem, 35-mm diameter
standard. No other units of measurement are included in this
opening.
standard.
5.6 Heater, variable control.
1.3 This standard does not purport to address all of the
5.7 Light Bulb, 100 W.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5.8 Beaker, 400 mL.
priate safety and health practices and determine the applica-
5.9 Analytical Balance.
bility of regulatory limitations prior to use.
6. Reagents and Materials
2. Referenced Documents
2.1 ASTM Standards: 6.1 Purity of Reagents—Reagent grade chemicals shall be
used in all tests. Unless otherwise indicated, it is intended that
E200 Practice for Preparation, Standardization, and Storage
of Standard and Reagent Solutions for ChemicalAnalysis all reagents shall conform to the specifications of the Commit-
tee on Analytical Reagents of the American Chemical Society,
3. Summary of Test Method
where such specifications are available. Other grades may be
used, provided it is first ascertained that the reagent is of
3.1 Clean copper strips are subjected to the action of liquid
sufficiently high purity to permit its use without lessening the
and vapor phases of boiling perchloroethylene for 72 h in the
accuracy of the determination.
presence of light. Weight loss of copper strips and acid
formation are determined at the end of the test period.
6.2 Purity of Water—Unless otherwise indicated, references
to water shall be understood to mean distilled water or water of
4. Significance and Use
equal purity.
4.1 This test method is to be used as a guide in selecting or
6.3 Acetone, practical grade.
eliminating certain grades of perchloroethylene used for dry-
6.4 Copper, electrolytic foil, 0.05 mm thick. Cut three
cleaning fabrics or degreasing metal parts.
copper strips, 20 by 75 mm. Immerse the strips in concentrated
HCl until the surface is bright and free of tarnish. Scribe
5. Apparatus
consecutive identification numbers on the strips. Rinse thor-
5.1 Flask, 300-mL, 24/40 standard-taper joint.
oughly in running water and dry with a towel. Weigh the strips
5.2 Soxhlet Extractor, 30-mm inside diameter, 24/40
to the nearest 0.1 mg on an analytical balance.
standard-taper bottom joint, 34/45 standard-taper upper joint.
6.5 Hydrochloric Acid (sp gr 1.19)—Concentrated hydro-
chloric acid (HCl). Handle the concentrated HCl solution as
indicated in the supplier’s direction.
This test method is under the jurisdiction of ASTM Committee D26 on
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
responsibility of Subcommittee D26.04 on Test Methods.
Current edition approved Aug. 1, 2011. Published November 2011. Originally
approved in 1974. Last previous edition approved in 2006 as D3316 – 06. DOI: Reagent Chemicals, American Chemical Society Specifications, American
10.1520/D3316-06R11. Chemical Society, Washington, DC. For suggestions on the testing of reagents not
For referenced ASTM standards, visit the ASTM website, www.astm.org, or listed by the American Chemical Society, see Analar Standards for Laboratory
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
Standards volume information, refer to the standard’s Document Summary page on and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,
the ASTM website. MD.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West C
...

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