Plastics - Differential scanning calorimetry (DSC) - Part 5: Determination of characteristic reaction-curve temperatures and times, enthalpy of reaction and degree of conversion (ISO 11357-5:2013)

EN-ISO 11357-5 specifies a method for the determination of reaction temperatures and times, enthalpies of reaction and degrees of conversion using differential scanning calorimetry (DSC). The method applies to monomers, prepolymers and polymers in the solid or liquid state. The material may contain fillers and/or initiators in the solid or liquid state.

Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 5: Bestimmung von charakteristischen Reaktionstemperaturen und -zeiten, Reaktionsenthalpie und Umsatz (ISO 11357-5:2013)

Dieser Teil von ISO 11357 legt ein Verfahren für die Bestimmung von Reaktionstemperaturen und -zeiten, Reaktionsenthalpien und Umsätzen mithilfe der dynamischen Differenz-Thermoanalyse (DSC) fest.
Das Verfahren gilt für Monomere, Vorpolymere und Polymere im festen oder flüssigen Zustand. Das Material kann Füllstoffe und/oder Initiatoren im festen oder flüssigen Zustand enthalten.

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 5: Détermination des températures et temps caractéristiques de la courbe de réaction, de l'enthalpie de réaction et du degré de transformation (ISO 11357-5:2013)

L'ISO 11357-5:2013 spécifie une méthode de détermination des températures et temps de réaction, des enthalpies de réaction et degrés de transformation, en utilisant une analyse calorimétrique différentielle (DSC).
La méthode est applicable aux monomères, prépolymères et polymères à l'état solide ou liquide. Le matériau peut contenir des charges et/ou initiateurs à l'état solide ou liquide.

Polimerni materiali - Diferenčna dinamična kalorimetrija (DSC) - 5. del: Ugotavljanje karakterističnih reakcijskih temperatur in časov, entalpije reakcije in stopnje pretvorbe (ISO 11357-5:2013)

Standard EN-ISO 11357-5 določa metodo za ugotavljanje karakterističnih reakcijskih temperatur in časov, entalpije reakcije in stopnje pretvorbe z diferenčno dinamično kalorimetrijo (DSC). Metoda se nanaša na monomere, prepolimere in polimere v tekoči ali trdni obliki. Material lahko vsebuje polnila in/ali iniciatorje v tekoči ali trdni obliki.

General Information

Status
Published
Public Enquiry End Date
09-Feb-2014
Publication Date
10-Apr-2014
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
28-Mar-2014
Due Date
02-Jun-2014
Completion Date
11-Apr-2014

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Standards Content (sample)

SLOVENSKI STANDARD
SIST EN ISO 11357-5:2014
01-maj-2014
3ROLPHUQLPDWHULDOL'LIHUHQþQDGLQDPLþQDNDORULPHWULMD '6& GHO

8JRWDYOMDQMHNDUDNWHULVWLþQLKUHDNFLMVNLKWHPSHUDWXULQþDVRYHQWDOSLMHUHDNFLMHLQ

VWRSQMHSUHWYRUEH ,62

Plastics - Differential scanning calorimetry (DSC) - Part 5: Determination of characteristic

reaction-curve temperatures and times, enthalpy of reaction and degree of conversion

(ISO 11357-5:2013)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 5: Bestimmung von

charakteristischen Reaktionstemperaturen und -zeiten, Reaktionsenthalpie und Umsatz

(ISO 11357-5:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 5: Détermination des

températures et temps caractéristiques de la courbe de réaction, de l'enthalpie de

réaction et du degré de transformation (ISO 11357-5:2013)
Ta slovenski standard je istoveten z: EN ISO 11357-5:2014
ICS:
17.200.10 Toplota. Kalorimetrija Heat. Calorimetry
83.080.01 Polimerni materiali na Plastics in general
splošno
SIST EN ISO 11357-5:2014 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
SIST EN ISO 11357-5:2014
---------------------- Page: 2 ----------------------
SIST EN ISO 11357-5:2014
EUROPEAN STANDARD
EN ISO 11357-5
NORME EUROPÉENNE
EUROPÄISCHE NORM
March 2014
ICS 83.080.01
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 5:
Determination of characteristic reaction-curve temperatures and
times, enthalpy of reaction and degree of conversion (ISO
11357-5:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) -

