Petroleum and related products - Precision of measurement methods and results - Part 2: Interpretation and application of precision data in relation to methods of test (ISO 4259-2:2017)

ISO 4259-2:2017 specifies the methodology for the application of precision estimates of a test method derived from ISO 4259‑1. In particular, it defines the procedures for setting the property specification limits based upon test method precision where the property is determined using a specific test method, and in determining the specification conformance status when there are conflicting results between supplier and receiver. Other applications of this test method precision are briefly described in principle without the associated procedures.
The procedures in ISO 4259-2:2017 have been designed specifically for petroleum and petroleum-related products, which are normally homogeneous. However, the procedures described in ISO 4259-2:2017 can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259-2:2017 to products for which the assumption of homogeneity can be questioned.

Mineralölerzeugnisse - Präzision von Messverfahren und Ergebnissen - Teil 2: Anwendung der Präzisionsdaten von Prüfverfahren (ISO 4259-2:2017)

Produits pétroliers et connexes - Fidélité des méthodes de mesure et de leurs résultats - Partie 2: Application des valeurs de fidélité relatives aux méthodes d'essai (ISO 4259-2:2017)

Le présent document prescrit la méthodologie pour l'application des estimations de fidélité d'une méthode d'essai déterminée selon l'ISO 4259‑1. En particulier, il définit les procédures à suivre pour fixer les limites de spécification d'une caractéristique sur la base de la fidélité de la méthode d'essai qui permet de déterminer la caractéristique en utilisant une méthode d'essai spécifique et pour déterminer l'état de conformité à une spécification quand il y a des résultats contradictoires entre le fournisseur et le destinataire. D'autres applications de cette fidélité des méthodes d'essai sont brièvement décrites en principe sans les procédures associées.
Les procédures du présent document ont été conçues spécifiquement pour les produits pétroliers et leurs produits connexes qui sont normalement homogènes. Les procédures décrites dans le présent document peuvent cependant aussi s'appliquer à d'autres types de produits homogènes. Il est nécessaire de procéder à des contrôles attentifs avant d'appliquer le présent document à des produits pour lesquels la présomption d'homogénéité peut être mise en question.

Nafta in sorodni proizvodi - Natančnost merilnih metod in rezultatov - 2. del: Razlaga in uporaba podatkov o natančnosti preskusnih metod (ISO 4259-2:2017)

Ta dokument določa metodologijo za uporabo ocen natančnosti preskusne metode iz standarda ISO 4259-1. Določa predvsem postopke za določitev omejitev specifikacij lastnosti na podlagi natančnosti preskusne metode, če se lastnost določi z uporabo posebne preskusne metode,
in pri določanju statusa skladnosti specifikacije, če med dobaviteljem in prejemnikom obstajajo nasprotujoči si rezultati. Drugi načini uporabe natančnosti te preskusne metode so na kratko opisani brez povezanih postopkov.
Postopki v tem dokumentu so bili zasnovani posebej za nafto in sorodne proizvode, ki so običajno homogeni. Kljub temu se postopki, opisani v tem dokumentu, lahko uporabljajo pri drugih vrstah homogenih proizvodov. Pred uporabo tega dokumenta za proizvode, pri katerih je predpostavka o homogenosti lahko vprašljiva, so potrebne temeljite preiskave.

General Information

Status
Published
Publication Date
05-Dec-2017
Withdrawal Date
29-Jun-2018
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
06-Dec-2017
Completion Date
06-Dec-2017

