ASTM D939-54
(Test Method)Method of Test for Saponification Number by Potentiometric Titration (Withdrawn 1962)
Method of Test for Saponification Number by Potentiometric Titration (Withdrawn 1962)
General Information
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SIGNIFICANCE AND USE
4.1 The primary use of these test methods is testing to determine the specified mechanical properties of steel, stainless steel, and related alloy products for the evaluation of conformance of such products to a material specification under the jurisdiction of ASTM Committee A01 and its subcommittees as designated by a purchaser in a purchase order or contract.
4.1.1 These test methods may be and are used by other ASTM Committees and other standards writing bodies for the purpose of conformance testing.
4.1.2 The material condition at the time of testing, sampling frequency, specimen location and orientation, reporting requirements, and other test parameters are contained in the pertinent material specification or in a general requirement specification for the particular product form.
4.1.3 Some material specifications require the use of additional test methods not described herein; in such cases, the required test method is described in that material specification or by reference to another appropriate test method standard.
4.2 These test methods are also suitable to be used for testing of steel, stainless steel and related alloy materials for other purposes, such as incoming material acceptance testing by the purchaser or evaluation of components after service exposure.
4.2.1 As with any mechanical testing, deviations from either specification limits or expected as-manufactured properties can occur for valid reasons besides deficiency of the original as-fabricated product. These reasons include, but are not limited to: subsequent service degradation from environmental exposure (for example, temperature, corrosion); static or cyclic service stress effects, mechanically-induced damage, material inhomogeneity, anisotropic structure, natural aging of select alloys, further processing not included in the specification, sampling limitations, and measuring equipment calibration uncertainty. There is statistical variation in all aspects of mechanical testin...
SCOPE
1.1 These test methods2 cover procedures and definitions for the mechanical testing of steels, stainless steels, and related alloys. The various mechanical tests herein described are used to determine properties required in the product specifications. Variations in testing methods are to be avoided, and standard methods of testing are to be followed to obtain reproducible and comparable results. In those cases in which the testing requirements for certain products are unique or at variance with these general procedures, the product specification testing requirements shall control.
1.2 The following mechanical tests are described:
Sections
Tension
7 to 14
Bend
15
Hardness
16
Brinell
17
Rockwell
18
Portable
19
Impact
20 to 30
Keywords
32
1.3 Annexes covering details peculiar to certain products are appended to these test methods as follows:
Annex
Bar Products
Annex A1
Tubular Products
Annex A2
Fasteners
Annex A3
Round Wire Products
Annex A4
Significance of Notched-Bar Impact Testing
Annex A5
Converting Percentage Elongation of Round Specimens to
Equivalents for Flat Specimens
Annex A6
Testing Multi-Wire Strand
Annex A7
Rounding of Test Data
Annex A8
Methods for Testing Steel Reinforcing Bars
Annex A9
Procedure for Use and Control of Heat-cycle Simulation
Annex A10
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.5 When these test methods are referenced in a metric product specification, the yield and tensile values may be determined in inch-pound (ksi) units then converted into SI (MPa) units. The elongation determined in inch-pound gauge lengths of 2 in. or 8 in. may be report...
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SIGNIFICANCE AND USE
4.1 This test method enumerates salt tolerant (halophilic) bacteria, and proteolytic bacteria that are also salt tolerant. Under the conditions of this test method those bacteria are equated as halophilic organisms. Salt tolerant proteolytic bacteria have been known to cause damage to hides and skins in raceway brine.
SCOPE
1.1 This test method covers the enumeration of bacteria that can tolerate high salt concentrations or can hydrolyze protein/collagen, or both. This test method is applicable to raceway brine, brine-cured hides and skins, and pre-charge raceway liquor.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Both physical and chemical changes possibly occur from weather exposure, and these changes affect performance properties, service life, and maintenance schedules. For this reason, tests of properties relating to performance shall be made both before and after specific periods of outdoor exposure.
5.2 This test method recognizes that differing geographical locations, environmental conditions, differences between surface temperatures and ambient temperatures, and test durations have extremely varied effects upon the test results.
5.3 This test method is to be used for comparative qualitative testing.
SCOPE
1.1 This test method covers out-of-doors exposure testing of finishes that are normally field-applied to thermal insulation and possibly include joints or joint sealants, or both. Such exposure is essential prior to the determination of certain physical properties when the finish is to be exposed to exterior weather conditions. This test method also indicates possible compatibility problems between the joint sealant and the finish as well as the ability of the finish to span a dry joint. This test method is not intended to evaluate mildew resistance, efflorescence, or chemical resistance.
