ISO 10382:2002

Soil quality — Determination of organochlorine pesticides and polychlorinated biphenyls — Gas-chromatographic method with electron capture detection

ISO 10382:2002 specifies a method for quantitative determination of seven polychlorinated biphenyls and seventeen organochlorine pesticides in soil. ISO 10382:2002 is applicable to all types of soil. Under the conditions specified in ISO 10382:2002, limits of detection of 0,1 micrograms per kilogram to 4 micrograms per kilogram (expressed as dry matter) can be achieved.

Qualité du sol — Dosage des pesticides organochlorés et des biphényles polychlorés — Méthode par chromatographie en phase gazeuse avec détection par capture d'électrons

L'ISO 10382:2002 spécifie une méthode de dosage quantitatif de sept biphényls polychlorés et de dix-sept pesticides organochlorés dans le sol. L'ISO 10382:2002 est applicable à tous les types de sol. Dans les conditions spécifiées dans l'ISO 10382:2002, les limites de détection de 0,1 g/kg à 4 g/kg (exprimées en matière sèche) peuvent être obtenues.

Kakovost tal - Določevanje organoklornih pesticidov in polikloriranih bifenilov - Plinska kromatografija z detektorjem z zajemom elektronov (ECD)

Ta mednarodni standard določa metodo za kvantitativno določevanje sedmih polikloriranih bifenilov in sedemnajstih organoklornih pesticidov v tleh.
Ta mednarodni standard se uporablja za vse vrste tal.
Pod pogoji, določenimi v tem mednarodnem standardu, je mogoče doseči meje zaznavanja od 0,1 μg/kg do 4 μg/kg (izraženo kot suha snov).

General Information

• Status: Withdrawn
• Publication Date: 16-Oct-2002
• ICS: 13.080.10 - Chemical characteristics of soils
• Technical Committee: ISO/TC 190/SC 3 - Chemical and physical characterization
• Drafting Committee: ISO/TC 190/SC 3/WG 6 - Organic analysis
• Current Stage: 9599 - Withdrawal of International Standard
• Completion Date: 05-Oct-2023
• Directive: TP111 - Uredba o določanju statusa zaradi fitofarmacevtskih sredstev ogroženega območja vodonosnikov in njihovih hidrografskih zaledij in o ukrepih celovite sanacije
• Ref Project: SIST ISO 10382:2019 - Soil quality - Determination of organochlorine pesticides and polychlorinated biphenyls - Gas-chromatographic method with electron capture detection

Relations

• Revised: ISO 23646:2022 - Soil quality — Determination of organochlorine pesticides by gas chromatography with mass selective detection (GC-MS) and gas chromatography with electron-capture detection (GC-ECD)
• Effective Date: 26-Nov-2021
• Revised: ISO 18475:2023 - Environmental solid matrices — Determination of polychlorinated biphenyls (PCB) by gas chromatography - mass selective detection (GC-MS) or electron-capture detection (GC-ECD)
• Effective Date: 06-Jun-2022

Standards Content (Sample)

SLOVENSKI STANDARD
SIST ISO 10382:2019
01-oktober-2019
Kakovost tal - Določevanje organoklornih pesticidov in polikloriranih bifenilov -
Plinska kromatografija z detektorjem z zajemom elektronov (ECD)
Soil quality - Determination of organochlorine pesticides and polychlorinated biphenyls -
Gas-chromatographic method with electron capture detection
Qualité du sol - Dosage des pesticides organochlorés et des biphényles polychlorés -
Méthode par chromatographie en phase gazeuse avec détection par capture d'électrons
Ta slovenski standard je istoveten z: ISO 10382:2002
ICS:
13.080.10 Kemijske značilnosti tal Chemical characteristics of
soils
71.040.50 Fizikalnokemijske analitske Physicochemical methods of
metode analysis
SIST ISO 10382:2019 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST ISO 10382:2019

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SIST ISO 10382:2019


INTERNATIONAL ISO
STANDARD 10382
First edition
2002-10-15


Soil quality — Determination of
organochlorine pesticides and
polychlorinated biphenyls — Gas-
chromatographic method with electron
capture detection
Qualité du sol — Dosage des pesticides organochlorés et des biphényles
polychlorés — Méthode par chromatographie en phase gazeuse avec
détection par capture d'électrons




Reference number
ISO 10382:2002(E)
©
 ISO 2002

---------------------- Page: 3 ----------------------
SIST ISO 10382:2019
ISO 10382:2002(E)
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©  ISO 2002
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic
or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body
in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
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Printed in Switzerland

ii © ISO 2002 – All rights reserved

---------------------- Page: 4 ----------------------
SIST ISO 10382:2019
ISO 10382:2002(E)
Contents Page
Foreword . iv
1 Scope. 1
2 Normative references. 1
3 Principle . 1
4 Reagents . 2
5 Apparatus. 4
6 Preparation of standard solutions of PCB and OCP . 7
7 Sampling and preservation of samples . 8
7.1 Sampling . 8
7.2 Sample preservation and pretreatment . 8
8 Procedure. 8
8.1 Blank.
...

