ASTM D1337-10
(Test Method)Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength
Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength
SIGNIFICANCE AND USE
This practice may be used to determine the storage life of any adhesive where this information is required.
This practice is intended to determine whether the storage life conforms to the minimum specified storage life required of an adhesive by viscosity tests (Procedure A) or by bond strength tests (Procedure B), or by both. It does so by providing results before and after a set of standard conditions that simulate storage life. The determination of what the requirements for percentage of the original property retained or the minimum value for a property is found in the relevant material specification, or as agreed between manufacturer and user.
SCOPE
1.1 This practice describes a laboratory method by which the storage life of an adhesive may be measured using viscosity, adhesive strength, or a combination thereof.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D1337 − 10
StandardPractice for
1
Storage Life of Adhesives by Viscosity and Bond Strength
This standard is issued under the fixed designation D1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 This practice describes a laboratory method by which 4.1 This practice may be used to determine the storage life
the storage life of an adhesive may be measured using of any adhesive where this information is required.
viscosity, adhesive strength, or a combination thereof.
4.2 This practice is intended to determine whether the
1.2 The values stated in SI units are to be regarded as the storage life conforms to the minimum specified storage life
standard. The values given in parentheses are for information required of an adhesive by viscosity tests (Procedure A) or by
only. bond strength tests (Procedure B), or by both. It does so by
providing results before and after a set of standard conditions
1.3 This standard does not purport to address all of the
that simulate storage life. The determination of what the
safety concerns, if any, associated with its use. It is the
requirements for percentage of the original property retained or
responsibility of the user of this standard to establish appro-
the minimum value for a property is found in the relevant
priate safety and health practices and determine the applica-
material specification, or as agreed between manufacturer and
bility of regulatory limitations prior to use.
user.
2. Referenced Documents
PROCEDURE A—VISCOSITY TEST
2
2.1 ASTM Standards:
5. Apparatus
D618 Practice for Conditioning Plastics for Testing
D897 Test Method for Tensile Properties ofAdhesive Bonds
5.1 Viscometer—Use the apparatus as described in ISO
D906 Test Method for Strength Properties of Adhesives in
2555.
Plywood Type Construction in Shear by Tension Loading
5.2 Controlled-Temperature Chamber, capable of maintain-
D907 Terminology of Adhesives
ing temperature to 63°C (65°F), to provide temperature
D1002 Test Method for Apparent Shear Strength of Single-
storage conditions.
Lap-Joint Adhesively Bonded Metal Specimens by Ten-
sion Loading (Metal-to-Metal)
6. Storage of Adhesive
D1084 Test Methods for Viscosity of Adhesives
6.1 Store the adhesive and all its components, if there are
3
2.2 Other Standard:
any, in their original and unopened containers when the
ISO2555 Plastics—Resinsintheliquidstateorasemulsions
container is approximately litre (or quart) size. When the
or dispersions—Determination of apparent viscosity by
adhesive is supplied in larger containers, the desired number of
the Brookfield Test method
samples is withdrawn from the large container. In this latter
case, the size, type of closure, and nature (such as glass, steel,
3. Terminology
or tin-coated steel) of the small storage container is agreed
3.1 Definitions—Many terms in this practice are defined in
upon by the purchaser and the manufacturer.
Terminology D907.
6.2 For storage temperature, use any one of the standard
temperatures specified in Practice D618. The time of storage is
any time agreed upon by the purchaser and the manufacturer. If
1
This practice is under the jurisdiction of ASTM Committee D14 on Adhesives
and is the direct responsibility of Subcommittee D14.10 on Working Properties. the effect of storage time is desired, it is suggested that at least
Current edition approved Nov. 1, 2010. Published December 2010. Originally
three quantities of the adhesive be stored under the prescribed
approved in 1954. Last previous edition approved in 2004 as D1337 – 04. DOI:
conditions, and tested at various intervals of time. Use a
10.1520/D1337-10.
2 separate, unopened container at each such test.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on 7. Conditioning
the ASTM website.
3
7.1 Condition all containers after storage at 23 6 3°C (73.4
Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
4th Floor, New York, NY 10036, http://www.ansi.org. 6 5°F) before opening. If the adhesive consists of two or more
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D1337 − 10
components, blend the components in accordance with the 13. Preparation of Test Specimens
instructions from the manufacturer, and again adjust the
13.1 Prepare test panels or sheets for
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D1337–04 Designation:D1337–10
Standard Practice for
1
Storage Life of Adhesives by Viscosity and Bond Strength
This standard is issued under the fixed designation D1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1This practice covers a means by which the storage life of an adhesive can be measured using viscosity and adhesive
performance testing.
1.1 This practice describes a laboratory method by which the storage life of an adhesive may be measured using viscosity,
adhesive strength, or a combination thereof.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D618 Practice for Conditioning Plastics for Testing
D897 Test Method for Tensile Properties of Adhesive Bonds
D906 Test Method for Strength Properties of Adhesives in Plywood Type Construction in Shear by Tension Loading
D907 Terminology of Adhesives
D1002 Test Method forApparent Shear Strength of Single-Lap-JointAdhesively Bonded Metal Specimens byTension Loading
(Metal-to-Metal)
D1084 Test Methods for Viscosity of Adhesives
3
2.2 Other Standard:
ISO 2555 Plastics—Resins in the liquid state or as emulsions or dispersions—Determination of apparent viscosity by the
Brookfield Test method
3. Terminology
3.1 Definitions—Many terms in this practice are defined in Terminology D907.
4. Significance and Use
4.1This practice is applicable to all adhesives having a relatively short storage life.
4.1 This practice may be used to determine the storage life of any adhesive where this information is required.
4.2 This practice is intended to determine whether the storage life conforms to the minimum specified storage life required of
an adhesive by viscosity tests (Procedure A) or by bond strength tests (Procedure B), or by both. It does so by providing results
before and after a set of standard conditions that simulate storage life. The determination of what the requirements for percentage
of the original property retained or the minimum value for a property is found in the relevant material specification, or as agreed
between manufacturer and user.
PROCEDURE A—VISCOSITY TEST
5. Apparatus
5.1 Viscometer—Use the apparatus as described in Test Methods D1084, Method B. —Use the apparatus as described in ISO
2555.
1
This practice is under the jurisdiction of ASTM Committee D14 on Adhesives and is the direct responsibility of Subcommittee D14.10 on Working Properties.
Current edition approved AprilNov. 1, 2004.2010. Published April 2004.December 2010. Originally approved in 1954. Last previous edition approved in 19962004 as
D1337–96.D1337 – 04. DOI: 10.1520/D1337-104.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D1337–10
5.2 Controlled-Temperature Chamber, capable of maintaining temperature to 63°C (65°F), to provide temperature storage
conditions.
6. Storage of Adhesive
6.1 Store the adhesive and all its components, if there are any, in their original and unopened containers when the container is
approximately litre (or quart) size.When the adhesive is supplied in larger containers, the desired number of samples is withdrawn
from the large container. In this latter case, the size, type of closure, and nature (such as glass, steel, or tin-coated steel) of the small
storage container is agreed upon by the purchaser and the manufacturer.
6.2 For storage temperature, use any one of the standard temperatures specified in Practice D618. The time of storage is any
time ag
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