ASTM E1728-16
(Practice)Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead Determination
Standard Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead Determination
SIGNIFICANCE AND USE
5.1 This practice is intended for the collection of settled dust samples in and around buildings and related structures for the subsequent determination of lead content in a manner consistent with that described in the HUD Guidelines5 and 40 CFR 745.63. The practice is meant for use in the collection of settled dust samples that are of interest in clearance, hazard assessment, risk assessment, and other purposes.
5.2 Use of different pressures applied to the sampled surface along with the use of different wiping patterns contribute to collection variability. Thus, the sampling result can vary between operators performing collection from identical surfaces as a result of collection variables. Collection for any group of sampling locations at a given sampling site is best when limited to a single operator.
5.3 This practice is recommended for the collection of settled dust samples from hard, relatively smooth, nonporous surfaces. This practice is less effective for collecting settled dust samples from surfaces with substantial texture such as rough concrete, brickwork, textured ceilings, and soft fibrous surfaces such as upholstery and carpeting.
SCOPE
1.1 This practice covers the collection of settled lead-containing dust on surfaces using the wipe sampling method. These samples are collected in a manner that will permit subsequent extraction and determination of lead using laboratory analysis techniques such as atomic spectrometry or electroanalysis. For collection of settled dust samples for determination of lead and other metals, use Practice D6966.
1.2 This practice does not address the sampling design criteria (that is, sampling plan which includes the number and location of samples) that are used for clearance, lead hazard evaluation, risk assessment, and other purposes. To provide for valid conclusions, sufficient numbers of samples should be obtained as directed by a sampling plan.
1.3 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: E1728 − 16
Standard Practice for
Collection of Settled Dust Samples Using Wipe Sampling
1
Methods for Subsequent Lead Determination
This standard is issued under the fixed designation E1728; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Induc-
1.1 This practice covers the collection of settled lead-
tively Coupled Plasma Atomic Emission Spectrometry
containing dust on surfaces using the wipe sampling method.
(ICP-AES), Flame Atomic Absorption Spectrometry
These samples are collected in a manner that will permit
(FAAS), or Graphite Furnace Atomic Absorption Spec-
subsequent extraction and determination of lead using labora-
trometry (GFAAS) Techniques
tory analysis techniques such as atomic spectrometry or
E1644 Practice for Hot Plate Digestion of Dust Wipe
electroanalysis. For collection of settled dust samples for
Samples for the Determination of Lead
determination of lead and other metals, use Practice D6966.
E1792 Specification for Wipe Sampling Materials for Lead
1.2 This practice does not address the sampling design
in Surface Dust
criteria (that is, sampling plan which includes the number and
E1979 Practice for Ultrasonic Extraction of Paint, Dust,
location of samples) that are used for clearance, lead hazard
Soil, and Air Samples for Subsequent Determination of
evaluation, risk assessment, and other purposes.To provide for
Lead
valid conclusions, sufficient numbers of samples should be
E2051 Practice for the Determination of Lead in Paint,
obtained as directed by a sampling plan.
Settled Dust, Soil and Air Particulate by Field-Portable
3
Electroanalysis (Withdrawn 2010)
1.3 This practice contains notes that are explanatory and are
4
not part of the mandatory requirements of this practice.
2.2 Federal Regulations:
40 CFR 745.63 U.S. Environmental ProtectionAgency Fed-
1.4 The values stated in SI units are to be regarded as
eral Register, Vol 66, No. 4, 5 Jan. 2001, p. 1206
standard. No other units of measurement are included in this
standard.
3. Terminology
1.5 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 3.1 For definitions of terms not listed here, seeTerminology
responsibility of the user of this standard to establish appro- E1605.
priate safety and health practices and determine the applica-
3.2 Definitions:
bility of regulatory limitations prior to use.
3.2.1 batch, n—a group of field or quality control (QC)
samples that are collected or processed together at the same
2. Referenced Documents
time using the same reagents and equipment.
2
2.1 ASTM Standards:
3.2.2 sampling location, n—a specific area within a sam-
D4840 Guide for Sample Chain-of-Custody Procedures
pling site that is subjected to sample collection.