INTERNATIONAL ISO
STANDARD 10382
First edition
2002-10-15


Soil quality — Determination of
organochlorine pesticides and
polychlorinated biphenyls — Gas-
chromatographic method with electron
capture detection
Qualité du sol — Dosage des pesticides organochlorés et des biphényles
polychlorés — Méthode par chromatographie en phase gazeuse avec
détection par capture d'électrons




Reference number
ISO 10382:2002(E)
©
 ISO 2002

---------------------- Page: 1 ----------------------
ISO 10382:2002(E)
PDF disclaimer
This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not
be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this
file, parties accept therein the responsibility of not infringing Adobe's licensing policy. The ISO Central Secretariat accepts no liability in this
area.
Adobe is a trademark of Adobe Systems Incorporated.
Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters
were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event
that a problem relating to it is found, please inform the Central Secretariat at the address given below.


©  ISO 2002
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic
or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body
in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail [e-mail]
Web www.iso.ch
Printed in Switzerland

ii © ISO 2002 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 10382:2002(E)
Contents Page
Foreword . iv
1 Scope. 1
2 Normative references. 1
3 Principle . 1
4 Reagents . 2
5 Apparatus. 4
6 Preparation of standard solutions of PCB and OCP . 7
7 Sampling and preservation of samples . 8
7.1 Sampling . 8
7.2 Sample preservation and pretreatment . 8
8 Procedure. 8
8.1 Blank. 8
8.2 Extraction and concentration . 8
8.3 Clean-up of the extract . 9
8.4 Column-chromatographic separation of PCBs and non-polar OCPs from several polar OCPs. 9
8.5 Gas chromatographic analysis. 10
9 Test report. 14
10 Accuracy . 14
Annex A (informative) Table of retention times of polychlorinated biphenyls and
...

NORME ISO
INTERNATIONALE 10382
Première édition
2002-10-15



Qualité du sol — Dosage des pesticides
organochlorés et des biphényles
polychlorés — Méthode par
chromatographie en phase gazeuse avec
détection par capture d'électrons
Soil quality — Determination of organochlorine pesticides and
polychlorinated biphenyls — Gas-chromatographic method with electron
capture detection




Numéro de référence
ISO 10382:2002(F)
©
 ISO 2002

---------------------- Page: 1 ----------------------
ISO 10382:2002(F)
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©  ISO 2002
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Imprimé en Suisse

ii © ISO 2002 – Tous droits réservés

---------------------- Page: 2 ----------------------
ISO 10382:2002(F)
Sommaire Page
Avant-propos . iv
1 Domaine d'application . 1
2 Références normatives. 1
3 Principe . 1
4 Réactifs. 2
5 Appareillage. 4
6 Préparation des solutions étalons de PCB et de POC .7
7 Échantillonnage et conservation des échantillons . 8
7.1 Échantillonnage. 8
7.2 Conservation et prétraitement des échantillons. 8
8 Mode opératoire . 8
8.1 Essai à blanc. 8
8.2 Extraction et concentration. 8
8.3 Purification de l’extrait. 9
8.4 Séparation par chromatographie en colonnes entre PCB et POC non polaires d’une part et
plusieurs POC polaires d’autre part. 10
8.5 Analyse par chromatographie en phase gazeuse . 10
9 Rapport d'essai.
...

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Qualité du sol - Dosage des pesticides organochlorés et des biphényles polychlorés - Méthode par chromatographie en phase gazeuse avec détection par capture d'électronsSoil quality - Determination of organochlorine pesticides and polychlorinated biphenyls - Gas-chromatographic method with electron capture detection71.040.50Fizikalnokemijske analitske metodePhysicochemical methods of analysis13.080.10Chemical characteristics of soilsICS:Ta slovenski standard je istoveten z:ISO 10382:2002oSIST ISO 10382:2019en01-maj-2019oSIST ISO 10382:2019SLOVENSKI
STANDARD



oSIST ISO 10382:2019



Reference numberISO 10382:2002(E)© ISO 2002
INTERNATIONAL STANDARD ISO10382First edition2002-10-15Soil quality — Determination of organochlorine pesticides and polychlorinated biphenyls — Gas-chromatographic method with electron capture detection Qualité du sol — Dosage des pesticides organochlorés et des biphényles polychlorés — Méthode par chromatographie en phase gazeuse avec détection par capture d'électrons
oSIST ISO 10382:2019



ISO 10382:2002(E) PDF disclaimer This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not be edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this file, parties accept therein the responsibility of not infringing Adobe's licensing policy. The ISO Central Secretariat accepts no liability in this area. Adobe is a trademark of Adobe Systems Incorporated. Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event that a problem relating to it is found, please inform the Central Secretariat at the address given below.
©
ISO 2002 All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's member body in the country of the requester. ISO copyright office Case postale 56 • CH-1211 Geneva 20 Tel.
+ 41 22 749 01 11 Fax
+ 41 22 749 09 47 E-mail
[e-mail] Web
www.iso.ch Printed in Switzerland
ii © ISO 2002 – All rights reserved
oSIST ISO 10382:2019



ISO 10382:2002(E) © ISO 2002 – All rights reserved iii Contents Page Foreword.iv 1 Scope.1 2 Normative references.1 3 Principle.1 4 Reagents.2 5 Apparatus.4 6 Preparation of standard solutions of PCB and OCP.7 7 Sampling and preservation of samples.8 7.1 Sampling.8 7.2 Sample preservation and pretreatment.8 8 Procedure.8 8.1 Blank.8 8.2 Extraction and concentration.8 8.3 Clean-up of the extract.9 8.4 Column-chromatographic separation of PCBs and non-polar OCPs from several polar OCPs.9 8.
...