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ASTM D1319-02a

(Test Method)

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

SCOPE
1.1 This test method covers the determination of hydrocarbon types over the concentration ranges from 5 to 99 volume % aromatics, 0.3 to 55 volume % olefins, and 1 to 95 volume % saturates in petroleum fractions that distill below 315°C. This test method may apply to concentrations outside these ranges, but the precision has not been determined. Samples containing dark-colored components that interfere in reading the chromatographic bands cannot be analyzed.
Note 1—The scope of this test method today is NOT to depentanize to reflect current practice. Results obtained from the analysis of samples containing significant levels of C5 and lighter hydrocarbons might be less accurate. The potential bias is not certain and may not be consistent. Prior versions of Test Method D 1319 have specified depentanization when samples contain any of the following: C3 or lighter hydrocarbons, more than 5 % C4 hydrocarbons, or more than 10 % C4 and C5 hydrocarbons. The results of this are still unclear and certainly controversial. In such a case, depentanization was done according to Test Method D 2001 followed by subsequent analysis of the depentanized sample by Test Method D 1319. A correction to the depentanized sample results was then required to place them on an as-received basis by using such method as Test Method D 2427 which determined the amounts of C5 minus hydrocarbons in the undepentanized sample.
1.2 This test method is intended for use with full boiling range products. Cooperative data have established that the precision statement does not apply to narrow boiling petroleum fractions near the 315°C limit. Such samples are not eluted properly, and results are erratic.
1.3 The applicability of this test method to products derived from fossil fuels other than petroleum, such as coal, shale, or tar sands, has not been determined, and the precision statement may or may not apply to such products.
1.4 The precision statement for this test method has been determined with unleaded fuels that do not contain oxygenated blending components. It may or may not apply to automotive gasolines containing lead antiknock mixtures or oxygenated gasoline blending components, or both.
1.5 The oxygenated blending components, methanol, ethanol, methyl-tert-butylether (MTBE), methyl- tert-amylmethyl (TAME), and ethyl-tert-butylether (ETBE), do not interfere with the determination of hydrocarbon types at concentrations normally found in commercial blends. These oxygenated components are not detected since they elute with the alcohol desorbent. Other oxygenated compounds shall be individually verified. When samples containing oxygenated blending components are analyzed, correct the results to a total-sample basis.
1.6 The values stated in SI units are to be regarded as standard.
Note 2—For the determination of olefins below 0.3 volume %, other test methods are available, such as Test Method D 2710.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7, 8.1, and 10.5.

General Information

Status
Historical
Publication Date
09-Apr-2002
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0C - Liquid Chromatography
Current Stage
Ref Project

Relations

Replaces
ASTM D1319-02 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
Effective Date
10-Apr-2002
Replaced By
ASTM D1319-03 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
Effective Date
01-Nov-2003
Referred By
ASTM D6591-19 - Standard Test Method for Determination of Aromatic Hydrocarbon Types in Middle Distillates—High Performance Liquid Chromatography Method with Refractive Index Detection
Effective Date
10-Apr-2002
Referred By
ASTM D8114-23 - Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIE Spark Ignition
Effective Date
10-Apr-2002
Referred By
ASTM D7566-22a - Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons
Effective Date
10-Apr-2002
Referred By
ASTM D8305-19 - Standard Test Method for The Determination of Total Aromatic Hydrocarbons and Total Polynuclear Aromatic Hydrocarbons in Aviation Turbine Fuels and other Kerosene Range Fuels by Supercritical Fluid Chromatography
Effective Date
10-Apr-2002
Referred By
ASTM D6201-19a - Standard Test Method for Dynamometer Evaluation of Unleaded Spark-Ignition Engine Fuel for Intake Valve Deposit Formation
Effective Date
10-Apr-2002
Referred By
ASTM D2425-21 - Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
Effective Date
10-Apr-2002
Referred By
ASTM D975-23 - Standard Specification for Diesel Fuel
Effective Date
10-Apr-2002
Referred By
ASTM D5186-22 - Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
Effective Date
10-Apr-2002
Referred By
ASTM D6729-20 - Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100 Metre Capillary High Resolution Gas Chromatography
Effective Date
10-Apr-2002
Referred By
ASTM D4054-23 - Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives
Effective Date
10-Apr-2002
Referred By
ASTM D8226-21ae1 - Standard Test Method for Measurement of Effects of Automotive Engine Oils on Fuel Economy of Passenger Cars and Light-Duty Trucks in Sequence VIF Spark Ignition Engine<rangeref></rangeref >
Effective Date
10-Apr-2002
Referred By
ASTM D8275-22 - Standard Specification for Gasoline-like Test Fuel for Compression-Ignition Engines
Effective Date
10-Apr-2002
Referred By
ASTM D8048-21ae1 - Standard Test Method for Evaluation of Diesel Engine Oils in T-13 Diesel Engine
Effective Date
10-Apr-2002

