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ASTM D3316-06

(Test Method)

Standard Test Method for Stability of Perchloroethylene with Copper

Standard Test Method for Stability of Perchloroethylene with Copper

SIGNIFICANCE AND USE
This test method is to be used as a guide in selecting or eliminating certain grades of perchloroethylene used for drycleaning fabrics or degreasing metal parts.
SCOPE
1.1 This test method covers the evaluation of the corrosiveness to copper metal by perchloroethylene.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2006
ICS
77.060 - Corrosion of metals
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.04 - Test Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D3316-96(2000) - Standard Test Method for Stability of Perchloroethylene with Copper
Effective Date
01-Jun-2006
Replaced By
ASTM D3316-06(2011) - Standard Test Method for Stability of Perchloroethylene with Copper
Effective Date
01-Aug-2011

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ASTM D3316-06 - Standard Test Method for Stability of Perchloroethylene with CopperASTM D3316-06 - Standard Test Method for Stability of Perchloroethylene with Copper
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ASTM D3316-06 - Standard Test Method for Stability of Perchloroethylene with Copper
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3316–06
Standard Test Method for
1
Stability of Perchloroethylene with Copper
This standard is issued under the fixed designation D3316; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 5.7 Light Bulb, 100 W.
5.8 Beaker, 400 mL.
1.1 This test method covers the evaluation of the corrosive-
5.9 Analytical Balance.
ness to copper metal by perchloroethylene.
1.2 This standard does not purport to address all of the
6. Reagents and Materials
safety concerns, if any, associated with its use. It is the
6.1 Purity of Reagents—Reagent grade chemicals shall be
responsibility of the user of this standard to establish appro-
used in all tests. Unless otherwise indicated, it is intended that
priate safety and health practices and determine the applica-
all reagents shall conform to the specifications of the Commit-
bility of regulatory limitations prior to use.
tee onAnalytical Reagents of theAmerican Chemical Society,
3
2. Referenced Documents where such specifications are available. Other grades may be
2 used, provided it is first ascertained that the reagent is of
2.1 ASTM Standards:
sufficiently high purity to permit its use without lessening the
E200 Practice for Preparation, Standardization, and Storage
accuracy of the determination.
of Standard and Reagent Solutions for Chemical Analysis
6.2 Purity of Water—Unless otherwise indicated, references
3. Summary of Test Method to water shall be understood to mean distilled water or water of
equal purity.
3.1 Clean copper strips are subjected to the action of liquid
6.3 Acetone, practical grade.
and vapor phases of boiling perchloroethylene for 72 h in the
6.4 Copper, electrolytic foil, 0.05 mm thick. Cut three
presence of light. Weight loss of copper strips and acid
copper strips, 20 by 75 mm. Immerse the strips in concentrated
formation are determined at the end of the test period.
HCl until the surface is bright and free of tarnish. Scribe
4. Significance and Use
consecutive identification numbers on the strips. Rinse thor-
oughly in running water and dry with a towel. Weigh the strips
4.1 This test method is to be used as a guide in selecting or
to the nearest 0.1 mg on an analytical balance.
eliminating certain grades of perchloroethylene used for dry-
6.5 Hydrochloric Acid (sp gr 1.19)—Concentrated hydro-
cleaning fabrics or degreasing metal parts.
chloric acid (HCl). Handle the concentrated HCl solution as
5. Apparatus
indicated in the supplier’s direction.
6.6 Sodium Hydroxide, Standard Solution (0.01 N 6
5.1 Flask, 300-mL, 24/40 standard-taper joint.
0.001)—Dissolve0.4 60.04gofanhydroussodiumhydroxide
5.2 Soxhlet Extractor, 30-mm inside diameter, 24/40
(NaOH) in 1 L of water and standardize in accordance with
standard-taper bottom joint, 34/45 standard-taper upper joint.
Practice E200.
5.3 Allihn Condenser, bulb type, 34/45 standard-taper bot-
6.7 Phenolphthalein Indicator—Dissolve5gof phenol-
tom joint.
phthalein in 500 mL of 95 % ethanol, dilute to 1 L with
5.4 Bottle, wide-mouth, 8 oz.
distilled water, and mix thoroughly.
5.5 Funnel, 8-mm outside diameter stem, 35-mm diameter
opening.
7. Procedure
5.6 Heater, variable control.
7.1 Clean the flask and Soxhlet extractor with soap and
water. Should any residue be present, clean thoroughly with
1
This test method is under the jurisdiction of ASTM Committee D26 on
acid and rinse with water. Flush out the condenser with water.
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
responsibility of Subcommittee D26.04 on Test Methods.
Current edition approved June 1, 2006. Published June 2006. Originally
3
approved in 1974 as D3316 – 74 T. Last previous edition approved in 2000 as Reagent Chemicals, American Chemical Society Specifications, American
D3316 – 96(2000). DOI: 10.1520/D3316-06. Chemical Society, Washington, DC. For suggestions on the testing of reagents not
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or listed by the American Chemical Society, see Analar Standards for Laboratory
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Chemicals, BDH Ltd., Poole, Dorset, U.K., and the United States Pharmacopeia
Standards volume information, refer to the standard’s Document Summary page on and National Formulary, U.S. Pharmacopeial Convention, Inc. (USPC), Rockville,
the ASTM website. MD.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3316–06
Rinse the flask, Soxhlet, and condenser with ac
...

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Note 1: All terms are listed alphabetically. When a subsidiary term is defined in conjunction with the definition of a more generic term, an alphabetically-listed cross-reference is provided.  
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