Note 1: For testing free plastic films, see Practice D1435.
1.2 This test method does not prescribe the method of application, test duration, or inspection intervals.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 The UNS provides a means of correlating many nationally used numbering systems currently administered by societies, trade associations, and individual users and producers of metals and alloys, thereby avoiding confusion caused by use of more than one identification number for the same material; and by the opposite situation of having the same number assigned to two or more entirely different materials. It also provides the uniformity necessary for efficient indexing, record keeping, data storage and retrieval, and cross referencing.
4.2 A UNS number is not in itself a specification, since it establishes no requirements for form, condition, quality, etc. It is a unified identification of metals and alloys for which controlling limits have been established in specifications published elsewhere.
Note 5: Organizations that issue specifications should report to appropriate UNS number-assigning offices (3.1.2) any specification changes that affect descriptions shown in published UNS listings.
SCOPE
1.1 This practice (Note 1) covers a unified numbering system (UNS) for metals and alloys that have a “commercial standing” (see Note 2), and covers the procedure by which such numbers are assigned. Section 2 describes the system of alphanumeric designations or “numbers” established for each family of metals and alloys. Section 3 outlines the organization established for administering the system. Section 5 describes the procedure for requesting number assignment to metals and alloys for which UNS numbers have not previously been assigned.
Note 1: UNS designations are not to be used for metals and alloys that are not registered under the system described herein, or for any metal or alloy whose composition differs from those registered.
Note 2: The terms “commercial standing,” “production usage,” and other similar terms are intended to apply to metals and alloys in active commercial production and use, although the actual amount of such use will depend, among other things, upon the type of metals and alloys involved and their application.
The various standardizing organizations involved with the individual industries apply their own established criteria to define the status of a metal or alloy in terms of when a UNS designation number will be assigned. For instance, ASTM Committee A01 requires details of heat analysis, mechanical properties, and processing requirements for addition of a new grade or alloy to its specifications. The Copper Development Association requires that the material be “in commercial use (without tonnage limits);” the Aluminum Association requires that the alloy be “offered for sale (not necessarily in commercial use);” the SAE Aerospace Materials Division calls for “repetitive procurement by at least two users.”
Thus, while no universal definition for usage criteria is established, the UNS numbers are intended to identify metals and alloys that are generally in regular production and use. A UNS number will not ordinarily be issued for a material that has just been conceived or that is still in only experimental trial.
1.2 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers emergency conditions, occupant safety and accommodations for occupants and cargo. The applicant for a design approval must seek the individual guidance of their respective civil aviation authority (CAA) body concerning the use of this standard as part of a certification plan.
SCOPE
1.1 This specification addresses emergency conditions, occupant safety and accommodations for occupants and cargo.
1.2 The applicant for a design approval must seek the individual guidance of their respective civil aviation authority (CAA) body concerning the use of this standard as part of a certification plan. For information on which CAA regulatory bodies have accepted this standard (in whole or in part) as a means of compliance to their airworthiness regulations (Hereinafter referred to as “the Rules”), refer to ASTM F44 webpage (www.ASTM.org/COMITTEE/F44.htm) which includes CAA website links.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification covers a group of common requirements that, unless covered by the individual product specification in another ASTM document, applies to steel forgings for general use. Materials shall be produced primarily by either electric-furnace, basic oxygen, vacuum-induction (VIM), or open-hearth melting process. The primary melting may incorporate separate degassing or refining and may be followed by secondary melting, using electro slag (ESR) or vacuum arc remelting (VAR). Steel shall be forged by any of these three classes based on forging temperature: cold-worked forging, hot-cold-worked forging, or hot-worked forging. After forging, specimens shall be allowed to cool prior to reheating for heat treatment. Details of heat and product analyses for the evaluation of chemical composition are thoroughly discussed. Tension and hardness tests shall be conducted to evaluate mechanical properties such as percentage of elongation and reduction of area. Repair welding shall not be allowed unless permitted by the product specification.
