Plastics - Differential scanning calorimetry (DSC) - Part 3: Determination of temperature and enthalpy of melting and crystallization (ISO 11357-3:2018)

This document specifies a method for the determination of the temperatures and enthalpies of melting
and crystallization of crystalline or partially crystalline plastics.

Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 3: Bestimmung der Schmelz- und Kristallisationstemperatur und der Schmelz- und Kristallisationsenthalpie (ISO 11357-3:2018)

Dieses Dokument legt ein Verfahren für die Bestimmung der Schmelz- und Kristallisationstemperaturen und
der Schmelz- und Kristallisationsenthalpien von kristallinen oder teilkristallinen Kunststoffen fest.

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 3: Détermination de la température et de l'enthalpie de fusion et de cristallisation (ISO 11357-3:2018)

L'ISO 11357-3:2018 spécifie une méthode permettant de déterminer les températures et les enthalpies de fusion et de cristallisation des plastiques cristallins ou partiellement cristallins.

Polimerni materiali - Diferenčna dinamična kalorimetrija (DSC) - 3. del: Ugotavljanje temperature in entalpije taljenja in kristalizacije (ISO 11357-3:2018)

Ta dokument določa metodo za ugotavljanje temperature in entalpije taljenja
in kristalizacije kristalničnih ali delno kristalničnih polimernih materialov.

General Information

Status
Published
Public Enquiry End Date
28-Jun-2017
Publication Date
14-May-2018
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
10-May-2018
Due Date
15-Jul-2018
Completion Date
15-May-2018

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SLOVENSKI STANDARD
SIST EN ISO 11357-3:2018
01-julij-2018
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SIST EN ISO 11357-3:2013
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Plastics - Differential scanning calorimetry (DSC) - Part 3: Determination of temperature

and enthalpy of melting and crystallization (ISO 11357-3:2018)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 3: Bestimmung der

Schmelz- und Kristallisationstemperatur und der Schmelz- und Kristallisationsenthalpie

(ISO 11357-3:2018)

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 3: Détermination de la

température et de l'enthalpie de fusion et de cristallisation (ISO 11357-3:2018)
Ta slovenski standard je istoveten z: EN ISO 11357-3:2018
ICS:
17.200.10 Toplota. Kalorimetrija Heat. Calorimetry
83.080.01 Polimerni materiali na Plastics in general
splošno
SIST EN ISO 11357-3:2018 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 11357-3:2018
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SIST EN ISO 11357-3:2018
EN ISO 11357-3
EUROPEAN STANDARD
NORME EUROPÉENNE
May 2018
EUROPÄISCHE NORM
ICS 83.080.01 Supersedes EN ISO 11357-3:2013
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 3:
Determination of temperature and enthalpy of melting and
crystallization (ISO 11357-3:2018)

Plastiques - Analyse calorimétrique différentielle (DSC) Kunststoffe - Dynamische Differenz-Thermoanalyse

- Partie 3: Détermination de la température et de (DSC) - Teil 3: Bestimmung der Schmelz- und

l'enthalpie de fusion et de cristallisation (ISO 11357- Kristallisationstemperatur und der Schmelz- und

3:2018) Kristallisationsenthalpie (ISO 11357-3:2018)
This European Standard was approved by CEN on 24 February 2018.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this

European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references

concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN

member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by

translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,

Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,

Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 11357-3:2018 E

worldwide for CEN national Members.
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SIST EN ISO 11357-3:2018
EN ISO 11357-3:2018 (E)
Contents Page

European foreword ....................................................................................................................................................... 3

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SIST EN ISO 11357-3:2018
EN ISO 11357-3:2018 (E)
European foreword

This document (EN ISO 11357-3:2018) has been prepared by Technical Committee ISO/TC 61 “Plastics”

in collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by

NBN.

This European Standard shall be given the status of a national standard, either by publication of an

identical text or by endorsement, at the latest by November 2018, and conflicting national standards

shall be withdrawn at the latest by November 2018.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. CEN shall not be held responsible for identifying any or all such patent rights.

This document supersedes EN ISO 11357-3:2013.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the

following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,

Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,

France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,

Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,

Turkey and the United Kingdom.
Endorsement notice

The text of ISO 11357-3:2018 has been approved by CEN as EN ISO 11357-3:2018 without any

modification.
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SIST EN ISO 11357-3:2018
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SIST EN ISO 11357-3:2018
INTERNATIONAL ISO
STANDARD 11357-3
Third edition
2018-03
Plastics — Differential scanning
calorimetry (DSC) —
Part 3:
Determination of temperature and
enthalpy of melting and crystallization
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 3: Détermination de la température et de l'enthalpie de fusion
et de cristallisation
Reference number
ISO 11357-3:2018(E)
ISO 2018
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SIST EN ISO 11357-3:2018
ISO 11357-3:2018(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2018

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting

on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address

below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved
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SIST EN ISO 11357-3:2018
ISO 11357-3:2018(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 2

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Test specimen .......................................................................................................................................................................................................... 2

7 Test conditions and specimen conditioning ............................................................................................................................ 2

8 Calibration .................................................................................................................................................................................................................. 2

9 Procedure..................................................................................................................................................................................................................... 2

9.1 Setting up the apparatus................................................................................................................................................................. 2

9.2 Loading the test specimen into the crucible .................................................................................................................. 2

9.3 Insertion of crucibles ......................................................................................................................................................................... 2

9.4 Temperature scan ................................................................................................................................................................................. 2

10 Expression of results ........................................................................................................................................................................................ 3

10.1 Determination of transition temperatures ..................................................................................................................... 3

10.2 Determination of enthalpies ....................................................................................................................................................... 4

11 Precision ....................................................................................................................................................................................................................... 5

12 Test report ................................................................................................................................................................................................................... 5

Bibliography ................................................................................................................................................................................................................................ 6

© ISO 2018 – All rights reserved iii
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SIST EN ISO 11357-3:2018
ISO 11357-3:2018(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www .iso .org/ patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.
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