Plastics - Unsaturated polyesters and epoxide resins - Determination of total chlorine content (ISO 4615:1979)

Specification of two methods for the determination of chlorine: Oxidation of the test portion with sodium peroxide (method A) in a Parr bomb or with gaseous oxygen (method B) in a flask, followed by electrometric or volumetric titration of the resulting chlorides. Blank tests shall be carried out by using the same quanities of reagents as in the determination.

Kunststoffe - Ungesättigte Polyester und Epoxidharze - Bestimmung des Gesamtchlorgehaltes (ISO 4615:1979)

Diese Internationale Norm legt zwei Verfahren zur Bestimmung des Gesamtchlor- gehaltes in ungesättigten Polyestern und Epoxidharzen fest, nämlich: Verfahren A: Aufschluß in einer Verbrennungsbombe; Verfahren B: Aufschluß im Erlenmeyerkolben.

Plastiques - Résines de polyesters non saturés et époxydes - Détermination de la teneur totale en chlore (ISO 4615:1979)

La présente Norme internationale spécifie deux méthodes de dosage du chlore total dans les résines de polyesters non saturés et époxydes, à savoir :  - méthode A combustion dans une bombe ;  - méthode B combustion dans un ballon.  
NOTES  1 La détermination de la teneur en chlore et brome combinés, ou de la teneur en brome seulement, est également possible par ces méthodes. Le mode opératoire approprié doit faire l'objet d'un accord entre 1 "acheteur et le vendeur".  2 Ces méthodes ne sont pas applicables au dosage du chlore total dans les résines époxydes contenant du chlore comme impureté.

Polimerni materiali - Nenasičeni poliestri in epoksidne smole - Določevanje celotnega klora (ISO 4615:1979)

General Information

Status
Published
Publication Date
18-May-1999
Withdrawal Date
29-Nov-1999
Technical Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
19-May-1999
Completion Date
19-May-1999

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 4615:2000
01-maj-2000
3ROLPHUQLPDWHULDOL1HQDVLþHQLSROLHVWULLQHSRNVLGQHVPROH'RORþHYDQMH
FHORWQHJDNORUD ,62
Plastics - Unsaturated polyesters and epoxide resins - Determination of total chlorine
content (ISO 4615:1979)
Kunststoffe - Ungesättigte Polyester und Epoxidharze - Bestimmung des
Gesamtchlorgehaltes (ISO 4615:1979)
Plastiques - Résines de polyesters non saturés et époxydes - Détermination de la teneur
totale en chlore (ISO 4615:1979)
Ta slovenski standard je istoveten z: EN ISO 4615:1999
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
83.080.10 Duromeri Thermosetting materials
SIST EN ISO 4615:2000 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 4615:2000

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SIST EN ISO 4615:2000

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SIST EN ISO 4615:2000

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SIST EN ISO 4615:2000
International Standard
INTERNATIONAL ORGANIZATION FOR STANDARDIZATION.MEXJIYHAPO~HAR OPTAHI’l3ALU4R fl0 CTAHAAPTt43A~MM~ORGANISATION INTERNATIONALE DE NORMALISATION
Plastics - Unsaturated polyesters and epoxide resins -
Determination of total chlorine content
Plas tiques - Rksines de polyesters non saturb et Kapoxydes - Dbtermina tion de Ia teneur totale en chlore
First edition - 1979-12-01
UDC 678.674 + 678.685 : 543.848 Ref. No. ISO 46151979 (EI
Bescriptors : plastics, Polyester resins, epoxy resins, Chemical analysis, determination of content, chlorine, combustion analysis.
Price based on 5 pages

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SIST EN ISO 4615:2000
ISO (the International Organization for Standardization) is a worldwide federation
of national Standards institutes (ISO member bodies). The work of developing
International Standards is carried out through ISO technical committees. Every
member body interested in a subject for which a technical committee has been set
up has the right to be represented on that committee. International organizations,
governmental and non-governmental, in liaison with ISO, also take part in the work.
Draft International Standards adopted by the technical committees are circulated
to the member bodies for approval before their acceptance as International
Standards by the ISO Council.
International Standard ISO 4615 was developed by Technical Committee
ISO/TC 61, Plastics, and was circulated to the member bodies in August 1978.
lt has been approved by the member bodies of the following countries :
South Africa, Rep. of
Austria Hungary
Belgium Iran Sweden
Bulgaria I taly Switzerland
Canada Japan Turkey
Czechoslovakia Korea, Rep. of USA
Egypt, Arab Rep. of Mexico USSR
Netherlands Yugoslavia
Finland
New Zealand
Germany, F.R.
Romania
G reece
Th e member body o f the following country expressed disapproval of the document
on technical grounds
United Kingdom
0 Internationaf Organkation for Standardization, 1979 l
Printed in Seitzerland

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SIST EN ISO 4615:2000
INTERNATIONAL STANDARD ISO 4615-1979 (E)
Plastics - Unsaturated polyesters and epoxide resins -
Determination of total chlorine content
1 SCOPE AND FIELD OF APPLICATION 3.3 Nitrit acid, concentrated, p = 1,42 g/mI.
This International Standard specifies two methods for the
3.4 Sodium Peroxide, granulated.
determination of the total chlorine content of unsaturated
Polyesters and epoxide resins, namely :
3.5 Starch or sucrose as combustion aids.
-
method A : combustion in a bomb;
For method B only :
-
method B : combustion in a flask.
3.6 Oxygen, gaseous.
NOTES
1 Determination of combined chlorine and bromine content or
3.7 Sodium nitrate.
is also possible by these methods. The
bromine content only,
appropriate procedure shall be agreed upon by the purchaser and
the supplier.
3.8 Potassium hydroxide Solution, 100 g/l.
2 These methods are not applicable to the determination of total
chlorine in epoxy resins containing chlorine as an impurity.
3.9 Hydrogen peroxide Solution, 300 g/l.
2 PRINCIPLE
4 APPARATUS
Oxidation of a test Portion with sodium peroxide (method A)
or gaseous Oxygen (method B) followed by electrometric
or volumetric titration of the resulting chlorides. 4.1 Balance, to weigh to an accuracy of 0,000 1 g.
4.2 Equipment for Volhard titration or for electrometric
3 REAGENTS
titration, with a burette having a capacity and accuracy
appropriate to the Chosen method (A or B).
During the analysis, use only reagents of known analytical
quality, and only distilled water or water of at least equival-
For method A only :
ent purity.
4.3 Combustion bomb (for example Parr bomb or another
3.1 Silver nitrate, Standard volumetric Solution,
bomb which gives the same res
...

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