ASTM D5363-03(2008)

Standard Specification for Anaerobic Single-Component Adhesives (AN)

ABSTRACT
This specification establishes the requirements for single-component anaerobic adhesives suitable for locking, sealing, and retaining threaded or cylindrical assemblies. It is intended to be a means of classifying the adhesives, and does not address engineering design purposes. The adhesives are cured to a solid state when confined between closely fitting active metal surfaces. Materials shall undergo test procedures and conform accordingly to the following requirements: ultraviolet fluorescence; color and workmanship; flash point; storage stability; toxicity; solvent resistance; hot strength; heat aging; cold strength; lubricity; fluid tightness; wicking; viscosity; speed of cure; prevailing torque strength (strength at standard conditions); and qualification of primers.
SCOPE
1.1 This specification covers single-component anaerobic adhesives suitable for locking, sealing, and retaining threaded or cylindrical assemblies. The adhesives are cured to a solid state when confined between closely fitting active metal surfaces.
1.2 This specification is intended to be a means of classifying anaerobic adhesives. It is not intended for engineering design purposes.
1.3 This specification is intended to replace Military Specifications MIL-S-22473, MIL-S-46163, and MIL-R-46082.
1.4 The values stated in SI units are to be regarded as the standard.
1.5 The following safety hazards caveat pertains only to the test methods portion, Section 7, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

• Status: Historical
• Publication Date: 30-Sep-2008
• ICS: 83.180 - Adhesives
• Technical Committee: D14 - Adhesives
• Drafting Committee: D14.60 - Adhesive Material Classification System

Relations

• Replaces: ASTM D5363-03e1 - Standard Specification for Anaerobic Single-Component Adhesives (AN)
• Effective Date: 01-Oct-2008
• Referred By: ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
• Effective Date: 01-Oct-2008
• Referred By: ASTM D4054-23 - Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives
• Effective Date: 01-Oct-2008
• Referred By: ASTM D4800-94(2023) - Standard Guide for Classifying and Specifying Adhesives
• Effective Date: 01-Oct-2008

