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ASTM D1319-03

(Test Method)

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption

SCOPE
1.1 This test method covers the determination of hydrocarbon types over the concentration ranges from 5 to 99 volume % aromatics, 0.3 to 55 volume % olefins, and 1 to 95 volume % saturates in petroleum fractions that distill below 315°C. This test method may apply to concentrations outside these ranges, but the precision has not been determined. Samples containing dark-colored components that interfere in reading the chromatographic bands cannot be analyzed.
1.2 This test method is intended for use with full boiling range products. Cooperative data have established that the precision statement does not apply to narrow boiling petroleum fractions near the 315°C limit. Such samples are not eluted properly, and results are erratic.
1.3 The applicability of this test method to products derived from fossil fuels other than petroleum, such as coal, shale, or tar sands, has not been determined, and the precision statement may or may not apply to such products.
1.4 This test method has two precision statements depicted in tables. The first table is applicable to unleaded fuels that do not contain oxygenated blending components. It may or may not apply to automotive gasolines containing lead antiknock mixtures. The second table is applicable to oxygenate blended (for example, MTBE, ethanol) automotive spark ignition fuel samples with a concentration range of 13-40 volume percent aromatics, 4-33 volume percent olefins, and 45-68 volume percent saturates.
1.5 The oxygenated blending components, methanol, ethanol, methyl-tert-butylether (MTBE),  tert-amylmethylether (TAME), and ethyl-tert-butylether (ETBE), do not interfere with the determination of hydrocarbon types at concentrations normally found in commercial blends. These oxygenated components are not detected since they elute with the alcohol desorbent. Other oxygenated compounds shall be individually verified. When samples containing oxygenated blending components are analyzed, correct the results to a total-sample basis.
1.6 The values stated in SI units are to be regarded as standard.
Note 1—For the determination of olefins below 0.3 volume %, other test methods are available, such as Test Method D 2710.
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7, 8.1, and 10.5.

General Information

Status
Historical
Publication Date
31-Oct-2003
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.04.0C - Liquid Chromatography
Current Stage
Ref Project

Relations

Replaces
ASTM D1319-02a - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
Effective Date
01-Nov-2003
Replaced By
ASTM D1319-03e1 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
Effective Date
01-Nov-2003
Referred By
ASTM D6729-20 - Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100 Metre Capillary High Resolution Gas Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D2425-21 - Standard Test Method for Hydrocarbon Types in Middle Distillates by Mass Spectrometry
Effective Date
01-Nov-2003
Referred By
ASTM D7484-23 - Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine
Effective Date
01-Nov-2003
Referred By
ASTM D7320-18e1 - Standard Test Method for Evaluation of Automotive Engine Oils in the Sequence IIIG, Spark-Ignition Engine
Effective Date
01-Nov-2003
Referred By
ASTM D8321-22 - Standard Practice for Development and Validation of Multivariate Analyses for Use in Predicting Properties of Petroleum Products, Liquid Fuels, and Lubricants based on Spectroscopic Measurements
Effective Date
01-Nov-2003
Referred By
ASTM D5966-22 - Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine
Effective Date
01-Nov-2003
Referred By
ASTM D3343-22 - Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels
Effective Date
01-Nov-2003
Referred By
ASTM D3831-22 - Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy
Effective Date
01-Nov-2003
Referred By
ASTM D6593-18e1 - Standard Test Method for Evaluation of Automotive Engine Oils for Inhibition of Deposit Formation in a Spark-Ignition Internal Combustion Engine Fueled with Gasoline and Operated Under Low-Temperature, Light-Duty Conditions
Effective Date
01-Nov-2003
Referred By
ASTM D8275-22 - Standard Specification for Gasoline-like Test Fuel for Compression-Ignition Engines
Effective Date
01-Nov-2003
Referred By
ASTM D7467-20a - Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20)
Effective Date
01-Nov-2003
Referred By
ASTM D8305-19 - Standard Test Method for The Determination of Total Aromatic Hydrocarbons and Total Polynuclear Aromatic Hydrocarbons in Aviation Turbine Fuels and other Kerosene Range Fuels by Supercritical Fluid Chromatography
Effective Date
01-Nov-2003
Referred By
ASTM D6618-23 - Standard Test Method for Evaluation of Engine Oils in Diesel Four-Stroke Cycle Supercharged 1M-PC Single Cylinder Oil Test Engine
Effective Date
01-Nov-2003

