EN 15705:2010
(Main)Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylen-urea oligomers (method B)
Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylen-urea oligomers (method B)
Fertilizers containing the condensates of urea and specified aldehydes (with crotonaldehyde called crotonyliden diurea or CDU, with isobutyraldehyde called isobutylidene diurea or IBDU, with formaldehyde called urea formaldehyde or methylene urea or MU) are covered by Annex I of the Regulation (EC) 2003/2003 [1] as nitrogenous fertilizers. The methods described in this European Standard enable the quantitative determination of these condensates and the determination of the solubility of the MU-oligomers according to the Regulation.
Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B)
Diese Europäische Norm legt Verfahren für die Bestimmung von Isobutylidendiharnstoff (IBDU), Crotony-lidendiharnstoff (CDU) (Verfahren A) und Methylenharnstoff-Oligomere (MU) (Verfahren B) in Düngemitteln mit Hochleistungs-Flüssigchromatographie (HPLC) fest.
Das Verfahren gilt für alle Düngemittel, die keine störenden organischen Verbindungen enthalten.
Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylène-urée (méthode B)
La présente Norme européenne spécifie les méthodes de dosage de l’isobutylidène diurée (IBDU), de la
crotonylidène diurée (CDU) (méthode A) et des oligomères de méthylène-urée (MU) (méthode B) dans les
engrais par chromatographie liquide haute performance (HPLC).
La méthode est applicable à tous les engrais qui ne contiennent pas de composés organiques interférents.
Gnojila - Določevanje kondenzatov sečnine s tekočinsko kromatografijo visoke ločljivosti (HPLC) - Izobutilidendiurea in krotonilidendiurea (metoda A) in oligomeri metilenuree (metoda B)
Ta evropski standard določa metode za določevanje izobutilidendiura(IBDU), krotonilidendiurea(CDU) (metoda A) ter oligomeri metilenuree (MU) (metoda B) v gnojilih s tekočinsko kromatografijo visoke ločljivosti (HPLC). Metoda se uporablja za vsa gnojila, ki ne vsebujejo motečih organskih spojin.
General Information
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B)Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylene-urée (méthode B)Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylene-urea oligomers (method B)65.080GnojilaFertilizersICS:Ta slovenski standard je istoveten z:EN 15705:2010SIST EN 15705:2010en,fr,de01-oktober-2010SIST EN 15705:2010SLOVENSKI
STANDARDSIST-TS CEN/TS 15705:20091DGRPHãþD
SIST EN 15705:2010
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15705
March 2010 ICS 65.080 Supersedes CEN/TS 15705:2009English Version
Fertilizers - Determination of urea condensates using high-performance liquid chromatography (HPLC) - Isobutylidenediurea and crotonylidenediurea (method A) and methylen-urea oligomers (method B)
Engrais - Dosage des condensats d'urée par chromatographie liquide haute performance (HPLC) - Isobutylidène diurée et crotonylidène diurée (méthode A) et oligomères de méthylène-urée (méthode B)
Düngemittel - Bestimmung von Harnstoffkondensaten mit Hochleistungs-Flüssigchromatographie (HPLC) - Isobutylidendiharnstoff und Crotonylidendiharnstoff (Verfahren A) und Methylenharnstoff-Oligomere (Verfahren B) This European Standard was approved by CEN on 21 February 2010.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
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B-1000 Brussels © 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 15705:2010: ESIST EN 15705:2010
EN 15705:2010 (E) 2 Contents Page Foreword .3Introduction .41Scope .52Normative references .53Terms and definitions .54Sampling and sample preparation .55Method A: Determination of CDU and IBDU .56Method B: Determination of methylen-urea oligomers (MU) .87Precision method A and method B . 138Test report . 14Annex A (informative)
Results of the inter-laboratory tests . 15Annex B (informative)
Chromatogram and calibration curves method A . 17Annex C (informative)
Chromatogram and calibration curves method B . 19Bibliography .
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