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ASTM E539-07

(Test Method)

Standard Test Method for X-Ray Fluorescence Spectrometric Analysis of 6Al-4V Titanium Alloy

Standard Test Method for X-Ray Fluorescence Spectrometric Analysis of 6Al-4V Titanium Alloy

SIGNIFICANCE AND USE
This method is suitable for providing data on the chemical composition of 6Al-4V titanium alloys for the scope elements. It is intended to be used for routine production control and for determination of chemical composition for the purpose of certifying material specification compliance. Additionally, the analytical performance data included with this method may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy.
SCOPE
1.1 This test method covers the X-ray fluorescence analysis of 6Al-4V titanium alloy for the following elements in the ranges indicated:
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 10.

General Information

Status
Historical
Publication Date
31-May-2007
ICS
71.040.50 - Physicochemical methods of analysis
77.120.50 - Titanium and titanium alloys
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.06 - Ti, Zr, W, Mo, Ta, Nb, Hf, Re
Current Stage
Ref Project

Relations

Replaces
ASTM E539-06 - Standard Test Method for X-Ray Emission Spectrometric Analysis of 6Al-4V Titanium Alloy
Effective Date
01-Jun-2007
Replaced By
ASTM E539-11 - Standard Test Method for Analysis of Titanium Alloys by X-Ray Fluorescence Spectrometry
Effective Date
01-May-2011
Referred By
ASTM B348/B348M-21 - Standard Specification for Titanium and Titanium Alloy Bars and Billets
Effective Date
01-Jun-2007
Referred By
ASTM F3001-14(2021) - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium ELI (Extra Low Interstitial) with Powder Bed Fusion
Effective Date
01-Jun-2007
Referred By
ASTM B977/B977M-19 - Standard Specification for Titanium and Titanium Alloy Ingots
Effective Date
01-Jun-2007
Referred By
ASTM B863-19 - Standard Specification for Titanium and Titanium Alloy Wire
Effective Date
01-Jun-2007
Referred By
ASTM B862-19 - Standard Specification for Titanium and Titanium Alloy Welded Pipe
Effective Date
01-Jun-2007
Referred By
ASTM F1472-23 - Standard Specification for Wrought Titanium-6Aluminum-4Vanadium Alloy for Surgical Implant Applications (UNS R56400)
Effective Date
01-Jun-2007
Referred By
ASTM F3046-21 - Standard Specification for Wrought Titanium-3Aluminum-2.5Vanadium Alloy for Surgical Implant Applications (UNS R56320)
Effective Date
01-Jun-2007
Referred By
ASTM F2924-14(2021) - Standard Specification for Additive Manufacturing Titanium-6 Aluminum-4 Vanadium with Powder Bed Fusion
Effective Date
01-Jun-2007
Referred By
ASTM F90-23 - Standard Specification for Wrought Cobalt-20Chromium-15Tungsten-10Nickel Alloy for Surgical Implant Applications (UNS R30605)
Effective Date
01-Jun-2007
Referred By
ASTM F2066-23 - Standard Specification for Wrought Titanium-15 Molybdenum Alloy for Surgical Implant Applications (UNS R58150)
Effective Date
01-Jun-2007
Referred By
ASTM B861-19 - Standard Specification for Titanium and Titanium Alloy Seamless Pipe
Effective Date
01-Jun-2007
Referred By
ASTM B381-21 - Standard Specification for Titanium and Titanium Alloy Forgings
Effective Date
01-Jun-2007
Referred By
ASTM F2989-21 - Standard Specification for Metal Injection Molded Unalloyed Titanium Components for Surgical Implant Applications
Effective Date
01-Jun-2007