Partie 5: Détermination des températures et temps Teil 5: Bestimmung von charakteristischen

caractéristiques de la courbe de réaction, de l'enthalpie de Reaktionstemperaturen und -zeiten, Reaktionsenthalpie

réaction et du degré de transformation (ISO 11357-5:2013) und Umsatz (ISO 11357-5:2013)

This European Standard was approved by CEN on 6 March 2014.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European

Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national

standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation

under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same

status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,

Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United

Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2014 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 11357-5:2014 E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
SIST EN ISO 11357-5:2014
EN ISO 11357-5:2014 (E)
Contents Page

Foreword ..............................................................................................................................................................3

---------------------- Page: 4 ----------------------
SIST EN ISO 11357-5:2014
EN ISO 11357-5:2014 (E)
Foreword

The text of ISO 11357-5:2013 has been prepared by Technical Committee ISO/TC 61 “Plastics” of the

International Organization for Standardization (ISO) and has been taken over as EN ISO 11357-5:2014 by

Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.

This European Standard shall be given the status of a national standard, either by publication of an identical

text or by endorsement, at the latest by September 2014, and conflicting national standards shall be

withdrawn at the latest by September 2014.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent

rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following

countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech

Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,

Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,

Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.

Endorsement notice

The text of ISO 11357-5:2013 has been approved by CEN as EN ISO 11357-5:2014 without any modification.

---------------------- Page: 5 ----------------------
SIST EN ISO 11357-5:2014
---------------------- Page: 6 ----------------------
SIST EN ISO 11357-5:2014
INTERNATIONAL ISO
STANDARD 11357-5
Second edition
2013-03-15
Plastics — Differential scanning
calorimetry (DSC) —
Part 5:
Determination of characteristic
reaction-curve temperatures and
times, enthalpy of reaction and degree
of conversion
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 5: Détermination des températures et temps caractéristiques
de la courbe de réaction, de l’enthalpie de réaction et du degré de
transformation
Reference number
ISO 11357-5:2013(E)
ISO 2013
---------------------- Page: 7 ----------------------
SIST EN ISO 11357-5:2014
ISO 11357-5:2013(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2013

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form

or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior

written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of

the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved
---------------------- Page: 8 ----------------------
SIST EN ISO 11357-5:2014
ISO 11357-5:2013(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 1

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Test specimens........................................................................................................................................................................................................ 2

7 Test conditions and specimen conditioning ............................................................................................................................ 2

8 Calibration .................................................................................................................................................................................................................. 2

9 Procedure..................................................................................................................................................................................................................... 2

9.1 General ........................................................................................................................................................................................................... 2

9.2 Temperature-scanning method ................................................................................................................................................ 2

9.3 Isothermal method .............................................................................................................................................................................. 2

10 Determination of results .............................................................................................................................................................................. 4

10.1 Determination of characteristic temperatures and enthalpy of reaction (temperature-

scanning method) ................................................................................................................................................................................. 4

10.2 Determination of characteristic times and enthalpy of reaction (isothermal method)........... 4

10.3 Determination of degree of conversion ............................................................................................................................. 6

11 Precision ....................................................................................................................................................................................................................... 9

12 Test report ................................................................................................................................................................................................................... 9

Bibliography .............................................................................................................................................................................................................................10

© ISO 2013 – All rights reserved iii
---------------------- Page: 9 ----------------------
SIST EN ISO 11357-5:2014
ISO 11357-5:2013(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International

Standards adopted by the technical committees are circulated to the member bodies for voting.

Publication as an International Standard requires approval by at least 75 % of the member bodies

casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 11357-5 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-

chemical properties.

This second edition cancels and replaces the first edition (ISO 11357-5:1999), which has been technically

revised. Significant technical changes are the following:

— adaption of definition of characteristic temperatures and endo-/exothermic direction in accordance

with ISO 11357-1;
— revision of determination of results;
— revision of test report.

