EN ISO 3262-17:2024
(Main)Extenders - Specifications and methods of test - Part 17: Precipitated calcium silicate (ISO 3262-17:2024)
Extenders - Specifications and methods of test - Part 17: Precipitated calcium silicate (ISO 3262-17:2024)
This document specifies requirements and corresponding methods of test for precipitated calcium silicate.
Füllstoffe - Anforderungen und Prüfverfahren - Teil 17: Gefälltes Calciumsilicat (ISO 3262-17:2024)
Dieses Dokument legt Anforderungen und die entsprechenden Prüfverfahren für gefälltes Calciumsilicat fest.
Matières de charge - Spécifications et méthodes d’essai - Partie 17: Silicate de calcium précipité (ISO 3262-17:2024)
Le présent document spécifie les exigences relatives au silicate de calcium précipité ainsi que les méthodes d’essai correspondantes.
Polnila - Specifikacije in preskusne metode - 17. del: Oborjeni kalcijev silikat (ISO 3262-17:2024)
Ta dokument določa zahteve in ustrezne preskusne metode za oborjeni kalcijev silikat.
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-marec-2024
Nadomešča:
SIST EN ISO 3262-17:2001
Polnila - Specifikacije in preskusne metode - 17. del: Oborjeni kalcijev silikat (ISO
3262-17:2024)
Extenders - Specifications and methods of test - Part 17: Precipitated calcium silicate
(ISO 3262-17:2024)
Füllstoffe - Anforderungen und Prüfverfahren - Teil 17: Gefälltes Calciumsilicat (ISO
3262-17:2024)
Matières de charge - Spécifications et méthodes d’essai - Partie 17: Silicate de calcium
précipité (ISO 3262-17:2024)
Ta slovenski standard je istoveten z: EN ISO 3262-17:2024
ICS:
87.060.10 Pigmenti in polnila Pigments and extenders
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EN ISO 3262-17
EUROPEAN STANDARD
NORME EUROPÉENNE
January 2024
EUROPÄISCHE NORM
ICS 87.060.10 Supersedes EN ISO 3262-17:2000
English Version
Extenders - Specifications and methods of test - Part 17:
Precipitated calcium silicate (ISO 3262-17:2024)
Matières de charge - Spécifications et méthodes d'essai Füllstoffe - Anforderungen und Prüfverfahren - Teil 17:
- Partie 17: Silicate de calcium précipité (ISO 3262- Gefälltes Calciumsilicat (ISO 3262-17:2024)
17:2024)
This European Standard was approved by CEN on 7 January 2024.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2024 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3262-17:2024 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
This document (EN ISO 3262-17:2024) has been prepared by Technical Committee ISO/TC 256
"Pigments, dyestuffs and extenders" in collaboration with Technical Committee CEN/TC 298 “Pigments
and extenders” the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by July 2024, and conflicting national standards shall be
withdrawn at the latest by July 2024.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 3262-17:2000.
Any feedback and questions on this document should be directed to the users’ national standards
body/national committee. A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO 3262-17:2024 has been approved by CEN as EN ISO 3262-17:2024 without any
modification.
International
Standard
ISO 3262-17
Second edition
Extenders — Specifications and
2024-01
methods of test —
Part 17:
Precipitated calcium silicate
Matières de charge — Spécifications et méthodes d’essai —
Partie 17: Silicate de calcium précipité
Reference number
ISO 3262-17:2024(en) © ISO 2024
ISO 3262-17:2024(en)
© ISO 2024
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
ISO 3262-17:2024(en)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Requirements and test methods . 2
5 Sampling . 2
6 Determination of silica content . 2
6.1 Principle .2
6.2 Reagents .2
6.3 Apparatus .3
6.4 Procedure .3
6.4.1 Number of determinations .3
6.4.2 Test portion .4
6.4.3 Determination .4
6.4.4 Determination of the total loss on ignition .4
6.5 Expression of results . .5
6.6 Precision . . .5
7 Determination of the composition by spectrometry . 5
7.1 Principle .5
7.2 Reagents and materials .6
7.3 Apparatus .6
7.4 Procedure .7
7.4.1 Preparation of standard matching solutions .7
7.4.2 Spectrometric measurement .7
7.4.3 Calibration graph .8
7.4.4 Preparation of the test solution .8
7.4.5 Determination .8
7.5 Expression of results .9
7.5.1 Concentration of Ca, Na and Si.9
7.5.2 Calculation of the oxide content for each element .9
7.6 Precision . . .9
8 Determination of residue on sieve . 10
8.1 Principle .10
8.2 Materials .10
8.3 Apparatus .10
8.4 Procedure .10
8.4.1 Number of determinations .10
8.4.2 Test portion .10
8.4.3 Determination .10
8.5 Expression of results . .11
8.6 Precision . . .11
9 Test report .
...
