ASTM E1560-11
(Test Method)Standard Test Method for Gravimetric Determination of Nonvolatile Residue From Cleanroom Wipers
Standard Test Method for Gravimetric Determination of Nonvolatile Residue From Cleanroom Wipers
SIGNIFICANCE AND USE
The NVR obtained by this test method is that amount which is available for release by wipers in normal use.
Evaporation of the solvent at the stated temperature is to quantify the NVR that can be expected to exist at room temperature, since the slight difference between room temperature and test temperature has not been shown to result in significant variances.
This test method may be more aggressive than necessary for the evaluation of wipers that will be restricted to dry use only.
Numerous other methods are being used to determine NVR. This test method is not intended to replace test methods used for other applications.
SCOPE
1.1 This test method covers the determination of solvent extractable nonvolatile residue (NVR) from wipers used in assembly, cleaning, or testing of spacecraft, but not from those used for analytical surface sampling of hardware.
1.2 The NVR of interest is that which can be extracted from cleanroom wipers using a specified solvent that has been selected for its extractive qualities. Alternative solvents may be selected, but since their use may result in different values being generated, they must be identified in the procedure data sheet.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3.1 Exception—The inch-pound units are included for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:E1560–11
Standard Test Method for
Gravimetric Determination of Nonvolatile Residue From
1
Cleanroom Wipers
This standard is issued under the fixed designation E1560; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Micrometre and Larger Particles
3
2.2 Military Standards:
1.1 This test method covers the determination of solvent
MIL-STD-1916 Acceptance on Zero Sampling Inspection
extractable nonvolatile residue (NVR) from wipers used in
3
2.3 Federal Standards:
assembly, cleaning, or testing of spacecraft, but not from those
Fed. Std. 209E Airborne Particulate Cleanliness Classes in
used for analytical surface sampling of hardware.
4
Cleanrooms and Clean Zones
1.2 The NVR of interest is that which can be extracted from
2.4 Other Documents:
cleanroom wipers using a specified solvent that has been
,
5 6
IEST-RP-CC001 HEPA and ULPA Filters
selectedforitsextractivequalities.Alternativesolventsmaybe
IEST-RP-CC005 Gloves and Finger Cots Used in Clean-
selected,butsincetheirusemayresultindifferentvaluesbeing
4
rooms and Other Controlled Environments
generated, they must be identified in the procedure data sheet.
ISO 14644-1 Cleanrooms and Associated Controlled Envi-
1.3 The values stated in SI units are to be regarded as
7
ronments, Classification of air cleanliness
standard. No other units of measurement are included in this
ISO 14644-2 Cleanrooms and Associated Controlled Envi-
standard.
ronments, Specifications for testing and monitoring to
1.3.1 Exception—The inch-pound units are included for
5
prove continued compliance with ISO 14644-1
information only.
1.4 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 Definitions:
responsibility of the user of this standard to establish appro-
3.1.1 contaminant—unwanted molecular or particulate mat-
priate safety and health practices and determine the applica-
ter that could affect or degrade the performance of the
bility of regulatory limitations prior to use.
components on which they are deposited.
2. Referenced Documents 3.1.2 contamination—a process of contaminant transport or
2
accretion or both.
2.1 ASTM Standards:
3.1.3 environmentally controlled area—cleanrooms, clean
D1193 Specification for Reagent Water
facilities, controlled work areas, and other enclosures that are
E2217 Practice for Design and Construction of Aerospace
designed to protect hardware from contamination. Cleanliness
Cleanrooms and Contamination Controlled Areas
is achieved by controlling airborne particulate matter, tempera-
F24 Test Method for Measuring and Counting Particulate
ture, relative humidity, materials, garments, and personnel
Contamination on Surfaces
activities. Guidelines for controlled areas can be found in
F50 Practice for Continuous Sizing and Counting of Air-
Practice E2217.
borne Particles in Dust-ControlledAreas and Clean Rooms
Using Instruments Capable of Detecting Single Sub-
3
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
1
This test method is under the jurisdiction of ASTM Committee E21 on Space dodssp.daps.dla.mil.
