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ASTM D7626-19e1

(Test Method)

Standard Test Methods for Determining the Organic Treat Loading of Organophilic Clay

Standard Test Methods for Determining the Organic Treat Loading of Organophilic Clay

SIGNIFICANCE AND USE
5.1 This standard test method is intended as an index test to determine the organic treat loading of organophilic clay. This standard test method can be used for manufacturing quality control and construction quality assurance material evaluation.  
5.2 The percent organic treat loading of organophilic clay is a relative indicator of its adsorptive capacity. Organophilic clay is used for remediation of contaminated sediment, soil, and groundwater.  
5.3 The two test methods denote different devices, a muffle furnace and a thermal gravimetric analyzer. The thermal gravimetric analyzer may be programmed to reach a higher temperature than the muffle furnace, but the organic matter will be burnt off at 750 °C.
Note 3: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This standard covers two index test methods that can be used in the evaluation of the amount of organic compound chemically bonded to the base clay portion of a representative sample of organophilic clay.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
Note 1: This standard is presented using SI units. Use of units other than SI is allowed. However, if other units are used, the performance of a units conversion check of the calculations should be included as a part of the calculations.  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.3.1 Two test methods are provided in this standard. The methods differ in equipment, the size of the specimen (mass) required and the significant digits reported.  
1.3.2 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of the reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Jan-2019
ICS
91.100.15 - Mineral materials and products
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.21 - Groundwater and Vadose Zone Investigations
Current Stage
Ref Project

Relations

Replaces
ASTM D7626-19 - Standard Test Methods for Determining the Organic Treat Loading of Organophilic Clay
Effective Date
01-Feb-2019
Refers
ASTM D4753-15 - Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
Effective Date
01-May-2015
Refers
ASTM D3740-19 - Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
Effective Date
01-Oct-2019
Refers
ASTM D653-14 - Standard Terminology Relating to Soil, Rock, and Contained Fluids
Effective Date
01-Aug-2014
Refers
ASTM E145-19 - Standard Specification for Gravity-Convection and Forced-Ventilation Ovens
Effective Date
01-Mar-2019

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ASTM D7626-19e1 - Standard Test Methods for Determining the Organic Treat Loading of Organophilic ClayASTM D7626-19e1 - Standard Test Methods for Determining the Organic Treat Loading of Organophilic Clay
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ASTM D7626-19e1 - Standard Test Methods for Determining the Organic Treat Loading of Organophilic Clay
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
´1
Designation: D7626 − 19
Standard Test Methods for
Determining the Organic Treat Loading of Organophilic
1
Clay
This standard is issued under the fixed designation D7626; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Corrected data sheet editorially in Appendix X1 in February 2020.
1. Scope priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 This standard covers two index test methods that can be
1.5 This international standard was developed in accor-
used in the evaluation of the amount of organic compound
dance with internationally recognized principles on standard-
chemically bonded to the base clay portion of a representative
ization established in the Decision on Principles for the
sample of organophilic clay.
Development of International Standards, Guides and Recom-
1.2 The values stated in SI units are to be regarded as the
mendations issued by the World Trade Organization Technical
standard. No other units of measurement are included in this
Barriers to Trade (TBT) Committee.
standard. Reporting of test results in units other than SI shall
not be regarded as nonconformance with this standard.
2. Referenced Documents
2
NOTE 1—This standard is presented using SI units. Use of units other
2.1 ASTM Standards:
than SI is allowed. However, if other units are used, the performance of a
D653 Terminology Relating to Soil, Rock, and Contained
units conversion check of the calculations should be included as a part of
Fluids
the calculations.
D3740 Practice for Minimum Requirements for Agencies
1.3 All observed and calculated values shall conform to the
Engaged in Testing and/or Inspection of Soil and Rock as
guidelines for significant digits and rounding established in
Used in Engineering Design and Construction
Practice D6026.
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
1.3.1 Two test methods are provided in this standard. The
ances and Standard Masses for Use in Soil, Rock, and
methods differ in equipment, the size of the specimen (mass)
Construction Materials Testing
required and the significant digits reported.
D6026 Practice for Using Significant Digits in Geotechnical
1.3.2 Theproceduresusedtospecifyhowdataarecollected/
Data
recorded or calculated in this standard are regarded as the
E11 Specification for Woven Wire Test Sieve Cloth and Test
industry standard. In addition, they are representative of the
Sieves
significant digits that generally should be retained. The proce-
E145 Specification for Gravity-Convection and Forced-
dures used do not consider material variation, purpose for
Ventilation Ovens
obtaining the data, special purpose studies, or any consider-
ations for the user’s objectives; and it is common practice to
3. Terminology
increase or reduce significant digits of the reported data to be
3.1 Definitions—For definitions of common technical terms
commensuratewiththeseconsiderations.Itisbeyondthescope
of this standard to consider significant digits used in analysis in this standard, refer to Terminology D653.
methods for engineering design.
3.2 Definitions of Terms Specific to This Standard:
1.4 This standard does not purport to address all of the
3.2.1 base clay, n—an untreated naturally occurring clay
safety concerns, if any, associated with its use. It is the (for example, bentonite, kaolinite).
responsibility of the user of this standard to establish appro-
3.2.2 initial mass loss, n—the amount of water and residual
organic compound not bound to the base clay.
1
These test methods are under the jurisdiction ofASTM Committee D18 on Soil
andRockandarethedirectresponsibilityofSubcommitteeD18.21onGroundwater
2
and Vadose Zone Investigations. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Feb. 1, 2019. Published February 2019. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2010. Last previous edition approved in 2018 as D7626–10(2018). Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/D7626-19E01. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
´1
D7626 − 19
3.2.3 organic treat loading, n—the amount of organic com- 6.2 Muffle Furnace, capable of producing
...