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ASTM E539-07 - Standard Test Method for X-Ray Fluorescence Spectrometric Analysis of 6Al-4V Titanium AlloyASTM E539-07 - Standard Test Method for X-Ray Fluorescence Spectrometric Analysis of 6Al-4V Titanium Alloy
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ASTM E539-07 - Standard Test Method for X-Ray Fluorescence Spectrometric Analysis of 6Al-4V Titanium Alloy
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:E539–07
Standard Test Method for
X-Ray Fluorescence Spectrometric Analysis of 6Al-4V
1
Titanium Alloy
This standard is issued under the fixed designation E539; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E1361 Guide for Correction of Interelement Effects in
2 X-Ray Spectrometric Analysis
1.1 Thistestmethod coverstheX-rayfluorescenceanalysis
E1621 Guide for X-Ray Emission Spectrometric Analysis
of 6Al-4V titanium alloy for the following elements in the
ranges indicated:
3. Terminology
Element Concentration Range, %
3.1 Definitions:
Aluminum 4.6 to 7.2
Chromium 0.023 to 0.071
3.1.1 For definitions of terms used in this test method, refer
Copper 0.015 to 0.066
to Terminology E135.
Iron 0.1 to 0.3
Manganese 0.009 to 0.068
4. Summary of Test Method
Molybdenum 0.018 to 0.072
Nickel 0.026 to 0.073
4.1 The specimen is finished to a clean, uniform surface and
Silicon 0.03 to 0.06
then irradiated by high energy X-ray photons. Secondary X-
Tin 0.016 to 0.076
Vanadium 2.6 to 5.4
rays are produced and emitted from the sample. This radiation
Zirconium 0.009 to 0.064
is diffracted by means of analyzing crystals and focused on a
1.2 This standard does not purport to address all of the detector which measures the count rates at specified wave-
safety concerns, if any, associated with its use. It is the lengths. The outputs of the detectors in voltage pulses are
responsibility of the user of this standard to establish appro- integrated or counted. Radiation measurements are made based
priate safety and health practices and determine the applica- on the time required to reach a fixed number of counts, or on
bility of regulatory limitations prior to use. Specific precau- the total counts obtained for a fixed time (generally expressed
tionary statements are given in Section 10. in counts per unit time). Concentrations of the elements are
determined by relating the measured radiation of unknown
2. Referenced Documents
samples to calibration curves prepared using reference materi-
3
2.1 ASTM Standards: als of known compositions.
E135 Terminology Relating to Analytical Chemistry for
5. Significance and Use
Metals, Ores, and Related Materials
5.1 This method is suitable for providing data on the
E1172 Practice for Describing and Specifying a
chemical composition of 6Al-4V titanium alloys for the scope
Wavelength-Dispersive X-Ray Spectrometer
elements. It is intended to be used for routine production
E1329 PracticeforVerificationandUseofControlChartsin
control and for determination of chemical composition for the
Spectrochemical Analysis
purpose of certifying material specification compliance. Addi-
tionally, the analytical performance data included with this
method may be used as a benchmark to determine if similar
1
This test method is under the jurisdiction of ASTM Committee E01 on
X-ray spectrometers provide equivalent precision and accu-
Analytical Chemistry for Metals, Ores, and Related Materials and is the direct
racy.
responsibility of Subcommittee E01.06 on Ti, Zr, W, Mo, Ta, Nb, Hf, Re.
Current edition approved June 1, 2007. Published June 2007. Originally
approved in 1975. Last previous edition approved in 2006 as E539 – 06. DOI: 6. Interferences
10.1520/E0539-07.
2 6.1 Line overlaps, interelement effects and matrix effects
Supporting data for this test method as determined by cooperative testing have
may exist for some of the scope elements. A list of potential
been filed at ASTM International Headquarters and may be obtained by requesting
Research Report RR:E2-1010 and Research Report RR:E01-1061.
line overlaps is provided in section 6.2. Modern X-ray spec-
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
trometers provide software for generation of mathematical
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
corrections to model the effects of line overlaps, interelement
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. and matrix interferences. The user of this method may choose
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
E539–07
to use these mathematical corrections for analysis. Guide as well as state and local regulations relating to radiation
E1621 provide a more extensive overview of mathematical hygiene must be followed. Additionally, the safety guidelines
interference correction methods. established by the instrument manufacturer should be fol-
6.2 Potential lin
...