SCOPE
1.1 This specification2 covers a group of common requirements that, unless otherwise specified in the individual product specification, shall apply to steel forgings under any of the following specifications issued by ASTM:
ASTM Designation
Title
A266/A266M
Carbon Steel Forgings for Pressure Vessel Components
A288
Carbon and Alloy Steel Forgings for Magnetic Retaining Rings for Turbine Generators
A289/A289M
Alloy Steel Forgings for Nonmagnetic Retaining Rings for Generators
A290/A290M
Carbon and Alloy Steel Forgings for Rings for Reduction Gears
A291/A291M
Steel Forgings, Carbon and Alloy, for Pinions, Gears, and Shafts for Reduction Gears
A336/A336M
Alloy Steel Forgings for Pressure and High-Temperature Parts
A372/A372M
Carbon and Alloy Steel Forgings for Thin-Walled Pressure Vessels
A469/A469M
Vacuum-Treated Steel Forgings for Generator Rotors
A470/A470M
Vacuum-Treated Carbon and Alloy Steel Forgings for Turbine Rotors and Shafts
A471/A471M
Vacuum-Treated Alloy Steel Forgings for Turbine Rotor Disks and Wheels
A473
Stainless Steel Forgings
A504/A504M
Wrought Carbon Steel Wheels
A508/A508M
Quenched and Tempered Vacuum-Treated Carbon and Alloy Steel Forgings for Pressure Vessels
A541/A541M
Quenched and Tempered Carbon and Alloy Steel Forgings for Pressure Vessel Components
A579/A579M
Superstrength Alloy Steel Forgings
A592/A592M
High-Strength Quenched and Tempered Low-Alloy Steel Forged Parts for Pressure Vessels
A646/A646M
Premium Quality Alloy Steel Blooms and Billets for Aircraft and Aerospace Forgings
A649/A649M
Forged Steel Rolls Used for Corrugating Paper Machinery
A668/A668M
Steel Forgings, Carbon and Alloy, for General Industrial Use
A705/A705M
Age-Hardening Stainless Steel Forgings
A711/A711M
Steel Forging Stock
A723/A723M
Alloy Steel Forgings for High-Strength Pressure Component Application
A729/A729M
Carbon and Alloy Steel Axles, Heat Treated, for Mass Transit and Electric Railway Service
A765/A765M
Carbon Steel and Low-Alloy Steel Pressure-Vessel-Component Forgings with Mandatory Toughness Requirements
A837/A837M
Steel Forgings, Alloy, for Carburizing Applications
A859/A859M
Age-Hardening Alloy Steel Forgings for Pressure Vessel Components
A891/A891M
Precipitation Hardening Iron Base Superalloy Forgings for Turbine Rotor Disks and Wheels
A909/A909M
Steel Forgings, Microalloy, for General Industrial Use
A965/A965M
Steel Forgings, Austenitic, for Pressure and High Temperature Parts
A982/A982M
Steel Forgings, Stainless, for Compressor and Turbine Airfoils
A983/A983M
Continuous Grain Flow Forged Carbon and Alloy Steel Crankshafts for Medium Speed Diesel Engines
A986/A986M
Magnetic Particle Examination of Cont...
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ABSTRACT
This specification covers iron-chromium-nickel-copper corrosion resistance steel castings capable of being strengthened by precipitation hardening heat treatment. The steel shall be made by electric furnace process with or without separate refining such as argon-oxygen decarburization. The steel materials shall also undergo homogenization heat treatment, solution annealing heat treatment, precipitation hardening and shall conform to the required values of temperature and time and cooling treatment. The materials shall conform to the required chemical compositions of carbon, manganese, phosphorus, sulfur, silicon, chromium, nickel, copper, columbium, and nitrogen.
SCOPE
1.1 This specification covers iron-chromium-nickel-copper corrosion-resistant steel castings, capable of being strengthened by precipitation hardening heat treatment.
1.2 These castings may be used in services requiring corrosion resistance and high strengths at temperatures up to 600 °F [315 °C]. They may be machined in the solution heat-treated condition and subsequently precipitation hardened to the desired high-strength mechanical properties specified in Table S51.1 with little danger of cracking or distortion.
1.3 The material is not intended for use in the solution heat-treated condition.
Note 1: If the service environment in which the material is to be used is considered conducive to stress-corrosion cracking, precipitation hardening should be performed at a temperature that will minimize the susceptibility of the material to this type of attack.
1.4 Supplementary requirements of an optional nature are provided for use at the option of the purchaser. The supplementary requirements shall apply only when specified individually by the purchaser in the purchase order or contract.
1.5 This specification is expressed in both inch-pound units and in SI units; however, unless the purchase order or contract specifies the applicable M-specification designation (SI units), the inch-pound units shall apply.