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5363 −03(Reapproved 2008)
Standard Specification for
1
Anaerobic Single-Component Adhesives (AN)
This standard is issued under the fixed designation D5363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope D56Test Method for Flash Point by Tag Closed Cup Tester
D439Specification for Automotive Gasoline (Withdrawn
1.1 This specification covers single-component anaerobic
3
1990)
adhesives suitable for locking, sealing, and retaining threaded
D445Test Method for Kinematic Viscosity of Transparent
or cylindrical assemblies. The adhesives are cured to a solid
and Opaque Liquids (and Calculation of DynamicViscos-
state when confined between closely fitting active metal
ity)
surfaces.
D770Specification for Isopropyl Alcohol
1.2 This specification is intended to be a means of classify-
D907Terminology of Adhesives
ing anaerobic adhesives. It is not intended for engineering
D1084Test Methods for Viscosity of Adhesives
design purposes.
D1193Specification for Reagent Water
1.3 This specification is intended to replace Military Speci-
D2693Specification for Ethylene Glycol
fications MIL-S-22473, MIL-S-46163, and MIL-R-46082.
D3951Practice for Commercial Packaging
D4562Test Method for Shear Strength of Adhesives Using
1.4 The values stated in SI units are to be regarded as the
Pin-and-Collar Specimen
standard.
D4800Guide for Classifying and Specifying Adhesives
1.5 The following safety hazards caveat pertains only to the
D5648Test Method for Torque-Tension Relationship of
test methods portion, Section 7, of this specification.This
Adhesives Used on Threaded Fasteners (Lubricity)
standard does not purport to address all of the safety concerns,
D5649Test Method for Torque Strength ofAdhesives Used
if any, associated with its use. It is the responsibility of the user
on Threaded Fasteners
of this standard to establish appropriate safety and health
D5657TestMethodforFluidTightnessAbilityofAdhesives
practices and determine the applicability of regulatory limita-
Used on Threaded Fasteners
tions prior to use.
E122PracticeforCalculatingSampleSizetoEstimate,With
2. Referenced Documents Specified Precision, the Average for a Characteristic of a
2
Lot or Process
2.1 ASTM Standards:
A109/A109MSpecification for Steel, Strip, Carbon (0.25
2.2 Military Standards:
Maximum Percent), Cold-Rolled MIL-STD-105Sampling Procedures and Tables for Inspec-
4
B36/B36MSpecification for Brass Plate, Sheet, Strip, And
tion by Attributes
4
Rolled Bar
MIL-STD-129Marking for Shipment and Storage
B209Specification for Aluminum and Aluminum-Alloy
MIL-STD-810Environmental Test Methods and Engineer-
4
Sheet and Plate
ing Guides
B633SpecificationforElectrodepositedCoatingsofZincon
MIL-STD-118 Commercial Packaging of Supplies and
4
Iron and Steel
Equipment
2.3 Federal Standards:
FED-STD-313Material Safety Data Sheets, Preparation and
1
This specification is under the jurisdiction of ASTM Committee D14 on
4
Submission of
Adhesives and is the direct responsibility of Subcommittee D14.60 on Adhesive
Material Classification System.
Current edition approved Oct. 1, 2008. Published October 2008. Originally
ε1
approved in 1993. Last previous edition approved in 2003 as D5363–03 . DOI:
3
10.1520/D5363-03R08. The last approved version of this historical standard is referenced on
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or www.astm.org.
4
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Standards volume information, refer to the standard’s Document Summary page on Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
the ASTM website. www.dodssp.daps.mil.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5363−03 (2008)
2.4 Federal Specifications: 3.2.2 prevailing torque, n—the torque measured at 180°
FF-N-836 Nut: Square, Hexagon, Cap, Slotted, Castle, rotation of the nut.
4
Knurled, Welding and Single Ball Seat
3.2.2.1 Discussion—Prevailing torque was originally de-
4
PPP-B-636Box, Shipping, Fiberboard
fined in MIL-S-46163 and MIL-S-22473 as the average of the
4
QQ-P-416Plating, Cadmium, Electrodeposited
fourtorquesmeasuredat90,180,270,and360°rotationofthe
2.5 Military Specifications:
nut. Studies have shown that the torque measured at 180°
MIL-R-46082Retaining Compounds, Single-Component,
rotation of the nut is stat
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D5363–97 Designation: D 5363 – 03 (Reapproved 2008)
Standard Specification for
1
Anaerobic Single-Component Adhesives (AN)
This standard is issued under the fixed designation D5363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1 This specification covers single-component anaerobic adhesives suitable for locking, sealing, and retaining threaded or
cylindrical assemblies. The adhesives are cured to a solid state when confined between closely fitting active metal surfaces.
1.2 This specification is intended to be a means of classifying anaerobic adhesives. It is not intended for engineering design
purposes.
1.3 This specification is intended to replace Military Specifications MIL-S-22473, MIL-S-46163, and MIL-R-46082.
1.4 The values stated in SI units are to be regarded as the standard.
1.5 Thefollowingsafetyhazardscaveatpertainsonlytothetestmethodsportion,Section7,ofthisspecification. This standard
does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this
standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
A109Specification for Steel, Strip, Carbon, Cold-Rolled 109/A109M Specification for Steel, Strip, Carbon (0.25 Maximum
Percent), Cold-Rolled
B36/B36M Specification for Brass Plate, Sheet, Strip, andAnd Rolled Bar
B209 Specification for Aluminum and Aluminum-Alloy Sheet and Plate
B633 Specification for Electrodeposited Coatings of Zinc on Iron and Steel
D56 Test Method for Flash Point by Tag Closed Cup Tester
3
D439Specification for Automotive Gasoline Specification for Automotive Gasoline
D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
D770 Specification for Isopropyl Alcohol
D907 Terminology of Adhesives
D1084 Test Methods for Viscosity of Adhesives
D1193 Specification for Reagent Water
D2693 Specification for Ethylene Glycol
D3951 Practice for Commercial Packaging
D4562 Test Method for Shear Strength of Adhesives Using Pin-and-Collar Specimen
D4800 Guide for Classifying and Specifying Adhesives
D5648 Test Method for Torque-Tension Relationship of Adhesives Used on Threaded Fasteners (Lubricity)
D5649 Test Method for Torque Strength of Adhesives Used on Threaded Fasteners
D5657 Test Method for Fluid Tightness Ability of Adhesives Used on Threaded Fasteners
E122PracticeforChoiceofSampleSizetoEstimateaMeasureofQualityforaLotorProcess PracticeforCalculatingSample
Size to Estimate, With Specified Precision, the Average for a Characteristic of a Lot or Process
2.2 Military Standards:
1
This specification is under the jurisdiction of ASTM Committee D-14 on Adhesives and is the direct responsibility of Subcommittee D14.60 on Adhesive Material
Classification System.
Current edition approved Nov. 10, 1997. Published March 1998. Originally published as D 5363–93. Last previous edition D 5363–93.
1
This specification is under the jurisdiction of ASTM Committee D14 on Adhesives and is the direct responsibility of Subcommittee D14.60 on Adhesive Material
Classification System.
´1
Current edition approved Oct. 1, 2008. Published October 2008. Originally approved in 1993. Last previous edition approved in 2003 as D5363–03 .
2
ForreferencedASTMstandards,visittheASTMwebsite,www.astm.org,[e-mail] Annual Book of ASTM Standards
, Vol 01.03.volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Withdrawn.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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D 5363 – 03 (2008)
4
MIL-STD-105 Sampling Procedures and Tables for Inspection by Attributes
4
MIL-STD-129 Marking for Shipment and Storage
4
MIL-STD-810 Environmental Test Methods and Engineering Guides
4
MIL-STD-118 Commercial Packaging of Supplies and Equipment
2.3 Federal Standards:
4
FED-STD-313 Material Safety Data Sheets, Preparation and Submission of
2.4 Federal Specifications:
4
FF-N-836 Nut: Square, Hexagon, Cap, Slotted, Castle, Knurled,
...