ISO 11357 consists of the following parts, under the general title Plastics — Differential scanning

calorimetry (DSC):
— Part 1: General principles

— Part 2: Determination of glass transition temperature and glass transition step height

— Part 3: Determination of temperature and enthalpy of melting and crystallization

— Part 4: Determination of specific heat capacity

— Part 5: Determination of characteristic reaction-curve temperatures and times, enthalpy of reaction

and degree of conversion

— Part 6: Determination of oxidation induction time (isothermal OIT) and oxidation induction temperature

(dynamic OIT)
— Part 7: Determination of crystallization kinetics
iv © ISO 2013 – All rights reserved
---------------------- Page: 10 ----------------------
SIST EN ISO 11357-5:2014
INTERNATIONAL STANDARD ISO 11357-5:2013(E)
Plastics — Differential scanning calorimetry (DSC) —
Part 5:
Determination of characteristic reaction-curve
temperatures and times, enthalpy of reaction and degree
of conversion

WARNING — Caution should be observed when working with materials which could give a

runaway reaction or exhibit other dangerous behaviour.
1 Scope

This part of ISO 11357 specifies a method for the determination of reaction temperatures and times,

enthalpies of reaction, and degrees of conversion using differential scanning calorimetry (DSC).

The method applies to monomers, prepolymers, and polymers in the solid or liquid state. The material

can contain fillers and/or initiators in the solid or liquid state.
2 Normative references
The following documents,
...

SLOVENSKI STANDARD
kSIST FprEN ISO 11357-5:2014
01-februar-2014
3ROLPHUQLPDWHULDOL'LIHUHQþQDGLQDPLþQDNDORULPHWULMD '6& GHO

8JRWDYOMDQMHNDUDNWHULVWLþQLKUHDNFLMVNLKWHPSHUDWXULQþDVRYHQWDOSLMHUHDNFLMHLQ

VWRSQMHSUHWYRUEH ,62

Plastics - Differential scanning calorimetry (DSC) - Part 5: Determination of characteristic

reaction-curve temperatures and times, enthalpy of reaction and degree of conversion

(ISO 11357-5:2013)
Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC) - Teil 5: Bestimmung von

charakteristischen Reaktionstemperaturen und -zeiten, Reaktionsenthalpie und Umsatz

(ISO 11357-5:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Partie 5: Détermination des

températures et temps caractéristiques de la courbe de réaction, de l'enthalpie de

réaction et du degré de transformation (ISO 11357-5:2013)
Ta slovenski standard je istoveten z: FprEN ISO 11357-5
ICS:
83.080.01 Polimerni materiali na Plastics in general
splošno
kSIST FprEN ISO 11357-5:2014 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST FprEN ISO 11357-5:2014
---------------------- Page: 2 ----------------------
kSIST FprEN ISO 11357-5:2014
EUROPEAN STANDARD
FINAL DRAFT
FprEN ISO 11357-5
NORME EUROPÉENNE
EUROPÄISCHE NORM
September 2013
ICS 83.080.01
English Version
Plastics - Differential scanning calorimetry (DSC) - Part 5:
Determination of characteristic reaction-curve temperatures and
times, enthalpy of reaction and degree of conversion (ISO
11357-5:2013)

Plastiques - Analyse calorimétrique différentielle (DSC) - Kunststoffe - Dynamische Differenz-Thermoanalyse (DSC)

Partie 5: Détermination des températures et temps - Teil 5: Bestimmung von charakteristischen

caractéristiques de la courbe de réaction, de l'enthalpie de Reaktionstemperaturen und -zeiten, Reaktionsenthalpie

réaction et du degré de transformation (ISO 11357-5:2013) und Umsatz (ISO 11357-5:2013)

This draft European Standard is submitted to CEN members for unique acceptance procedure. It has been drawn up by the Technical

Committee CEN/TC 249.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations which

stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other language

made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management

Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,

Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United

Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to

provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without notice and

shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2013 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprEN ISO 11357-5:2013: E

worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
kSIST FprEN ISO 11357-5:2014
FprEN ISO 11357-5:2013 (E)
Contents Page

Foreword ..............................................................................................................................................................3

---------------------- Page: 4 ----------------------
kSIST FprEN ISO 11357-5:2014
FprEN ISO 11357-5:2013 (E)
Foreword

The text of ISO 11357-5:2013 has been prepared by Technical Committee ISO/TC 61 “Plastics” of the

International Organization for Standardization (ISO) and has been taken over as FprEN ISO 11357-5:2013 by

Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.

