EN ISO 19628:2021

Fine ceramics (advanced ceramics, advanced technical ceramics) - Thermophysical properties of ceramic composites - Determination of specific heat capacity (ISO 19628:2017)

ISO 19628:2017 describes two methods for the determination of the specific heat capacity of ceramic matrix composites with continuous reinforcements (1D, 2D, 3D).
Unidirectional (1D), bi-directional (2D) and tridirectional (XD, with 2 < x ≤ 3).
The two methods are:
-      method A: drop calorimetry;
-      method B: differential scanning calorimetry.
They are applicable from ambient temperature up to a maximum temperature, depending on the method: method A can be used up to 2 250 K, while method B is limited to 1 900 K.
NOTE          Method A is limited to the determination of an average value of the specific heat capacity over a given temperature range and can give a larger spread of results.

Hochleistungskeramik - Thermophysikalische Eigenschaften von keramischen Verbundwerkstoffen - Bestimmung der spezifischen Wärmekapazität (ISO 19628:2017)

Dieses Dokument legt zwei Verfahren zur Bestimmung der spezifischen Wärmekapazität von keramischen Verbundwerkstoffen mit Endlos-Faserverstärkung (1D, 2D, 3D) fest.
Unidirektional (1D), bidirektional (2D) und tridirektional (XD, mit 2 < x <- 3).
Die beiden Verfahren sind:
- Verfahren A: Fallkalorimetrie;
- Verfahren B: dynamische Differenz-Kalorimetrie.
Die Verfahren sind von Umgebungstemperatur bis zu einer verfahrensabhängigen Höchsttemperatur anwendbar: Verfahren A kann bis 2 250 K angewendet werden, während Verfahren B auf Temperaturen bis 1 900 K beschränkt ist.
ANMERKUNG Verfahren A ist auf die Bestimmung einer mittleren spezifischen Wärmekapazität für einen vorgegebenen Temperaturbereich beschränkt und kann daher zu größeren Messwertstreuungen führen.

Céramiques techniques - Propriétés thermophysiques des composites céramiques - Détermination de la capacité thermique specifique (ISO 19628:2017)

L'ISO 19628:2017 décrit deux méthodes pour la détermination de la capacité thermique spécifique des composites à matrice céramique à renforts continus (1D, 2D, 3D).
Les matrices sont à renforts unidirectionnels (1D), bidirectionnels (2D) et tridirectionnels (XD, avec 2 < x ≤ 3).
Les deux méthodes sont:
-      méthode A: calorimétrie à chute;
-      méthode B: calorimétrie différentielle à balayage.
Elles sont applicables depuis la température ambiante jusqu'à une température maximale qui dépend de la méthode: la méthode A peut être utilisée jusqu'à 2 250 K, tandis que la méthode B est limitée à 1 900 K.
NOTE       La méthode A se limite à la détermination d'une valeur moyenne de la capacité thermique spécifique dans un intervalle de température donné et peut conduire à une dispersion importante des résultats.

Fina keramika (sodobna keramika, sodobna tehnična keramika) - Termofizikalne lastnosti keramičnih kompozitov - Ugotavljanje specifične toplotne kapacitete (ISO 19628:2017)

General Information

• Status: Withdrawn
• Publication Date: 02-Mar-2021
• Withdrawal Date: 12-Nov-2024
• ICS: 81.060.30 - Advanced ceramics
• Technical Committee: CEN/TC 184 - Advanced technical ceramics
• Drafting Committee: CEN/TC 184/SC 1 - Ceramic composites
• Current Stage: 6060 - Definitive text made available (DAV) - Publishing
• Start Date: 03-Mar-2021
• Due Date: 24-Apr-2022
• Completion Date: 03-Mar-2021
• Ref Project: SIST EN ISO 19628:2021 - Fine ceramics (advanced ceramics, advanced technical ceramics) - Thermophysical properties of ceramic composites - Determination of specific heat capacity (ISO 19628:2017)

Relations

• Replaces: EN 1159-3:2003/AC:2008 - Advanced technical ceramics - Ceramic composites, thermophysical properties - Part 3: Determination of specific heat capacity
• Effective Date: 10-Mar-2021
• Replaces: EN 1159-3:2003/AC:2007 - Advanced technical ceramics - Ceramic composites, thermophysical properties - Part 3: Determination of specific heat capacity
• Effective Date: 10-Mar-2021
• Replaces: EN 1159-3:2003 - Advanced technical ceramics - Ceramic composites, thermophysical properties - Part 3: Determination of specific heat capacity
• Effective Date: 04-Nov-2020
• Replaced By: EN ISO 19628:2024 - Fine ceramics (advanced ceramics, advanced technical ceramics) - Thermophysical properties of ceramic composites - Determination of specific heat capacity (ISO 19628:2024)
• Effective Date: 21-Jun-2023