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SLOVENSKI STANDARD
01-februar-2018
1DGRPHãþD
SIST EN ISO 4259:2006
1DIWDLQVRURGQLSURL]YRGL1DWDQþQRVWPHULOQLKPHWRGLQUH]XOWDWRYGHO
5D]ODJDLQXSRUDEDSRGDWNRYRQDWDQþQRVWLSUHVNXVQLKPHWRG ,62
Petroleum and related products - Precision of measurement methods and results - Part
2: Interpretation and application of precision data in relation to methods of test(ISO 4259-
2:2017)
Mineralölerzeugnisse - Präzision von Messverfahren und Ergebnissen - Teil 2:
Anwendung der Werte für die Präzision von Prüfverfahren (ISO 4259-2:2017)
Produits pétroliers - Fidélité des méthodes de mesure et des résultats - Partie 2:
Application des valeurs de fidélité relatives aux méthodes d'essai (ISO 4259-2:2017)
Ta slovenski standard je istoveten z: EN ISO 4259-2:2017
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
75.180.30 Oprema za merjenje Volumetric equipment and
prostornine in merjenje measurements
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 4259-2
EUROPEAN STANDARD
NORME EUROPÉENNE
December 2017
EUROPÄISCHE NORM
ICS 75.080 Supersedes EN ISO 4259:2006
English Version
Petroleum and related products - Precision of
measurement methods and results - Part 2: Interpretation
and application of precision data in relation to methods of
test (ISO 4259-2:2017)
Produits pétroliers - Fidélité des méthodes de mesure Mineralölerzeugnisse - Präzision von Messverfahren
et des résultats - Partie 2: Application des valeurs de und Ergebnissen - Teil 2: Anwendung der Werte für die
fidélité relatives aux méthodes d'essai (ISO 4259- Präzision von Prüfverfahren (ISO 4259-2:2017)
2:2017)
This European Standard was approved by CEN on 27 October 2017.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 4259-2:2017 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 4259-2:2017) has been prepared by Technical Committee ISO/TC 28
"Petroleum and related products, fuels and lubricants from natural or synthetic sources" in
collaboration with Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related
products of petroleum, synthetic and biological origin” the secretariat of which is held by NEN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by June 2018, and conflicting national standards shall be
withdrawn at the latest by June 2018.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 4259:2006.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 4259-2:2017 has been approved by CEN as EN ISO 4259-2:2017 without any
modification.
INTERNATIONAL ISO
STANDARD 4259-2
First edition
2017-11
Petroleum and related products —
Precision of measurement methods
and results —
Part 2:
Interpretation and application of
precision data in relation to methods
of test
Produits pétroliers — Fidélité des méthodes de mesure et des
résultats —
Partie 2: Application des valeurs de fidélité relatives aux méthodes
d'essai
Reference number
ISO 4259-2:2017(E)
©
ISO 2017
ISO 4259-2:2017(E)
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Ch. de Blandonnet 8 • CP 401
CH-1214 Vernier, Geneva, Switzerland
Tel. +41 22 749 01 11
Fax +41 22 749 09 47
copyright@iso.org
www.iso.org
ii © ISO 2017 – All rights reserved

ISO 4259-2:2017(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Application and significance of repeatability, r, and reproducibility, R .2
4.1 General . 2
4.2 Repeatability, r . 2
4.2.1 General. 2
4.2.2 Acceptability of results . 2
4.2.3 Confidence limits calculations using results collected under
repeatability conditions. 3
4.3 Reproducibility, R . 3
4.3.1 Acceptability of results . 3
4.3.2 Confidence limits calculations using results collected under
reproducibility conditions . 5
4.4 Use of reproducibility to determine bias between two different test methods that
purport to measure the same property . 5
4.4.1 General. 5
4.4.2 Process . 5
5 Specifications . 6
5.1 Aim of specifications . 6
5.2 Construction of specifications limits in relation to scope and precision of the
specified test method . 6
6 Assessment of quality conformance to specification . 7
6.1 General . 7
6.2 Assessment of quality conformance by the supplier . 8
6.3 Assessment of quality conformance by the recipient . 9
6.3.1 General. 9
6.3.2 Single batch of product . 9
6.3.3 Multiple batches of product . 9
6.3.4 Procedure for recipient to assess conformance for a single batch of product.10
7 Dispute procedure .11
7.1 Resolve dispute by negotiation .11
7.2 Use of the test method or procedure in case of dispute .11
7.3 Dispute resolution procedure .12
7.4 Dispute unresolved.12
7.5 Example of a dispute resolution.14
Annex A (informative) Explanation of formulae given in Clause 4 .15
Annex B (informative) Dispute resolution for specifications based on a specified degree
of criticality .18
Annex C (informative) Statistical control in the execution of test methods by a laboratory.21
Annex D (informative) General approach to bias assessment using multiple materials .23
Annex E (informative) Glossary .24
Bibliography .25
ISO 4259-2:2017(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing Internation
...

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