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ASTM D1319-03 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator AdsorptionASTM D1319-03 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
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ASTM D1319-03 - Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
An American National Standard
Designation: D 1319 – 03
Designation: 156/97
Standard Test Method for
Hydrocarbon Types in Liquid Petroleum Products by
1
Fluorescent Indicator Adsorption
This standard is issued under the fixed designation D 1319; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope* with the determination of hydrocarbon types at concentrations
normally found in commercial blends. These oxygenated
1.1 This test method covers the determination of hydrocar-
components are not detected since they elute with the alcohol
bontypesovertheconcentrationrangesfrom5to99volume %
desorbent. Other oxygenated compounds shall be individually
aromatics, 0.3 to 55 volume % olefins, and 1 to 95 volume %
verified. When samples containing oxygenated blending com-
saturates in petroleum fractions that distill below 315°C. This
ponentsareanalyzed,correcttheresultstoatotal-samplebasis.
test method may apply to concentrations outside these ranges,
1.6 The values stated in SI units are to be regarded as
but the precision has not been determined. Samples containing
standard.
dark-colored components that interfere in reading the chro-
matographic bands cannot be analyzed.
NOTE 1—For the determination of olefins below 0.3 volume %, other
1.2 This test method is intended for use with full boiling
test methods are available, such as Test Method D 2710.
range products. Cooperative data have established that the
1.7 This standard does not purport to address all of the
precisionstatementdoesnotapplytonarrowboilingpetroleum
safety concerns, if any, associated with its use. It is the
fractions near the 315°C limit. Such samples are not eluted
responsibility of the user of this standard to establish appro-
properly, and results are erratic.
priate safety and health practices and determine the applica-
1.3 The applicability of this test method to products derived
bility of regulatory limitations prior to use. For specific hazard
from fossil fuels other than petroleum, such as coal, shale, or
statements, see Section 7, 8.1, and 10.5.
tar sands, has not been determined, and the precision statement
may or may not apply to such products. 2. Referenced Documents
1.4 This test method has two precision statements depicted 2
2.1 ASTM Standards:
in tables. The first table is applicable to unleaded fuels that do
D 86 Test Method for Distillation of Petroleum Products at
not contain oxygenated blending components. It may or may
Atmospheric Pressure
not apply to automotive gasolines containing lead antiknock
D 1655 Specification for Aviation Turbine Fuels
mixtures. The second table is applicable to oxygenate blended
D 2710 Test Method for Bromine Index of Petroleum Hy-
(for example, MTBE, ethanol) automotive spark ignition fuel
drocarbons by Electrometric Titration
samples with a concentration range of 13–40 volume percent
D 3663 Test Method for Surface Area of Catalysts and
aromatics, 4–33 volume percent olefins, and 45–68 volume
Catalyst Carriers
percent saturates.
D 4057 Practice for Manual Sampling of Petroleum and
1.5 The oxygenated blending components, methanol, etha-
Petroleum Products
nol, methyl-tert-butylether (MTBE), tert-amylmethylether
D 4815 Test Method for Determination of MTBE, ETBE,
(TAME), and ethyl-tert-butylether (ETBE), do not interfere
TAME, DIPE, tertiary-Amyl Alcohol and C to C Alco-
1 4
hols in Gasoline by Gas Chromatography
D 5599 Test Method for Determination of Oxygenates in
1
This test method is under the jurisdiction of ASTM Committee D02 on
Gasoline by Gas Chromatography and Oxygen Selective
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D02.04 on Hydrocarbon Analysis.
In the IP, this test method is under the jurisdiction of the Standardization
2
Committee. This test method has been approved by the sponsoring committees and
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
accepted by the cooperating societies in accordance with established procedures. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved Nov. 1, 2003. Published January 2004. Originally Standards volume information, refer to the standard’s Document Summary page on
approved in 1954. Last previous edition approved in 2002 as D 1319–02a. the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
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Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

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5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
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ASTM
ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
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  • Standard
    35 pages
    English language
    sale 15% off