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4.1 Riprap is a commonly used form of scour protection and general slope protection. Riprap provides a long term solution when properly sized and installed. Riprap has structural flexibility so it will conform to irregular surfaces and adapt to minor subgrade settlement. It is often appropriate for use in conjunction with soil bioengineering (vegetation establishment) alternatives. In some environments, riprap may provide habitat for benthic organisms and fish.  
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1.1 This guide covers methods to place riprap with associated filters for erosion control purposes. This guide does not recommend a specific course of action because of the diverse methods and procedures that are capable of producing a functional product. This guide identifies favorable riprap qualities and recommends practices best suited to obtain those qualities. The production of rock, use of recycled materials, rock with cut dimensions, and engineering and revetment design are beyond the scope of this guide. Special forms of riprap, including hand placed riprap, grouted riprap, or keyed (plated) riprap that is tamped into place to smooth the surface, are also beyond the scope of this guide.  
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SIGNIFICANCE AND USE
5.1 Rock for erosion control consists of individual pieces of natural quarried stone or large boulders and cobbles. The ability of these individual pieces of stone to resist deterioration due to weathering action affects the stability of the integral placement of rock for erosion control and hence, the stability of construction projects, structures, shorelines, and stream banks.  
5.2 Deterioration of stone in this test is one indicator that similar samples exposed to wet/dry and freeze/thaw cycles may break down in a water-soaked environment condition in service.  
5.3 This test method was developed to be used in conjunction with additional test methods listed in Practice D4992. This test method provides a quantitative value indicating potential resistance to weathering; however, the results of this test method are not to be used as the sole basis for the determination of rock durability.
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1.1 This test method covers the testing for and quantitative determination of the presence of swelling clays of the smectite group in rock for erosion control. The test particles are intended to be representative of erosion control rock and its durability. The test is appropriate for breakwater stone, armor stone, riprap and gabion sized rock materials.  
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SIGNIFICANCE AND USE
5.1 Rock for erosion control consists of individual pieces of natural stone. The ability of these individual pieces of stone to resist deterioration due to weathering action affects the stability of the integral placement of rock for erosion control and hence, the stability of construction projects, structures, shorelines, and stream banks.  
5.2 The sodium sulfate or magnesium sulfate soundness test is one method by which to estimate qualitatively the durability of rock under weathering conditions. This test method was developed to be used in conjunction with additional test methods listed in Practice D4992. This test method does not provide an absolute value, but rather an indication of the resistance to freezing and thawing; therefore, the results of this test method are not to be used as the sole basis for the determination of rock durability.  
5.3 This test method has been used to evaluate many different types of rocks. There have been occasions when test results have provided data that have not agreed with the durability of rock under actual field conditions; samples yielding a low soundness loss have disintegrated in actual usage, and the reverse has been true.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing it and suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors and Practice D3740 provides a means of evaluating some of them.
SCOPE
1.1 This test method covers test procedures for evaluating the soundness of rock for erosion control by the effects of a sodium or magnesium sulfate solution on slabs of rock. It is an accelerated weathering test. The rock slabs, prepared in accordance with procedures in Practice D5121, are intended to be representative of erosion control sized materials and their inherent weaknesses. The test is appropriate for breakwater stone, armor stone, riprap and gabion sized rock materials.  
1.1.1 The limitations of this test are twofold. First the test is a simulation of freezing and thawing conditions using accelerated life cycling techniques. The test evaluates the internal expansive force derived from the rehydration of the salt upon re-immersion, an event that may not occur in some natural environments, to simulate the expansion of water rather than the actual freezing of water. Secondly, the size of the cut rock slab specimens may eliminate some of the internal defects present in the rock structure. The test specimens may not be representative of the quality of the larger rock samples used in construction. Careful examination of the rock source and proper sampling are essential in minimizing this limitation.  
1.2 The use of reclaimed concrete and other materials for erosion control is beyond the scope of this test method.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.3.1 The gravitational system of inch-pound units is used when dealing with inch-pound units. In this system, the pound (lbf) represents a unit of force (weight), while the unit for mass is slugs. The slug unit is not given unless dynamic (F=ma) calculations are involved.  
1.3.2 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practi...

