SIST EN 15662:2009

Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method

This European Standard describes a method for the analysis of pesticide residues in produce with a low fat content, such as fruits, vegetables, cereals as well as processed products thereof including dried fruit. The method has been collaboratively studied on cucumber, lemon, wheat flour, raisins, apples, oranges and lettuce.

Pflanzliche Lebensmittel - Bestimmung von Pestizidrückständen mit GC-MS und/oder LC-MS/MS nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE - QuEChERS-Verfahren

Diese Europäische Norm beschreibt ein Verfahren für die Analyse von Pestizidrückständen in pflanz-lichen Lebensmitteln, wie z. B. Früchten (einschließlich Trockenfrüchten), Gemüse, Getreide und verarbei-teten Erzeugnissen davon. Das Verfahren wurde von verschiedenen Laboratorien an einer großen Anzahl an Lebensmittel/Pestizid-Kombinationen getestet.

Aliments d'origine végétale - Méthode polyvalente de détermination des résidus des pesticides par CG-SM et CL/SM(/SM) avec extraction/partition avec de l'acétonitrile et nettoyage par SPE dispersée - Méthode QuEChERS

Le présent projet de norme européenne décrit une méthode d’analyse des résidus de pesticides dans les aliments d'origine végétale tels que les fruits (y compris les fruits secs), les légumes, les céréales et leurs produits dérivés. Cette méthode a fait l’objet d’une étude collaborative sur un grand nombre de combinaisons denrées/pesticides.

Hrana rastlinskega izvora - Določanje ostankov pesticidov z uporabo GC-MS in/ali LC-MS(/MS) po delitvi in izpiranju acenotrila z disperzivno SPE - Metoda QuEChERS

General Information

• Status: Withdrawn
• Publication Date: 04-Dec-2008
• Withdrawal Date: 06-Jun-2018
• ICS: 67.050 - General methods of tests and analysis for food products
• Technical Committee: KŽP - Agricultural food products
• Current Stage: 9900 - Withdrawal (Adopted Project)
• Start Date: 07-Jun-2018
• Due Date: 30-Jun-2018
• Completion Date: 07-Jun-2018
• Ref Project: EN 15662:2008 - Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method

Relations

• Replaced By: SIST EN 15662:2018 - Foods of plant origin - Multimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE - Modular QuEChERS-method
• Effective Date: 08-Jun-2022
• Replaced By: SIST EN 15662:2018 - Foods of plant origin - Multimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and clean-up by dispersive SPE - Modular QuEChERS-method
• Effective Date: 01-Jul-2018

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.4X(&K(56Pflanzliche Lebensmittel - Bestimmung von Pestizidrückständen mit GC-MS und/oder LC-MS/MS nach Acetonitril-Extraktion/Verteilung und Reinigung mit dispersiver SPE - QuEChERS-VerfahrenAliments d'origine végétale - Méthode polyvalente de détermination des résidus des pesticides par CG-SM et CL/SM(/SM) avec extraction/partition avec de l'acétonitrile et nettoyage par SPE dispersée - Méthode QuEChERSFoods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method67.050Splošne preskusne in analizne metode za živilske proizvodeGeneral methods of tests and analysis for food productsICS:Ta slovenski standard je istoveten z:EN 15662:2008SIST EN 15662:2009en,fr,de01-januar-2009SIST EN 15662:2009SLOVENSKI
STANDARD



SIST EN 15662:2009



EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 15662November 2008ICS 67.050 English VersionFoods of plant origin - Determination of pesticide residues usingGC-MS and/or LC-MS/MS following acetonitrileextraction/partitioning and clean-up by dispersive SPE -QuEChERS-methodAliments d'origine végétale - Méthode polyvalente dedétermination des résidus des pesticides par CG-SM etSL/SM(SM) avec extraction/partition avec de l'acétonitrile etnettoyage par SPE dispersés - Méthode QuEchERSPflanzliche Lebensmittel - Bestimmung vonPestizidrückständen mit GC-MS und/oder LC-MS/MS nachAcetonitril-Extraktion/Verteilung und Reinigung mitdispersiver SPE - QuEChERS-VerfahrenThis European Standard was approved by CEN on 13 September 2008.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2008 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 15662:2008: ESIST EN 15662:2009



EN 15662:2008 (E) 2 Contents Page Foreword.3 1 Scope.4 2 Principle.4 3 Reagents.4 4 Apparatus.8 5 Procedure.10 6 Evaluation of results.16 7 Confirmatory tests.21 8 Precision.21 9 Test report.21 Annex A (informative)
Examples of experimental conditions.22 Annex B (informative)
Precision data.25 Annex C (informative)
Procedure schematically (for 10 g sample).
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