Surface active Agents - Determination of tetraacetyl ethylene diamine (TAED) content in TAED granules - Gas chromatographic method

This European Standard specifies a method for the determination of tetraacetyl ethylene diamine (TAED) content greater than or equal to 25 g/100 g in granules.

Grenzflächenaktive Stoffe - Bestimmung des Tetraacetylethylendiamin (TAED)-Gehalts in TAED-Granulaten - Gaschromatographisches Verfahren

Diese Europäische Norm legt ein Verfahren zur Bestimmung des Massenanteiles an Tetraacetylethylendiamin
(TAED) von größer oder gleich 25 g/100 g in Granulaten fest.

Agents de surface - Détermination de la teneur en tétra-acétyl-éthylène diamine (TAED) dans les granulés de TAED - Méthode par chromatographie en phase gazeuse

La présente Norme européenne spécifie une méthode de détermination des teneurs en tétra-acétyl-éthylène diamine (TAED) égales ou supérieures à 25 g/100 g dans des granulés.

Površinsko aktivne snovi – Določevanje tetraacetil etilendiamina (TAED) v granulah TAED – Metoda plinske kromatografije

General Information

Status
Published
Publication Date
21-Jun-2005
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Due Date
03-Jun-2020
Completion Date
03-Jun-2020

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SLOVENSKI STANDARD
SIST EN 14666:2005
01-november-2005
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Surface active Agents - Determination of tetraacetyl ethylene diamine (TAED) content in

TAED granules - Gas chromatographic method

Grenzflächenaktive Stoffe - Bestimmung des Tetraacetylethylendiamin (TAED)-Gehalts

in TAED-Granulaten - Gaschromatographisches Verfahren

Agents de surface - Détermination de la teneur en tétra-acétyl-éthylene diamine (TAED)

dans les granulés de TAED - Méthode par chromatographie en phase gazeuse
Ta slovenski standard je istoveten z: EN 14666:2005
ICS:
71.100.40 Površinsko aktivna sredstva Surface active agents
SIST EN 14666:2005 en

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 14666:2005
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SIST EN 14666:2005
EUROPEAN STANDARD
EN 14666
NORME EUROPÉENNE
EUROPÄISCHE NORM
June 2005
ICS 71.100.40
English version
Surface active Agents - Determination of tetraacetyl ethylene
diamine (TAED) content in TAED granules - Gas
chromatographic method

Agents de surface - Détermination de la teneur en tétra- Grenzflächenaktive Stoffe - Bestimmung des

acétyl-éthylène diamine (TAED) dans les granulés de Tetraacetylethylendiamin (TAED)-Gehalts in TAED-

TAED - Méthode par chromatographie en phase gazeuse Granulaten - Gaschromatographisches Verfahren

This European Standard was approved by CEN on 19 May 2005.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European

Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national

standards may be obtained on application to the Central Secretariat or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation

under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official

versions.

CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,

Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Slovakia,

Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36 B-1050 Brussels

© 2005 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 14666:2005: E

worldwide for CEN national Members.
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SIST EN 14666:2005
EN 14666:2005 (E)
Contents
Page

Foreword ..................................................................................................................................................................3

1 Scope ...........................................................................................................................................................4

2 Normative references .................................................................................................................................4

3 Principle.......................................................................................................................................................4

4 Reagents......................................................................................................................................................4

5 Apparatus ....................................................................................................................................................4

6 Sampling and preparation of the sample ..................................................................................................5

7 Procedure ....................................................................................................................................................5

8 Calculation and expression of results.......................................................................................................6

9 Precision......................................................................................................................................................6

10 Test report ...................................................................................................................................................7

Annex A (informative) Typical gas chromatogram...............................................................................................8

Annex B (informative) Results of interlaboratory test .......................................................................................10

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SIST EN 14666:2005
EN 14666:2005 (E)
Foreword

This document (EN 14666:2005) has been prepared by Technical Committee CEN/TC 276 “Surface active agents”,

the secretariat of which is held by AFNOR.

This European Standard shall be given the status of a national standard, either by publication of an identical text or

by endorsement, at the latest by December 2005, and conflicting national standards shall be withdrawn at the latest

by December 2005.

According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following

countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark,

Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,

Netherlands, Norway, Poland, Portugal, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

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SIST EN 14666:2005
EN 14666:2005 (E)
1 Scope

This European Standard specifies a method for the determination of tetraacetyl ethylene diamine (TAED) content

greater than or equal to 25 g/100 g in granules.
2 Normative references

The following referenced documents are indispensable for the application of this document. For dated references,

only the edition cited applies. For undated references, the latest edition of the referenced document (including any

amendments) applies.
ISO 607, Surface active agents and detergents – Methods of sample division.
3 Principle

The TAED granules are dissolved in acetonitrile, the internal standard is added to this solution and finally it is

injected to a gas chromatograph. A flame ionisation detector is used for detection. The results are calculated from

the peak areas taking into account the response factors that are determined previously.

4 Reagents

During the analysis, unless otherwise specified, use only reagents of recognized analytical grade that have been

checked in advance as not interfering with the analytical results.
4.1 Acetonitrile, C H N.
2 3
4.2 Stearic acid methyl ester, C H O , ≥ 99 % (m/m).
19 38 2
4.3 TAED, C H O N , ≥ 99 % (m/m).
10 16 4 2
4.4 Internal standard solution
Weigh into a 100 ml volumetric flask
...

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