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5.1 This test method for the chemical analysis of titanium and titanium alloys is primarily intended to test material for compliance with specifications of chemical composition such as those under the jurisdiction of ASTM Committee B10. It may also be used to test compliance with other specifications that are compatible with the test method.  
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1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:    
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Copper  
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Yttrium  
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1.2 This test method has been interlaboratory tested for the elements and ranges specified in the quantitative range part of the table in 1.1. It may be possible to extend this test method to other elements or broader mass fraction ranges as shown in the application range part of the table above provided that test method validation is performed that includes evaluation of method sensitivity, precision, and bias. Additionally, the validation study shall evaluate the acceptability of sample preparation methodology using reference materials or spike recoveries, or both. Guide E2857 provides information on validation of analytical methods for alloy analysis.  
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SIGNIFICANCE AND USE
5.1 This method is suitable for providing data on the chemical composition of titanium alloys having compositions within the scope of the standard. It is intended for routine production control and for determination of chemical composition for the purpose of certifying material specification compliance. Additionally, the analytical performance data included with this method may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy.  
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1.1 This test method2 covers the X-ray fluorescence analysis of titanium alloys for the following elements in the ranges indicated:    
Element  
Range, %  
Aluminum  
0.041 to 8.00  
Chromium  
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Copper  
0.015 to 0.60  
Iron  
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Palladium  
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0.019 to 0.050  
Silicon  
0.014 to 0.15  
Tin  
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Vanadium  
0.017 to 15.50  
Yttrium  
0.0011 to 0.0100  
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1.1 This method describes the analysis of titanium and titanium alloys, such as specified by committee B10, by inductively coupled plasma atomic emission spectrometry (ICP-AES) and direct current plasma atomic emission spectrometry (DCP-AES) for the following elements:    
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1.1 This specification covers preformed expansion joint fillers made from closed-cell polypropylene foam materials having suitable compressibility, recovery from compression, nonextruding, and weather-resistant characteristics.  
1.1.1 Type I, closed-cell polypropylene foam.  
1.2 These joint fillers are intended for use in concrete pavements in full-depth joints. There are several variations in size with typical thicknesses of 1/2 in. (12.7 mm), 3/4 in. (19.05 mm), and 1 in. (25.4 mm); typical widths of 31/2 in. (88.9 mm), 4 in. (101.6 mm), 5 in. (127 mm), 6 in. (152.5 mm), 7 in. (177.8 mm), 8 in. (203.2 mm), or 48 in. (1.2 m) sheet; and typical lengths of 5 ft (1.52 m) and 10 ft (3.05 m).  
1.3 The values stated in inch-pound units are to be regarded as the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
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  • Technical specification
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ASTM
ASTM F3337-23(Guide)
Standard Guide for Taking Property and Behavior Measurements on Weathered Fractions of Oil

SIGNIFICANCE AND USE
5.1 A standard procedure is necessary to establish property changes for spilled oils or petroleum products at different oil weathering stages.  
5.2 This procedure employs standardized equipment, and test procedures.  
5.3 This procedure should be performed at the stages of weathering corresponding to the spill conditions of interest.
SCOPE
1.1 This guide summarizes methods to fractionate oil by evaporative weathering and then measure the properties and behavior of the weathered oil. The results of this guide can provide oil behavior data for input into oil spill models and response method selection.  
1.2 This guide covers general procedures for oil weathering and behavior and does not cover all possible procedures which may be applicable to this topic.  
1.3 The results obtained using this guide are intended to provide baseline data for the behavior of oil and petroleum products when spilled and input to oil spill models.  
1.4 The results obtained using this guide can be used directly to predict certain facets of oil spill behavior or as input to oil spill models.  
1.5 The accuracy of the guide depends very much on the representative nature of the oil sample used. Certain oils can have different properties depending on their chemical contents at the moment a sample is taken.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Guide
    4 pages
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  • Guide
    4 pages
    English language
    sale 15% off