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ASTM D7213-11

(Test Method)

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography

Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography

SIGNIFICANCE AND USE
The boiling range distribution of light and medium petroleum distillate fractions provides an insight into the composition of feed stocks and products related to petroleum refining process, This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.
This test method extends the scope of boiling range determination by gas chromatography to include light and medium petroleum distillate fractions beyond the scope of Test Method D 2887 (538°C) and below Test Method D 6352 (700°C).
Boiling range distributions obtained by this test method are theoretically equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D 2892). They are not equivalent to results from low efficiency distillation such as those obtained with Test Method D 86 or D 1160.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. This test method is applicable to petroleum distillates having an initial boiling point greater than 100°C and a final boiling point less than 615°C at atmospheric pressure as measured by this test method.
1.2 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for example, naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example, alcohols, ethers, acids or esters) or residue are not to be analyzed by this test method. See Test Methods D 3710, D 2887, D 6352, or D 5307.
1.3 This test method uses the principles of simulated distillation methodology.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Apr-2011
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0H - Chromatographic Distribution Methods
Current Stage
Ref Project

Relations

Replaces
ASTM D7213-05e1 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography
Effective Date
01-May-2011
Replaced By
ASTM D7213-12 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography
Effective Date
01-Dec-2012
Referred By
ASTM D7500-15(2019) - Standard Test Method for Determination of Boiling Range Distribution of Distillates and Lubricating Base Oils—in Boiling Range from 100 °C to 735 °C by Gas Chromatography
Effective Date
01-May-2011
Referred By
ASTM D8519-23 - Standard Test Method for Determination of Hydrocarbon Types in Waste Plastic Process Oil Using Gas Chromatography with Vacuum Ultraviolet Absorption Spectroscopy Detection (GC-VUV)
Effective Date
01-May-2011
Referred By
ASTM D7398-21 - Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography
Effective Date
01-May-2011

