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ASTM D3699-01

(Specification)

Standard Specification for Kerosine

Standard Specification for Kerosine

SCOPE
1.1 This specification covers two grades of kerosine suitable for use in critical kerosine burner applications:  
1.1.1 No. 1-K -A special low-sulfur grade kerosine suitable for use in nonflue-connected kerosine burner appliances and for use in wick-fed illuminating lamps.  
1.1.2 No. 2-K -A regular grade kerosine suitable for use in flue-connected burner appliances and for use in wick-fed illuminating lamps.  
1.2 This specification is intended for use in purchasing, as a reference for industry and governmental standardization, and as a source of technical information.  
1.3 This specification, unless otherwise provided by agreement between the purchaser and the supplier, prescribes the required properties of kerosine at the time and place of custody transfer.  
1.4 Nothing in this specification shall preclude observance of federal, state, or local regulations which can be more restrictive.
1.5 All values are stated in SI units and are regarded as the standard.  Note 1-The generation and dissipation of static electricity can create problems in the handling of kerosines. For more information on the subject, see Guide D4865.

General Information

Status
Historical
Publication Date
09-Jun-2001
ICS
75.160.20 - Liquid fuels
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.E0 - Burner, Diesel and Non-Aviation Gas Turbine Fuels
Current Stage
Ref Project

Relations

Replaces
ASTM D3699-98 - Standard Specification for Kerosine
Effective Date
10-Jun-2001
Replaced By
ASTM D3699-02 - Standard Specification for Kerosine
Effective Date
10-Aug-2002
Referred By
ASTM D6136/D6136M-15(2021) - Standard Test Method for Kerosine Number of Unsaturated (Dry) Felt by Vacuum Method
Effective Date
10-Jun-2001
Referred By
ASTM D8166-22 - Standard Test Method for Sizing and Counting Particulates in Middle Distillate Fuels and Biodiesel Blend (B6 to B20) Using Continuous Flow and Bottle Sampler Particle Contamination Monitors
Effective Date
10-Jun-2001
Referred By
ASTM D187-18 - Standard Test Method for Burning Quality of Kerosene
Effective Date
10-Jun-2001
Referred By
ASTM D7058-19 - Standard Test Method for Determination of the Red Dye Concentration and Estimation of Saybolt Color of Aviation Turbine Fuels and Kerosine Using a Portable Visible Spectrophotometer
Effective Date
10-Jun-2001
Referred By
ASTM D3320/D3320M-18 - Standard Specification for Emulsified Coal-Tar Pitch (Mineral Colloid Type)
Effective Date
10-Jun-2001
Referred By
ASTM D6258-17 - Standard Test Method for Determination of Solvent Red 164 Dye Concentration in Diesel Fuels
Effective Date
10-Jun-2001
Referred By
ASTM D6217-21 - Standard Test Method for Particulate Contamination in Middle Distillate Fuels by Laboratory Filtration<rangeref></rangeref >
Effective Date
10-Jun-2001
Referred By
ASTM D6468-22 - Standard Test Method for High Temperature Stability of Middle Distillate Fuels
Effective Date
10-Jun-2001
Referred By
ASTM C474-15(2020) - Standard Test Methods for Joint Treatment Materials for Gypsum Board Construction
Effective Date
10-Jun-2001
Referred By
ASTM E1259-23 - Standard Practice for Evaluation of Antimicrobials in Liquid Fuels Boiling Below 390 °C
Effective Date
10-Jun-2001
Referred By
ASTM D2709-22 - Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
Effective Date
10-Jun-2001
Referred By
ASTM F852/F852M-22 - Standard Specification for Portable Gasoline, Kerosene, and Diesel Containers for Consumer Use
Effective Date
10-Jun-2001
Referred By
ASTM D6756-17 - Standard Test Method for Determination of the Red Dye Concentration and Estimation of the ASTM Color of Diesel Fuel and Heating Oil Using a Portable Visible Spectrophotometer
Effective Date
10-Jun-2001