This document is currently submitted to the Unique Acceptance Procedure.
Endorsement notice

The text of ISO 11357-5:2013 has been approved by CEN as FprEN ISO 11357-5:2013 without any

modification.
---------------------- Page: 5 ----------------------
kSIST FprEN ISO 11357-5:2014
---------------------- Page: 6 ----------------------
kSIST FprEN ISO 11357-5:2014
INTERNATIONAL ISO
STANDARD 11357-5
Second edition
2013-03-15
Plastics — Differential scanning
calorimetry (DSC) —
Part 5:
Determination of characteristic
reaction-curve temperatures and
times, enthalpy of reaction and degree
of conversion
Plastiques — Analyse calorimétrique différentielle (DSC) —
Partie 5: Détermination des températures et temps caractéristiques
de la courbe de réaction, de l’enthalpie de réaction et du degré de
transformation
Reference number
ISO 11357-5:2013(E)
ISO 2013
---------------------- Page: 7 ----------------------
kSIST FprEN ISO 11357-5:2014
ISO 11357-5:2013(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2013

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form

or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior

written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of

the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved
---------------------- Page: 8 ----------------------
kSIST FprEN ISO 11357-5:2014
ISO 11357-5:2013(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ...................................................................................................................................................................................... 1

3 Terms and definitions ..................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 1

5 Apparatus and materials.............................................................................................................................................................................. 2

6 Test specimens........................................................................................................................................................................................................ 2

7 Test conditions and specimen conditioning ............................................................................................................................ 2

8 Calibration .................................................................................................................................................................................................................. 2

9 Procedure..................................................................................................................................................................................................................... 2

9.1 General ........................................................................................................................................................................................................... 2

9.2 Temperature-scanning method ................................................................................................................................................ 2

9.3 Isothermal method .............................................................................................................................................................................. 2

10 Determination of results .............................................................................................................................................................................. 4

10.1 Determination of characteristic temperatures and enthalpy of reaction (temperature-

scanning method) ................................................................................................................................................................................. 4

10.2 Determination of characteristic times and enthalpy of reaction (isothermal method)........... 4

10.3 Determination of degree of conversion ............................................................................................................................. 6

11 Precision ....................................................................................................................................................................................................................... 9

12 Test report ................................................................................................................................................................................................................... 9

Bibliography .............................................................................................................................................................................................................................10

© ISO 2013 – All rights reserved iii
---------------------- Page: 9 ----------------------
kSIST FprEN ISO 11357-5:2014
ISO 11357-5:2013(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.

The main task of technical committees is to prepare International Standards. Draft International

Standards adopted by the technical committees are circulated to the member bodies for voting.

Publication as an International Standard requires approval by at least 75 % of the member bodies

casting a vote.

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights.

ISO 11357-5 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 5, Physical-

chemical properties.

This second edition cancels and replaces the first edition (ISO 11357-5:1999), which has been technically

revised. Significant technical changes are the following:

— adaption of definition of characteristic temperatures and endo-/exothermic direction in accordance

with ISO 11357-1;
— revision of determination of results;
— revision of test report.

ISO 11357 consists of the following parts, under the general title Plastics — Differential scanning

calorimetry (DSC):
— Part 1: General principles

— Part 2: Determination of glass transition temperature and glass transition step height

— Part 3: Determination of temperature and enthalpy of melting and crystallization

— Part 4: Determination of specific heat capacity

— Part 5: Determination of characteristic reaction-curve temperatures and times, enthalpy of reaction

and degree of conversion

— Part 6: Determination of oxidation induction time (isothermal OIT) and oxidation induction temperature

(dynamic OIT)
— Part 7: Determination of crystallization kinetics
iv © ISO 2013 – All rights reserved
---------------------- Page: 10 ----------------------
kSIST FprEN ISO 11357-5:2014
INTERNATIONAL STANDARD ISO 11357-5:2013(E)
Plastics — Differential scanning calorimetry (DSC) —
Part 5:
Determination of characteristic reaction-curve
temperatures and times, enthalpy of reaction and degree
of conversion

WARNING — Caution should be observed when working with materials which could give a

runaway reaction or exhibit other dangerous behaviour.
1 Scope

This part of ISO 11357 specifies a method for the determination of reaction temperatures and times,

enthalpies of reaction, and degrees of conversion using differential scanning calorimetry (DSC).

The method applies to monomers, prepolymers, and polymers in the solid or liquid state. The material

can contain fillers and/or initiators in the solid or liquid state.
2 Normative references

The following documents, in whole or in part, are normatively referenced in this document and are

indispensable for its application. For dated references, only the edition cited applies. For undated

references, the latest edition of the referenced document (including any amendments) applies.

ISO 11357-1,
...

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