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ASTM D7213-11 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography
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REDLINE ASTM D7213-11 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas ChromatographyREDLINE ASTM D7213-11 - Standard Test Method for Boiling Range Distribution of Petroleum Distillates in the Boiling Range from 100 to 615°C by Gas Chromatography
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7213 − 11
StandardTest Method for
Boiling Range Distribution of Petroleum Distillates in the
1
Boiling Range from 100 to 615°C by Gas Chromatography
This standard is issued under the fixed designation D7213; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D2887Test Method for Boiling Range Distribution of Pe-
troleum Fractions by Gas Chromatography
1.1 Thistestmethodcoversthedeterminationoftheboiling
D2892Test Method for Distillation of Crude Petroleum
range distribution of petroleum products. This test method is
(15-Theoretical Plate Column)
applicable to petroleum distillates having an initial boiling
D3710TestMethodforBoilingRangeDistributionofGaso-
point greater than 100°C and a final boiling point less than
line and Gasoline Fractions by Gas Chromatography
615°C at atmospheric pressure as measured by this test
D4626Practice for Calculation of Gas Chromatographic
method.
Response Factors
1.2 The test method is not applicable for analysis of
D5307Test Method for Determination of Boiling Range
petroleum distillates containing low molecular weight compo-
Distribution of Crude Petroleum by Gas Chromatography
nents (for example, naphthas, reformates, gasolines, crude 3
(Withdrawn 2011)
oils). Materials containing heterogeneous components (for
D6300Practice for Determination of Precision and Bias
example, alcohols, ethers, acids or esters) or residue are not to
Data for Use in Test Methods for Petroleum Products and
be analyzed by this test method. See Test Methods D3710,
Lubricants
D2887, D6352,or D5307.
D6352Test Method for Boiling Range Distribution of Pe-
troleumDistillatesinBoilingRangefrom174to700°Cby
1.3 This test method uses the principles of simulated distil-
lation methodology. Gas Chromatography
E355PracticeforGasChromatographyTermsandRelation-
1.4 The values stated in SI units are to be regarded as
ships
standard. No other units of measurement are included in this
E594Practice for Testing Flame Ionization Detectors Used
standard.
in Gas or Supercritical Fluid Chromatography
1.5 This standard does not purport to address all of the
E1510Practice for Installing Fused Silica Open Tubular
safety concerns, if any, associated with its use. It is the
Capillary Columns in Gas Chromatographs
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
3. Terminology
bility of regulatory limitations prior to use.
3.1 Definitions—This test method makes reference to many
common gas chromatographic procedures, terms, and relation-
2. Referenced Documents
ships. Detailed definitions of these can be found in Practices
2
2.1 ASTM Standards:
E355, E594, and E1510.
D86Test Method for Distillation of Petroleum Products at
3.2 Definitions of Terms Specific to This Standard:
Atmospheric Pressure
3.2.1 area slice—the area, resulting from the integration of
D1160TestMethodforDistillationofPetroleumProductsat
the chromatographic detector signal, within a specified reten-
Reduced Pressure
tiontimeinterval.Inareaslicemode(see6.4.2),peakdetection
parameters are bypassed and the detector signal integral is
recorded as area slices of consecutive, fixed duration time
1
This test method is under the jurisdiction of ASTM Committee D02 on
intervals.
PetroleumProductsandLubricantsandisthedirectresponsibilityofSubcommittee
D02.04.0H on Chromatographic Distribution Methods.
3.2.2 corrected area slice—an area slice corrected for base-
CurrenteditionapprovedMay1,2011.PublishedJuly2011.Originallyapproved
line offset, by subtraction of the exactly corresponding area
´1
in 2005. Last previous edition approved in 2005 as D7213–05 . DOI: 10.1520/
slice in a previously recorded blank (non-sample) analysis.
D7213-11.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D7213 − 11
3.2.3 cumulative corrected area—the accumulated sum of 5. Significance and Use
correctedareaslicesfromthebeginningoftheanalysisthrough
5.1 The boiling range distribution of light and medium
a given retention time, ignoring any non-sample area (for
petroleum distillate f
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
´1
Designation:D7213–05 Designation: D7213 – 11
Standard Test Method for
Boiling Range Distribution of Petroleum Distillates in the
1
Boiling Range from 100 to 615°C by Gas Chromatography
This standard is issued under the fixed designation D7213; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
´ NOTE—Corrected 6.3 editorially in October 2008.
1. Scope*
1.1 This test method covers the determination of the boiling range distribution of petroleum products. This test method is
applicable to petroleum distillates having an initial boiling point greater than 100°C and a final boiling point less than 615°C at
atmospheric pressure as measured by this test method.
1.2 The test method is not applicable for analysis of petroleum distillates containing low molecular weight components (for
example, naphthas, reformates, gasolines, crude oils). Materials containing heterogeneous components (for example, alcohols,
ethers, acids or esters) or residue are not to be analyzed by this test method. See Test Methods D3710, D2887, D6352, or D5307.
1.3 This test method uses the principles of simulated distillation methodology.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D86 Test Method for Distillation of Petroleum Products at Atmospheric Pressure
D1160 Test Method for Distillation of Petroleum Products at Reduced Pressure
D2887 Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
D2892 Test Method for Distillation of Crude Petroleum (15-Theoretical Plate Column)
D3710 Test Method for Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography
D4626 Practice for Calculation of Gas Chromatographic Response Factors
D5307 Test Method for Determination of Boiling Range Distribution of Crude Petroleum by Gas Chromatography D6300
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
D6352 Test Method for Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700C by Gas
Chromatography
E355 Practice for Gas Chromatography Terms and Relationships
E594 Practice for Testing Flame Ionization Detectors Used in Gas or Supercritical Fluid Chromatography
E1510 Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatographs
3. Terminology
3.1 Definitions—Thistestmethodmakesreferencetomanycommongaschromatographicprocedures,terms,andrelationships.
Detailed definitions of these can be found in Practices E355, E594, and E1510.
3.2 Definitions of Terms Specific to This Standard:
3.2.1 area slice—the area, resulting from the integration of the chromatographic detector signal, within a specified retention
time interval. In area slice mode (see 6.4.2), peak detection parameters are bypassed and the detector signal integral is recorded
as area slices of consecutive, fixed duration time intervals.
1
This test method is under the jurisdiction ofASTM Committee D02 on Petroleum Products and Lubricants and is the direct responsibility of Subcommittee D02.04.0H
on Chromatographic Distribution Methods.
Current edition approved Nov. 1, 2005. Published January 2006. DOI: 10.1520/D7213-05E01.
´1
CurrenteditionapprovedMay1,2011.PublishedJuly2011.Originallyapprovedin2005.Lastpreviouseditionapprovedin2005asD7213–05 .DOI:10.1520/D7213-11.
2
ForreferencedASTMstandards,visittheASTMwebsite,www.astm.org,orcontactASTMCustomerServiceatservice@astm.org.For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D7213 – 11
3.2.2 corrected area slice—an area slice corrected for baseline offset, by subtraction of the exactly
...

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Standard Test Method for Bromine Numbers of Petroleum Distillates and Commercial Aliphatic Olefins by Electrometric Titration

SIGNIFICANCE AND USE
5.1 The bromine number is useful as a measure of aliphatic unsaturation in petroleum samples. When used in conjunction with the calculation procedure described in Annex A2, it can be used to estimate the percentage of olefins in petroleum distillates boiling up to approximately 315 °C (600 °F).  
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SIGNIFICANCE AND USE
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5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
5.3 The Wright Blending Methods are generally preferred since they have a firmer basis in theory, and are more accurate. The Wright Blending Methods require component viscosities to be known at two temperatures. The ASTM Blending Methods are mathematically simpler and may be used when viscosities are known at a single temperature.  
5.4 Although this practice was developed using kinematic viscosity and volume fraction of each component, the dynamic viscosity or mass fraction, or both, may be used instead with minimal error if the densities of the components do not differ greatly. For fuel blends, it was found that viscosity blending using mass fractions gave more accurate results. For base stock blends, there was no significant difference between mass fraction and volume fraction calculations.  
5.5 The calculations described in this practice have been computerized as a spreadsheet and are available as an adjunct.3
SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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