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ASTM D3699-01 - Standard Specification for Kerosine
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 3699 – 01 An American National Standard
Standard Specification for
1
Kerosine
This standard is issued under the fixed designation D 3699; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope D 1266 Test Method for Sulfur in Petroleum Products
2
(Lamp Method)
1.1 This specification covers two grades of kerosine suitable
2
D 2386 Test Method for Freezing Point of Aviation Fuels
for use in critical kerosine burner applications:
D 2622 Test Method for Sulfur in Petroleum Products by
1.1.1 No. 1-K—A special low-sulfur grade kerosine suitable
3
X-Ray Spectrometry
for use in nonflue-connected kerosine burner appliances and
D 3227 Test Method for Mercaptan Sulfur in Gasoline,
for use in wick-fed illuminating lamps.
Kerosine, Aviation Turbine, and Distillate Fuels (Potentio-
1.1.2 No. 2-K—A regular grade kerosine suitable for use in
3
metric Method)
flue-connected burner appliances and for use in wick-fed
D 3828 Test Methods for Flash Point by Small Scale Closed
illuminating lamps.
3
Tester
1.2 This specification is intended for use in purchasing, as a
D 4294 Test Method for Sulfur in Petroleum Products by
reference for industry and governmental standardization, and
3
Energy Dispersive X-Ray Fluorescence Spectrometry
as a source of technical information.
D 4865 Guide for Generation and Dissipation of Static
1.3 This specification, unless otherwise provided by agree-
3
Electricity in Petroleum Fuel Systems
ment between the purchaser and the supplier, prescribes the
D 4952 Test Method for Qualitative Analysis for Active
required properties of kerosine at the time and place of custody
4
Sulfur Species in Fuels and Solvents (Doctor Test)
transfer.
D 5901 Test Method for Freezing Point of Aviation Fuels
1.4 Nothing in this specification shall preclude observance
4
(Automatic Optical Method)
of federal, state, or local regulations which can be more
D 5972 Test Method for Freezing Point of Aviation Fuels
restrictive.
5
(Automatic Phase Transition Method)
1.5 All values are stated in SI units and are regarded as the
D 6469 Guide for Microbial Contamination in Fuels and
standard.
5
Fuel Systems
NOTE 1—The generation and dissipation of static electricity can create
2.2 IP Standard:
problems in the handling of kerosines. For more information on the
6
IP 10 Burning Test—24 Hour
subject, see Guide D 4865.
3. General Requirements
2. Referenced Documents
3.1 Kerosine shall be a refined petroleum distillate consist-
2.1 ASTM Standards:
ing of a homogeneous mixture of hydrocarbons essentially free
2
D 56 Test Method for Flash Point by Tag Closed Tester
of water, inorganic acidic or basic compounds, and excessive
2
D 86 Test Method for Distillation of Petroleum Products
amounts of particulate contaminants. Additive usage can be
D 130 Test Method for Detection of Copper Corrosion from
established by mutual agreement of the supplier and the
2
Petroleum Products by the Copper Strip Tarnish Test
purchaser.
D 156 Test Method for Saybolt Color of Petroleum Prod-
2
ucts (Saybolt Chromometer Method)
4. Detailed Requirements
2
D 187 Test Method for Burning Quality of Kerosine
4.1 The kerosine shall conform to the detailed requirements
D 445 Test Method for Kinematic Viscosity of Transparent
prescribed in Table 1.
and Opaque Liquids (and the Calculation of Dynamic
4.2 The kerosine shall conform to the following require-
2
Viscosity)
ments when tested for burning quality as specified:
4.2.1 Time of Burning—A minimum of 16 h continuous
1
This specification is under the jurisdiction of ASTM Committee D02 on
3
Petroleum Products and Lubricantsand is the direct responsibility of Subcommittee Annual Book of ASTM Standards, Vol 05.02.
4
D02. E on Burner, Diesel, Non-aviation Gas Turbine, and Marine Fuels. Annual Book of ASTM Standards, Vol 05.03.
5
Current edition approved June 10, 2001. Published July 2001. Originally Annual Book of ASTM Standards, Vol 05.04.
6
published as D 3699 – 78. Last previous edition D 3699 – 98. Standard Methods for Analysis and Testing of Petroleum and Related Products,
2
Annual Book of ASTM Standards, Vol 05.01. Institute of Petroleum, 61 New Cavendish St., London, W7M 8AR, Vol 1.
Copyright © ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superseded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
D 3699
TABLE 1 Detailed Req
...

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Section  
Scope  
1  
Referenced Documents  
2  
Terminology  
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Summary of Test Method  
4  
Significance and Use  
5  
Apparatus  
6  
Engine Fluids and Cleaning Solvents  
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Engine/Stand Calibration and Non-Reference Oil Tests  
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Test Procedure  
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Report  
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Precision and Bias  
13  
Annexes  
Safety Precautions  
Annex A1  
Intake Air Aftercooler  
Annex A2  
The Cummins ISB Engine Build Parts Kit  
Annex A3  
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Annex A4  
External Oil System  
Annex A5  
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Annex A6  
Specified Units and Formats  
Annex A7  
Oil Analyses  
Annex A8  
Alternate Fuel Approval Process  
Annex A9  
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Test Method  
Petroleum Products  
Boiling Range, °C (°F)
(approximate)  
A  
Light Distillates  
15–260 (60–500)  
B  
Middle Distillates  
200–370 (400–700)  
Gas Oils  
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C  
Residua  
510+ (950+ )  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. The preferred units are mass %.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Sections 7.2 and 7.4.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8252-23(Test Method)
Standard Test Method for Vanadium and Nickel in Crude and Residual Oil by X-ray Spectrometry

SIGNIFICANCE AND USE
5.1 This test method provides a rapid and precise elemental measurement with simple sample preparation. Typical analysis times are approximately 4 min to 5 min per sample with a preparation time of approximately 1 min to 3 min per sample.  
5.2 The quality of crude oil is related to the amount of sulfur present. Knowledge of the vanadium and nickel concentration is necessary for processing purposes as well as contractual agreements.  
5.3 The presence of vanadium and nickel presents significant risks for contamination of the cracking catalysts in the refining process.  
5.4 This test method provides a means of determining whether the vanadium and nickel content of crude meets the operational limits of the refinery and whether the metal content will have a deleterious effect on the refining process or when used as a fuel.
SCOPE
1.1 This test method covers the quantitative determination of total vanadium and nickel in crude and residual oil in the concentration ranges shown in Table 1 using X-ray fluorescence (XRF) spectrometry.  
1.2 Sulfur is measured for analytical purposes only for the compensation of X-ray absorption matrix effects affecting the vanadium and nickel X-rays. For measurement of sulfur by standard test method use Test Methods D4294, D2622 or other suitable standard test method for sulfur in crude and residual oils.  
1.3 This test method is limited to the use of X-ray fluorescence (XRF) spectrometers employing an X-ray tube for excitation in conjunction with wavelength dispersive detection system or energy dispersive high resolution semiconductor detector with the ability to separate signals of adjacent and near-adjacent elements.  
1.4 This test method uses inter-element correction factors calculated from XRF theory, the fundamental parameters (FP) approach, or best fit regression.  
1.5 Samples containing higher concentrations than shown in Table 1 must be diluted to bring the elemental concentration of the diluted material within the scope of this test method.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6.1 The preferred concentrations units are mg/kg for vanadium and nickel.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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