4
Simulation andApplications of Space Technology and is the direct responsibility of Fed-Std-209E has been replaced by ISO 14644-1 and -2, but may continue to
Subcommittee E21.05 on Contamination. be used by mutual agreement.
5
Current edition approved Dec. 1, 2011. Published January 2012. Originally The use of Di Octyl Phthalate (DOP) in leak testing of filters or filter
approved in 1993. Last previous edition approved in 2006 as E1560 – 06. DOI: installation is not acceptable.
6
10.1520/E1560-11. Available from Institute of Environmental Sciences and Technology (IEST),
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Arlington Place One, 2340 S.Arlington Heights Rd., Suite 100,Arlington Heights,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM IL 60005-4516, http://www.iest.org.
7
Standards volume information, refer to the standard’s Document Summary page on Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
the ASTM website. 4th Floor, New York, NY 10036, http://www.ansi.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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E1560–11
3.1.4 high effıciency particulate air (HEPA)—a term de- ISO 14644-2 (Fed-Std-209), latest revision when tested in
scribing filters having
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:E1560–06 Designation:E1560–11
Standard Test Method for
Gravimetric Determination of Nonvolatile Residue From
1
Cleanroom Wipers
This standard is issued under the fixed designation E1560; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of solvent extractable nonvolatile residue (NVR) from wipers used in assembly,
cleaning, or testing of spacecraft, but not from those used for analytical surface sampling of hardware.
1.2The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.
1.3The NVR of interest is that which can be extracted from cleanroom wipers using a specified solvent that has been selected
for its extractive qualities.Alternative solvents may be selected, but since their use may result in different values being generated,
they must be identified in the procedure data sheet.
1.2 The NVR of interest is that which can be extracted from cleanroom wipers using a specified solvent that has been selected
for its extractive qualities.Alternative solvents may be selected, but since their use may result in different values being generated,
they must be identified in the procedure data sheet.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3.1 Exception—The inch-pound units are included for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
E2217 Practice for Design and Construction of Aerospace Cleanrooms and Contamination Controlled Areas
F24 Test Method for Measuring and Counting Particulate Contamination on Surfaces
F50 Practice for Continuous Sizing and Counting of Airborne Particles in Dust-Controlled Areas and Clean Rooms Using
Instruments Capable of Detecting Single Sub-Micrometre and Larger Particles
3
2.2 Military Standards:Air Force T.O. 00-25-203Contamination Control of Aerospace Facilities, U.S. Air Force MIL-F-
3,
51068FFilters, Particulate (High Effıciency, Fire Resistant)
MIL-STD-1916 Acceptance on Zero Sampling Inspection
2.3 Federal Standards:
3
Fed Spec. O-E-00760Ethyl Alcohol, Reagent Grade
3 3
Fed Spec. O-T-620 1,1,1-Trichloroethane, Technical, Inhibited (Methyl Chloroform) Federal Standards:
4
Fed. Std. 209E Airborne Particulate Cleanliness Classes forin Cleanrooms and Clean Zones,
2.4 Other Documents:
,
5 6
IEST-RP-CC001 HEPA and ULPA Filters
4
IEST-RP-CC005 Gloves and Finger Cots Used in Cleanrooms and Other Controlled Environments
1
This specification test method is under the jurisdiction of ASTM Committee E21 on Space Simulation and Applications of Space Technology and is the direct
responsibility of Subcommittee E21.05 on Contamination.
Current edition approved Nov. 1, 2006. Published December 2006. Originally approved in 1993. Last previous edition approved in 2001 as E1560–95 (2001). DOI:
10.1520/E1560-06.
Current edition approved Dec. 1, 2011. Published January 2012. Originally approved in 1993. Last previous edition approved in 2006 as E1560 – 06. DOI:
10.1520/E1560-11.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4, Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, Attn: NPODS.http://
dodssp.daps.dla.mil.
4
The use of Di Octyl Phthalate (DOP) in leak testing of filters or filter installation is not acceptable.
4
Fed-Std-209E has been replaced by ISO 14644-1 and -2, but may continue to be used by mutual agreement.
5
Fed-Std-209E has been replaced by ISO/DIS 14644-1 and -2, but may continue to be used by mutual agreement.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
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