SLOVENSKI STANDARD
oSIST prEN ISO 3262-17:2023
01-maj-2023
Polnila - Specifikacije in preskusne metode - 17. del: Oborjeni kalcijev silikat
(ISO/DIS 3262-17:2023)
Extenders - Specifications and methods of test - Part 17: Precipitated calcium silicate
(ISO/DIS 3262-17:2023)
Füllstoffe - Anforderungen und Prüfverfahren - Teil 17: Gefälltes Calciumsilicat (ISO/DIS
3262-17:2023)
Matières de charge - Spécifications et méthodes d’essai - Partie 17: Silicate de calcium
précipité (ISO/DIS 3262-17:2023)
Ta slovenski standard je istoveten z: prEN ISO 3262-17
ICS:
87.060.10 Pigmenti in polnila Pigments and extenders
oSIST prEN ISO 3262-17:2023 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
oSIST prEN ISO 3262-17:2023
oSIST prEN ISO 3262-17:2023
DRAFT INTERNATIONAL STANDARD
ISO/DIS 3262-17
ISO/TC 256 Secretariat: DIN
Voting begins on: Voting terminates on:
2023-03-09 2023-06-01
Extenders — Specifications and methods of test —
Part 17:
Precipitated calcium silicate
ICS: 87.060.10
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 3262-17:2023(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2023
oSIST prEN ISO 3262-17:2023
ISO/DIS 3262-17:2023(E)
DRAFT INTERNATIONAL STANDARD
ISO/DIS 3262-17
ISO/TC 256 Secretariat: DIN
Voting begins on: Voting terminates on:
Extenders — Specifications and methods of test —
Part 17:
Precipitated calcium silicate
ICS: 87.060.10
This document is circulated as received from the committee secretariat.
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
© ISO 2023
ISO/CEN PARALLEL PROCESSING
THEREFORE SUBJECT TO CHANGE AND MAY
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
NOT BE REFERRED TO AS AN INTERNATIONAL
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on STANDARD UNTIL PUBLISHED AS SUCH.
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
IN ADDITION TO THEIR EVALUATION AS
or ISO’s member body in the country of the requester. BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
ISO copyright office
USER PURPOSES, DRAFT INTERNATIONAL
CP 401 • Ch. de Blandonnet 8
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
CH-1214 Vernier, Geneva
POTENTIAL TO BECOME STANDARDS TO
Phone: +41 22 749 01 11
WHICH REFERENCE MAY BE MADE IN
Reference number
Email: copyright@iso.org
NATIONAL REGULATIONS.
Website: www.iso.org ISO/DIS 3262-17:2023(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
Published in Switzerland
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
ii
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2023
oSIST prEN ISO 3262-17:2023
ISO/DIS 3262-17:2023(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Requirements and test methods . 2
5 Sampling . 2
6 Determination of silica content . 2
6.1 Principle . 2
6.2 Reagents . 3
6.3 Apparatus . 3
6.4 Procedure . 3
6.5 Expression of results . . 5
6.6 Precision . . . 5
7 Determination of the composition by spectrometry . 5
7.1 Principle . 5
7.2 Reagents and materials . 6
7.3 Apparatus . 6
7.4 Procedure . 7
7.5 Expression of results . 9
7.6 Precision . . . 9
8 Determination of residue on sieve .10
8.1 Principle . 10
8.2 Materials . 10
8.3 Apparatus . 10
8.4 Procedure . 10
8.5 Expression of results . . 11
8.6 Precision . . . 11
9 Test report .11
iii
oSIST prEN ISO 3262-17:2023
ISO/DIS 3262-17:2023(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to
the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see
www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 256, Pigments, dyestuffs and extenders ,
in collaboration with the European Committee for Standardization (CEN) Technical Committee CEN/
TC 298, Pigments and extenders, in accordance with the Agreement on technical cooperation between
ISO and CEN (Vienna Agreement).
This second edition cancels and replaces the first edition (ISO 3262-17:2000), which has been technically
revised.
The main changes are as follows:
— the first part of the title has been changed to "Extenders";
— ISO 19246 has been added as an alternative test method for oil absorption value in Table 2;
— ISO 13320 has been added as test method for particle size distribution in Table 3;
— DIN 53163 has been added as test method for lightness (standard value Y) in Table 3;
— CAS-numbers have been added to all reagents used for the test methods specified;
— the normative references have been updated and the text has been editorially revised.
A list of all parts in the ISO 3262 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
iv
oSIST prEN ISO 3262-17:2023
DRAFT INTERNATIONAL STANDARD ISO/DIS 3262-17:2023(E)
Extenders — Specifications and methods of test —
Part 17:
Precipitated calcium silicate
1 Scope
This document specifies requirements and corresponding methods of test for precipitated calcium
silicate.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 648, Laboratory glassware — Single-volume pipettes
ISO 787-2, General methods of test for pigments and extenders — Part 2: Determination of matter volatile
at 105 °C
ISO 787-5, General methods of test for pigments and extenders — Part 5: Determination of oil absorption
value
ISO 787-9, General methods of test for pigments and extenders — Part 9: Determination of pH value of an
aqueous suspension
ISO 3262-1, Extenders — Specifications and methods of test — Part 1: Introduction and general test
methods
ISO 3696, Water for analytical laboratory use — Specification and test methods
ISO 5794-1:2010, Rubber compounding ingredients — Silica, precipitated, hydrated — Part 1: Non-rubber
tests
ISO 13320, Particle size analysis — Laser diffraction methods
ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling
ISO 18451-1, Pigments, dyestuffs and extenders — Terminology — Part 1: General terms
ISO 19246, Rubber compounding ingredients — Silica — Oil absorption of precipitated silica
DIN 53163, Pigments and extenders — Determination of lightness of extenders and white pigments in
powder form
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 184
...
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