C01.31 - Volume Change

SIGNIFICANCE AND USE
4.1 The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO or MgO, or both, when present in hydraulic cement.3
SCOPE
1.1 This test method covers determination of the expansion of a hardened cement paste when exposed to the autoclave conditions in this method.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see the section on Safety Precautions.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Numerous properties of cementitious materials are controlled by their initial hydration rate. Examples include early-age strength development, heat release, and crack resistance. One direct and convenient measure of this initial hydration rate is provided by the measurement of the chemical shrinkage of the cement paste during its hydration. As cement hydrates, the hydration products occupy less volume than the initial reacting materials (cement and water). Due to this volume change, a hydrating cement paste will sorb water from its immediate surroundings, when available. At early times, this sorption is in direct proportion to the amount of hydration that has occurred.5 This method is based on the one developed by Geiker.6 The results are relevant to understanding the hydration behavior of cements. This method does not measure the bulk volume changes (autogenous shrinkage) associated with chemical shrinkage nor the cracking potential of concretes produced with the evaluated cement.
SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage.  
1.1.1 Procedure A, volumetric method.  
1.1.2 Procedure B, the density method.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage.”  
4.2 The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions.4 Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as standard. When combined standards are referenced, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).2  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage”.  
4.2 The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions.4 Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as standard. When combined standards are referenced, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).2  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO or MgO, or both, when present in hydraulic cement.3
SCOPE
1.1 This test method covers determination of the expansion of a hardened cement paste when exposed to the autoclave conditions in this method.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see the section on Safety Precautions.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Numerous properties of cementitious materials are controlled by their initial hydration rate. Examples include early-age strength development, heat release, and crack resistance. One direct and convenient measure of this initial hydration rate is provided by the measurement of the chemical shrinkage of the cement paste during its hydration. As cement hydrates, the hydration products occupy less volume than the initial reacting materials (cement and water). Due to this volume change, a hydrating cement paste will sorb water from its immediate surroundings, when available. At early times, this sorption is in direct proportion to the amount of hydration that has occurred.4 This method is based on the one developed by Geiker.5 The results are relevant to understanding the hydration behavior of cements. This method does not measure the bulk volume changes (autogenous shrinkage) associated with chemical shrinkage nor the cracking potential of concretes produced with the evaluated cement.
SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage.  
1.1.1 Procedure A, volumetric method.  
1.1.2 Procedure B, the density method.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage”.  
4.2 The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions.4 Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as standard. When combined standards are referenced, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).2  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
3.1 The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO or MgO, or both, when present in hydraulic cement.3
SCOPE
1.1 This test method covers determination of the expansion of a hardened cement paste when exposed to the autoclave conditions in this method.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see the section on Safety Precautions.

SIGNIFICANCE AND USE
3.1 The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO or MgO, or both, when present in hydraulic cement.3
SCOPE
1.1 This test method covers determination of the autoclave expansion of hydraulic cement by means of a test on a neat cement specimen.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see the section on Safety Precautions.

SIGNIFICANCE AND USE
4. Significance and UseNumerous properties of cementitious materials are controlled by their initial hydration rate. Examples include early-age strength development, heat release, and crack resistance. One direct and convenient measure of this initial hydration rate is provided by the measurement of the chemical shrinkage of the cement paste during its hydration. As cement hydrates, the hydration products occupy less volume than the initial reacting materials (cement and water). Due to this volume change, a hydrating cement paste will sorb water from its immediate surroundings, when available. At early times, this sorption is in direct proportion to the amount of hydration that has occurred.4 This method is based on the one developed by Geiker.5 The results are relevant to understanding the hydration behavior of cements. This method does not measure the bulk volume changes (autogenous shrinkage) associated with chemical shrinkage nor the cracking potential of concretes produced with the evaluated cement.
SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage .  
1.1.1 Procedure A, volumetric method.  
1.1.2 Procedure B, the density method.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)

SIGNIFICANCE AND USE
This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage”.
The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions. Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.
1.2 The values stated in SI units are to be regarded as standard. When combined standards are referenced, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).

SIGNIFICANCE AND USE
4.1 This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage”.  
4.2 The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions.4 Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as standard. When combined standards are referenced, the selection of measurement system is at the user’s discretion subject to the requirements of the referenced standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).2

SIGNIFICANCE AND USE
The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO, or MgO, or both, when present in hydraulic cement.
SCOPE
1.1 This test method covers determination of the autoclave expansion of hydraulic cement by means of a test on a neat cement specimen.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.For specific precaution statements, see the section on Safety Precautions.

SIGNIFICANCE AND USE
Numerous properties of cementitious materials are controlled by their initial hydration rate. Examples include early-age strength development, heat release, and crack resistance. One direct and convenient measure of this initial hydration rate is provided by the measurement of the chemical shrinkage of the cement paste during its hydration. As cement hydrates, the hydration products occupy less volume than the initial reacting materials (cement and water). Due to this volume change, a hydrating cement paste will sorb water from its immediate surroundings, when available. At early times, this sorption is in direct proportion to the amount of hydration that has occurred.4 This method is based on the one developed by Geiker.5 The results are relevant to understanding the hydration behavior of cements. This method does not measure the bulk volume changes (autogenous shrinkage) associated with chemical shrinkage nor the cracking potential of concretes produced with the evaluated cement.
SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage.
1.1.1 Procedure A, volumetric method.
1.1.2 Procedure B, the density method.
1.2 The values stated in SI units are to be regarded as the standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning-Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.)

SIGNIFICANCE AND USE
This test method establishes a selected set of conditions of temperature, relative humidity and rate of evaporation of the environment to which a mortar specimen of stated composition shall be subjected for a specified period of time during which its change in length is determined and designated “drying shrinkage”.
The drying shrinkage of mortar as determined by this test method has a linear relation to the drying shrinkage of concrete made with the same cement and exposed to the same drying conditions.4 Hence this test method may be used when it is desired to develop data on the effect of a hydraulic cement on the drying shrinkage of concrete made with that cement.
SCOPE
1.1 This test method determines the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.
1.2 The values stated in SI units are to be regarded as the standard. Values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning- Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).

SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage.
1.1.1 Procedure A, volumetric method.
1.1.2 Procedure B, the density method.
1.2 The values stated in SI units are to be regarded as the standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning-Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.)

SIGNIFICANCE AND USE
The autoclave expansion test provides an index of potential delayed expansion caused by the hydration of CaO, or MgO, or both, when present in hydraulic cement.3
SCOPE
1.1 This test method covers determination of the autoclave expansion of hydraulic cement by means of a test on a neat cement specimen.
1.2 The values stated in inch-pound units are to be regarded as the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.For specific precaution statements, see the section on Safety Precautions.

SCOPE
1.1 This test method measures the internal (absolute) volume change of hydraulic cement paste that results from the hydration of the cementitious materials. This volume change is known as chemical shrinkage.
1.1.1 Procedure A, volumetric method.
1.1.2 Procedure B, the density method.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.²)

SCOPE
1.1 This test method determines of the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as the standard. Values given in parentheses are for information only.  
1.3  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).

SCOPE
1.1 This test method determines of the change in length on drying of mortar bars containing hydraulic cement and graded standard sand.  
1.2 The values stated in SI units are to be regarded as the standard. Values given in parentheses are for information only.  
1.3  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure).

SCOPE
1.1 This test method covers determination of the autoclave expansion of portland cement by means of a test on a neat cement specimen.  
1.2 The values stated in inch-pound units are to be regarded as the standard.  
1.3  This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see the section on Safety Precautions.