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ASTM D1319-02a - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator AdsorptionASTM D1319-02a - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
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ASTM D1319-02a - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 1319 – 02a
Designation: 156/97
Standard Test Method for
Hydrocarbon Types in Liquid Petroleum Products by
1
Fluorescent Indicator Adsorption
This standard is issued under the fixed designation D 1319; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This test method has been approved by the sponsoring committees and accepted by the cooperating societies in accordance with
established procedures.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope * tar sands, has not been determined, and the precision statement
may or may not apply to such products.
1.1 This test method covers the determination of hydrocar-
1.4 The precision statement for this test method has been
bon types over the concentration ranges from 5 to 99 volume %
determined with unleaded fuels that do not contain oxygenated
aromatics, 0.3 to 55 volume % olefins, and 1 to 95 volume %
blending components. It may or may not apply to automotive
saturates in petroleum fractions that distill below 315°C. This
gasolines containing lead antiknock mixtures or oxygenated
test method may apply to concentrations outside these ranges,
gasoline blending components, or both.
but the precision has not been determined. Samples containing
1.5 The oxygenated blending components, methanol, etha-
dark-colored components that interfere in reading the chro-
nol, methyl-tert-butylether (MTBE), tert-amylmethylether
matographic bands cannot be analyzed.
(TAME), and ethyl-tert-butylether (ETBE), do not interfere
NOTE 1—The scope of this test method today is NOT to depentanize to
with the determination of hydrocarbon types at concentrations
reflect current practice. Results obtained from the analysis of samples
normally found in commercial blends. These oxygenated
containing significant levels of C and lighter hydrocarbons might be less
5
components are not detected since they elute with the alcohol
accurate. The potential bias is not certain and may not be consistent. Prior
desorbent. Other oxygenated compounds shall be individually
versions of Test Method D 1319 have specified depentanization when
verified. When samples containing oxygenated blending com-
samples contain any of the following: C or lighter hydrocarbons, more
3
than 5 % C hydrocarbons, or more than 10 % C and C hydrocarbons.
ponents are analyzed, correct the results to a total-sample basis.
4 4 5
The results of this are still unclear and certainly controversial. In such a
1.6 The values stated in SI units are to be regarded as
case, depentanization was done according to Test Method D 2001 fol-
standard.
lowed by subsequent analysis of the depentanized sample by Test Method
D 1319. A correction to the depentanized sample results was then required NOTE 2—For the determination of olefins below 0.3 volume %, other
to place them on an as-received basis by using such method as Test test methods are available, such as Test Method D 2710.
Method D 2427 which determined the amounts of C minus hydrocarbons
5
1.7 This standard does not purport to address all of the
in the undepentanized sample.
safety concerns, if any, associated with its use. It is the
1.2 This test method is intended for use with full boiling
responsibility of the user of this standard to establish appro-
range products. Cooperative data have established that the
priate safety and health practices and determine the applica-
precision statement does not apply to narrow boiling petroleum
bility of regulatory limitations prior to use. For specific hazard
fractions near the 315°C limit. Such samples are not eluted
statements, see Section 7, 8.1, and 10.5.
properly, and results are erratic.
1.3 The applicability of this test method to products derived 2. Referenced Documents
from fossil fuels other than petroleum, such as coal, shale, or
2.1 ASTM Standards:
D 86 Test Method for Distillation of Petroleum Products at
2
Atmospheric Pressure
2
1
This test method is under the jurisdiction of ASTM Committee D02 on D 1655 Specification for Aviation Turbine Fuels
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D 2001 Test Method for Depentanization of Gasoline and
D02.04 on Hydrocarbon Analysis.
2
Naphthas
In the IP, this test method is under the jurisdiction of the Standardization
Committee.
Current edition approved April 10, 2002. Published July 2002. Originally
published as D 1319–54T. Last previous edition D 1319–02.
2
Annual Book of ASTM Standards, Vol 05.01.
*A Summary of Changes section appears at the end of this standard.
Copyright © AS
...

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SCOPE
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Note 2: Oil tubes and apparatus used in this test method have traditionally been marked in inches, (the tube is required to be etched with 1/8 in. divisions.) The Saybolt Color Numbers are aligned with inch, 1/2 in., 1/4 in., and 1/8 in. changes in the depth of oil. These fractional inch changes do not readily correspond to SI equivalents and in view of the preponderance of apparatus already in use and marked in inches, the inch/pound unit is regarded as the standard. However the test method does use SI units of length when the length is not directly related to divisions on the oil tube and Saybolt Color Numbers. The test method uses SI units for temperature.  
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Standard Practice for Calculating Viscosity of a Blend of Petroleum Products

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5.1 Predicting the viscosity of a blend of components is a common problem. Both the Wright Blending Method and the ASTM Blending Method, described in this practice, may be used to solve this problem.  
5.2 The inverse problem, predicating the required blend fractions of components to meet a specified viscosity at a given temperature may also be solved using either the Inverse Wright Blending Method or the Inverse ASTM Blending Method.  
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5.4 Although this practice was developed using kinematic viscosity and volume fraction of each component, the dynamic viscosity or mass fraction, or both, may be used instead with minimal error if the densities of the components do not differ greatly. For fuel blends, it was found that viscosity blending using mass fractions gave more accurate results. For base stock blends, there was no significant difference between mass fraction and volume fraction calculations.  
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SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
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Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
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5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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