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ASTM
ASTM D6910/D6910M-19(Test Method)
Standard Test Method for Marsh Funnel Viscosity of Construction Slurries

SIGNIFICANCE AND USE
5.1 Viscosity is a fundamental characteristic for slurries in construction applications. The Marsh Funnel Viscosity test can be used for field quality control of slurries. Relative changes in slurry viscosity can be identified using Marsh Funnel measurements and modifications can be made to mixing and handling procedures.
Note 1: The development of the Marsh Funnel is credited to Hallan N. Marsh of Los Angeles who published the design and use of his funnel viscometer in 1931.  
5.2 This test method allows for the assessment of the apparent viscosity of construction slurries in the laboratory and in the field. The Marsh Funnel Viscosity is not a true viscosity, it is an index value and can only be used to assess the relative viscosity of the slurry to water. Higher MFV values are obtained for slurries with higher viscosity and lower MFV values are obtained for slurries with lower viscosity.  
5.3 In this test, it is assumed that the apparent viscosity of a slurry is directly related to the flow duration through a specially shaped funnel (the Marsh Funnel).  
5.4 In slurry construction applications, the viscosity of a slurry must be maintained within a predetermined range to stabilize the surrounding soil being supported.  
5.5 The Marsh Funnel Viscosity has been widely used in drilling soil and rock for water wells and oil, gas, soil stabilization, foundation drilling, and hydraulic barrier applications.  
5.6 Inert suspended solids (such as fine sands, clays, and cement) and additives affect the viscosity of slurries. This test may be used to determine the relative effects of these and other such materials on the viscosity of a slurry.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling/inspection/etc. Us...
SCOPE
1.1 This test method provides an indirect measurement of the viscosity of construction slurries using a funnel (Marsh Funnel) and a graduated cup with specific volume marks. This test method provides an indicator of the viscosity on a routine basis. This test method has been modified from the API Recommended Practice 13B-1.  
1.2 The result determined using the method is referred to as the Marsh Funnel Viscosity. The Marsh Funnel Viscosity is an index property and is not an actual measurement of viscosity.  
1.3 This test can be performed in the laboratory or in the field to assess the Marsh Funnel Viscosity of a slurry for quality control purposes.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D4221-18(Test Method)
Standard Test Method for Dispersive Characteristics of Clay Soil by Double Hydrometer

SIGNIFICANCE AND USE
5.1 Dispersive clays are those which normally deflocculate when exposed to water of low-salt concentration, the opposite of aggregated clays that would remain flocculated in the same soil-water system  (3, 4, 7). Generally, dispersive clays are highly erosive, possibly subject to high shrink-swell potential, may have lower shear strength, and have lower permeability rates than aggregated clays.  
5.2 When the percent dispersion equals 100, it indicates a completely dispersive clay-size fraction. When the percent dispersion equals 0, it indicates completely nondispersive clay-size fraction.  
5.3 Available data (1) indicates that the test method has about 85 % reliance in predicting dispersive performance (85 % of dispersive clays show more than 35 % dispersion).  
5.4 Since this test method may not identify all dispersive clays, design decisions based solely on this test method may not be conservative. It is often run in conjunction with the crumb test (D6572) (4, 7), the pinhole test (D4647/D4647M), or the analysis of the pore water extract (D4542) (4, 7), or combination thereof, to identify possible dispersive clay behavior.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personal performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depends on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method provides an indication of the natural dispersive characteristics of clay soils by comparing the amount of particles finer than 2-μm as determined by this method compared to the amount of particles finer than 2-μm as determined by Test Method D7928 (1).2 In order to do this comparison, two similar specimens must be obtained from the sample.  
1.2 This test method follows the procedure given in Test Method D7928 with the exception that the soil slurry is not mechanically dispersed and no dispersing agent is added.  
1.3 This test method is applicable only to soils where the position of the plasticity index versus liquid limit plots (Test Methods D4318) falls on or above the “A” line (Practice D2487) and more than 12 % of the soil fraction is finer than 2-μm as determined in accordance with Test Method D7928 (2).  
1.4 Since this test method may not identify all dispersive clay soils, other tests such as, pinhole dispersion (Test Methods D4647/D4647M), crumb (Test Methods D6572) (3-5) and the analysis of pore water extraction (Test Methods D4542) (4-7) may be performed individually or used together to help verify dispersion.  
1.5 Units—The values stated in SI units are to be regarded as the standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method.  
1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use...

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