1.6 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Within the text, the SI units are shown in brackets.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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ABSTRACT
This specification contains the general requirements for the 245/7OR19.5 136/134M radial truck standard reference test. Provided in this specification is a 19.5 rim diameter code standard truck design and construction, standard dimensions, and standard conditions of storage. A reference tire is covered in this specification for braking traction, snow traction, wear evaluations pavement roughness, noise and other forms of test requiring a reference tire. Test methods of the tensile sheet cure, the 300% stress elongation, and tensile sheet strength should be in accordance to the specified testing requirements presented in D3182, and D412. The testing procedure also includes using of Type A durometer centred at the presser foot at a minimum of 6.0 mm, chaking the durometer operation and the state of durometer calibration with rubber reference, determining tire tread hardness by four readings and quickly applying the presser foot to the tire tread without inducing shock.
SCOPE
1.1 This specification covers the general requirements for the 245/70R19.5 136/134M radial truck standard reference test tire. The tire covered by this specification is primarily for use as a reference tire for braking traction, snow traction, and wear performance evaluations, but may also be used for other evaluations, such as pavement roughness, noise, or other tests that require a reference tire.
1.1.1 Other standard reference test tires are also used for these purposes and are referenced in Section 2.
1.2 This specification provides a 19.5 rim diameter code standard truck tire design and construction, standard dimensions, and specifies the conditions of storage.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 There is typically a higher concentration of soluble alkali salts in the surface region of a concrete slab due to the initial bleeding process of a freshly placed concrete slab. If after a resilient floor covering material is installed there is sufficient moisture within the slab to place these salts into solution a potentially damaging high pH solution can develop beneath the installed material.
4.2 Results obtained through the use of this guide indicate the comparative pH of reagent water placed on properly prepared concrete slab surfaces only at the time of the procedure and in the specific locations evaluated.
4.3 If pre-installation surface pH evaluation is required by the manufacturer of the resilient flooring, adhesive, patching/underlayment products or project specifications, their instructions and limitations should be consulted.
SCOPE
1.1 This guide discusses procedures that may be used for evaluating the comparative change in pH of reagent water placed on the surface of a properly prepared concrete slab surface.
1.2 This guide is intended to be used in conjunction with the flat surface electrode pH meter manufacturer’s calibration procedures, operation instructions, and interpretive data where available.
1.3 This guide is intended to be used in conjunction with the pH paper manufacturer’s instructions, product shelf life, and interpretive data where available.
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use Some specific hazards statements are given in Section 9 on Hazards.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
3.1 The objectives of a reactor vessel surveillance program are twofold. The first requirement of the program is to monitor changes in the fracture toughness properties of ferritic materials in the reactor vessel beltline region resulting from exposure to neutron irradiation and the thermal environment. The second requirement is to make use of the data obtained from the surveillance program to determine the conditions under which the vessel can be operated throughout its service life.
3.1.1 To satisfy the first requirement of 3.1, the tasks to be carried out are straightforward. Each of the irradiation capsules that comprise the surveillance program may be treated as a separate experiment. The goal is to define and carry to completion a dosimetry program that will, a posteriori, describe the neutron field to which the material test specimens were exposed. The resultant information will then become part of a database applicable in a stricter sense to the specific plant from which the capsule was removed, but also in a broader sense to the industry as a whole.
3.1.2 To satisfy the second requirement of 3.1, the tasks to be carried out are somewhat complex. The objective is to describe accurately the neutron field to which the pressure vessel itself will be exposed over its service life. This description of the neutron field must include spatial gradients within the vessel wall. Therefore, heavy emphasis must be placed on the use of neutron transport techniques as well as on the choice of a design basis for the computations. Since a given surveillance capsule measurement, particularly one obtained early in plant life, is not necessarily representative of long-term reactor operation, a simple normalization of neutron transport calculations to dosimetry data from a given capsule may not be appropriate (1-67).
3.2 The objectives and requirements of a reactor vessel's support structure's surveillance program are much less stringent, and at present, are limited to ...
SCOPE
1.1 This practice covers the methodology, summarized in Annex A1, to be used in the analysis and interpretation of neutron exposure data obtained from LWR pressure vessel surveillance programs and, based on the results of that analysis, establishes a formalism to be used to evaluate present and future condition of the pressure vessel and its support structures2 (1-74).3
1.2 This practice relies on, and ties together, the application of several supporting ASTM standard practices, guides, and methods (see Master Matrix E706) (1, 5, 13, 48, 49).2 In order to make this practice at least partially self-contained, a moderate amount of discussion is provided in areas relating to ASTM and other documents. Support subject areas that are discussed include reactor physics calculations, dosimeter selection and analysis, and exposure units.
1.3 This practice is restricted to direct applications related to surveillance programs that are established in support of the operation, licensing, and regulation of LWR nuclear power plants. Procedures and data related to the analysis, interpretation, and application of test reactor results are addressed in Practice E1006, Guide E900, and Practice E1035.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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