D6966 Practice for Collection of Settled Dust Samples
3.2.2.1 Discussion—Multiple sampling locations are com-
Using Wipe Sampling Methods for Subsequent Determi-
monly designated for a single sampling site (see 3.2.3).
nation of Metals
3.2.3 sampling site, n—a local geographic area that contains
the sampling locations (see 3.2.2).
3.2.3.1 Discussion—A sampling site is generally limited to
1
This practice is under the jurisdiction ofASTM Committee D22 on Air Quality
an area that is easily covered by walking.
and is the direct responsibility of Subcommittee D22.12 on Sampling andAnalysis,
of Lead, for Exposure and Risk Assessment.
Current edition approved Jan. 1, 2016. Published February 2016. Originally
approved in 1994. Last previous edition approved in 2010 as E1728-10. DOI:
3
10.1520/E1728-16. The last approved version of this historical standard is referenced on
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or www.astm.org.
4
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM AvailablefromUnitedStatesEnvironmentalProtectionAgency(EPA),William
Standards volume information, refer to the standard’s Document Summary page on Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
the ASTM website. http://www.epa.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
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E1728 − 16
NOTE 1—For most surfaces, it is recommended to collect settled dust
3.2.4 wipe,n—adisposabletowellettethatismoistenedwith
2
from a minimum of a 100 cm area to provide sufficient material for
a wetting agent. E1792
6
laboratory analysis. How
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1728 − 10 E1728 − 16
Standard Practice for
Collection of Settled Dust Samples Using Wipe Sampling
1
Methods for Subsequent Lead Determination
This standard is issued under the fixed designation E1728; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers the collection of settled lead-containing dust on surfaces using the wipe sampling method. These
samples are collected in a manner that will permit subsequent extraction and determination of lead using laboratory analysis
techniques such as atomic spectrometry or electroanalysis. For collection of settled dust samples for determination of lead and
other metals, use Practice D6966.
1.2 This practice does not address the sampling design criteria (that is, sampling plan which includes the number and location
of samples) that are used for clearance, lead hazard evaluation, risk assessment, and other purposes. To provide for valid
conclusions, sufficient numbers of samples should be obtained as directed by a sampling plan.
1.3 This practice contains notes that are explanatory and are not part of the mandatory requirements of this practice.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D4840 Guide for Sample Chain-of-Custody Procedures
D6966 Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
E1644 Practice for Hot Plate Digestion of Dust Wipe Samples for the Determination of Lead
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
E1979 Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead
E2051 Practice for the Determination of Lead in Paint, Settled Dust, Soil and Air Particulate by Field-Portable Electroanalysis
3
(Withdrawn 2010)
4
2.2 Federal Regulations:
40 CFR 745.63 U.S. Environmental Protection Agency Federal Register, Vol 66, No. 4, 5 Jan. 2001, p. 1206
3. Terminology
3.1 For definitions of terms not listed here, see Terminology E1605.
3.2 Definitions:
1
This practice is under the jurisdiction of ASTM Committee E06 on Performance of Buildings and is the direct responsibility of Subcommittee E06.23 on Lead Hazards
Associated with Buildings.
Current edition approved Oct. 1, 2010Jan. 1, 2016. Published November 2010February 2016. Originally approved in 1994. Last previous edition approved in 20032010
as E1728 – 03.E1728-10. DOI: 10.1520/E1728-10.10.1520/E1728-16.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
4
Available from United States Environmental Protection Agency (EPA), Ariel Rios William Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
http://www.epa.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E1728 − 16
3.2.1 batch, n—a group of field or quality control (QC) samples that are collected or processed together at the same time using
the same reagents and equipment.
3.2.2 sampling location, n—a specific area within a sampling site that is subjected to sample collection.
3.2.2.1 Discussion—
Multiple sampling locations are commonly designated for a single sampling site (see 3.2.3).
3.2.3 sampling site, n—a local geographic area that contains the sampling locations (see 3.2.2).
3.
...
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