Standards Content (Sample)

SLOVENSKI STANDARD
01-maj-2021
Nadomešča:
SIST EN 1159-3:2004
SIST EN 1159-3:2004/AC:2007
SIST EN 1159-3:2004/AC:2008
Fina keramika (sodobna keramika, sodobna tehnična keramika) - Termofizikalne
lastnosti keramičnih kompozitov - Ugotavljanje specifične toplotne kapacitete (ISO
19628:2017)
Fine ceramics (advanced ceramics, advanced technical ceramics) - Thermophysical
properties of ceramic composites - Determination of specific heat capacity (ISO
19628:2017)
Hochleistungskeramik - Thermophysikalische Eigenschaften von keramischen
Verbundwerkstoffen - Bestimmung der spezifischen Wärmekapazität (ISO 19628:2017)
Céramiques techniques - Propriétés thermophysiques des composites céramiques -
Détermination de la capacité thermique specifique (ISO 19628:2017)
Ta slovenski standard je istoveten z: EN ISO 19628:2021
ICS:
81.060.30 Sodobna keramika Advanced ceramics
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 19628
EUROPEAN STANDARD
NORME EUROPÉENNE
March 2021
EUROPÄISCHE NORM
ICS 81.060.30 Supersedes EN 1159-3:2003
English Version
Fine ceramics (advanced ceramics, advanced technical
ceramics) - Thermophysical properties of ceramic
composites - Determination of specific heat capacity (ISO
19628:2017)
Céramiques techniques - Propriétés thermophysiques Hochleistungskeramik - Thermophysikalische
des composites céramiques - Détermination de la Eigenschaften von keramischen Verbundwerkstoffen -
capacité thermique specifique (ISO 19628:2017) Bestimmung der spezifischen Wärmekapazität (ISO
19628:2017)
This European Standard was approved by CEN on 22 February 2021.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2021 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 19628:2021 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
The text of ISO 19628:2017 has been prepared by Technical Committee ISO/TC 206 "Fine ceramics” of
the International Organization for Standardization (ISO) and has been taken over as EN ISO 19628:2021
by Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by
DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by September 2021, and conflicting national standards
shall be withdrawn at the latest by September 2021.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 1159-3:2003.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the
United Kingdom.
Endorsement notice
The text of ISO 19628:2017 has been approved by CEN as EN ISO 19628:2021 without any modification.

INTERNATIONAL ISO
STANDARD 19628
First edition
2017-04
Fine ceramics (advanced ceramics,
advanced technical ceramics) —
Thermophysical properties of ceramic
composites — Determination of
specific heat capacity
Céramiques techniques — Propriétés thermophysiques des composites
céramiques — Détermination de la capacité thermique specifique
Reference number
ISO 19628:2017(E)
©
ISO 2017
ISO 19628:2017(E)
© ISO 2017, Published in Switzerland
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
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ii © ISO 2017 – All rights reserved

ISO 19628:2017(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Method A – drop calorimetry. 2
4.1 Principle . 2
4.2 Apparatus . 2
4.3 Standard reference materials . 2
4.4 Test specimens . 2
4.5 Calibration of calorimeter . 3
4.5.1 General. 3
4.5.2 Electrical calibration . 3
4.5.3 Calibration using standard reference material . 3
4.6 Test procedures . 3
4.6.1 Test without a crucible . 3
4.6.2 Test with a crucible . 4
4.6.3 Description of test. 4
4.7 Calculations . 5
4.7.1 General. 5
4.7.2 Determination of the calorimetric calibration factor . 5
4.7.3 Determination of mean specific heat capacity C .
p
5 Method B – differential scanning calorimetry . 6
5.1 Principle . 6
5.1.1 General. 6
5.1.2 Stepwise heating method . 6
5.1.3 Continuous heating method . 7
5.2 Apparatus . 8
5.3 Standard reference materials, SRM . 8
5.4 Test specimens . 8
5.5 Temperature calibration . 8
5.6 Test procedure for the determination of C .
p 8
5.6.1 General. 8
5.6.2 Method 1: Measurements requiring the knowledge of the K factor . 9
5.6.3 Method 2: measurements requiring the use of a reference standard
material (SRM) .11
5.7 Calculation of results .14
5.7.1 Method requiring the knowledge of the K factor .14
5.7.2 Method using an SRM .16
6 Test report .17
Annex A (normative) Drop calorimetry – determination of the calibration factor using
standard reference material .18
Annex B (informative) Standard reference material .20
Annex C (informative) Materials for calorimeter calibrations .25
Bibliography .26
ISO 19628:2017(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
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