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ASTM D4209-82(2002)

(Practice)

Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes

Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes

SCOPE
1.1 This practice is intended to serve as a guide to the selection of the proper ASTM test method for determining the volatile and nonvolatile content of cellulosics, emulsions, resin solutions, shellac, and varnishes.
Note 1—Standards for determining the composition of the volatile fraction are not covered by this practice.
1.2 The standards referenced in the practice are as follows:ClassificationSectionASTM StandardCellulosics5.1D 871 D 914D 1347Emulsions5.2D 2369Resin Solutions5.3D 1259 D 1490Shellac 5.4D 29D 1650Varnishes5.5D 115 D 1644

General Information

Status
Historical
Publication Date
25-Nov-1982
ICS
87.060.20 - Binders
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D4209-82(1996) - Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes
Effective Date
26-Nov-1982
Replaced By
ASTM D4209-07 - Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes
Effective Date
01-Jul-2007
Referred By
ASTM D16-23 - Standard Terminology for Paint, Related Coatings, Materials, and Applications
Effective Date
26-Nov-1982

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ASTM D4209-82(2002) - Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and VarnishesASTM D4209-82(2002) - Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes
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ASTM D4209-82(2002) - Standard Practice for Determining Volatile and Nonvolatile Content of Cellulosics, Emulsions, Resin Solutions, Shellac, and Varnishes
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D4209–82(Reapproved2002)
Standard Practice for
Determining Volatile and Nonvolatile Content of Cellulosics,
Emulsions, Resin Solutions, Shellac, and Varnishes
This standard is issued under the fixed designation D 4209; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 1644 Test Methods for Nonvolatile Content ofVarnishes
D 1650 Test Methods for Sampling and Testing Shellac
1.1 This practice is intended to serve as a guide to the
Varnish
selection of the proper ASTM test method for determining the
D 2369 Test Method for Volatile Content of Coatings
volatile and nonvolatile content of cellulosics, emulsions, resin
D 4758 Test Method for Nonvolatile Content of Latexes
solutions, shellac, and varnishes.
NOTE 1—Standards for determining the composition of the volatile 3. Terminology (see Terminology D 16)
fraction are not covered by this practice.
3.1 Definitions:
1.2 The standards referenced in the practice are as follows:
3.1.1 cellulose esters—derivatives of cellulose in which one
Classification Section ASTM Standard or more of the hydroxyl hydrogens have been replaced by acyl
Cellulosics 5.1 D 871
groups.
D 914
3.1.2 cellulose ethers—derivatives of cellulose in which
D 1347
Emulsions 5.2 D 2369 one or more of the hydroxyl hydrogens have been replaced by
Resin Solutions 5.3 D 1259
alkyl groups.
D 1490
3.1.3 cellulose nitrates (nitrocellulose)—derivatives of cel-
Shellac 5.4 D 29
D 1650
lulose in which one or more of the hydroxyl hydrogens have
Varnishes 5.5 D 115
been replaced by nitrate groups.
D 1644
3.1.4 emulsion vehicle—anemulsionofbinderinwater.The
2. Referenced Documents binder may be oil, oleoresinous varnish, resin, or other emul-
sifiable liquid.
2.1 ASTM Standards:
3.1.5 latex—a stable aqueous dispersion of synthetic resin,
D 16 Terminology for Paint, Related Coatings, Materials,
2 produced by emulsion polymerization, as the principal con-
and Applications
stituent of the binder.
D 29 Test Methods for Sampling and Testing Lac Resins
3.1.6 shellac varnish—a solution or “cut” of a specified
D 115 Test Methods for Testing Solvent Containing Var-
type and grade of dry lac resin in a suitable alcohol.
nishes Used for Electrical Insulation
3 3.1.7 varnish—a liquid composition that is converted by
D 360 Specification for Shellac Varnishes
oxidation or thermal cross-linking to a transparent or translu-
D 871 Test Methods of Testing Cellulose Acetate
3 cent solid film after application as a thin layer.
D 914 Test Methods For Ethylcellulose
D 1259 Test Methods for Nonvolatile Content of Resin
4. Significance and Use
Solutions
3 4.1 The nonvolatile content of raw materials may be used to
D 1347 Test Methods for Methylcellulose
determine the total nonvolatile content (solids) of paint and
D 1490 Test Method for Nonvolatile Content of Urea-
5 related coatings. Such information may be useful to coatings
Formaldehyde Resin Solutions
producers and users for the determination of the total solids
available for film formation and for the estimation of the
This practice is under the jurisdiction of ASTM Committee D01 on Paint and volatile organic content.
Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.21 on Chemical Analysis of Paint and Paint Materials.
5. Procedure
Current edition approved Nov. 26, 1982. Published January 1983.
5.1 Cellulosics:
Annual Book of ASTM Standards, Vol 06.01.
Annual Book of ASTM Standards, Vol 06.03.
Annual Book of ASTM Standards, Vol 10.01.
Annual Book of ASTM Standards, Vol 15.06.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D4209
5.1.1 Test Methods D 1644, Method A, should be used for 5.4 Shellac:
determining the amount of alcohol present in nitrocellulose 5.4.1 Sections 14 and 15 ofTest Methods D 29 describe two
shipments. This method may also be used for other cellulose methods for the determination of volatile matter (moisture) in
derivatives if mutually agreed upon by producer and user. lac resins. Method A (Section 14) is recommended for orange
5.1.2 Moisture in three different cellulose derivatives may shellac, button lac, garnet lac, and dry bleached
...

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