Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition

SCOPE
1.1 This practice covers the sampling of all grades of steel, both cast and wrought, and all types (grades) of cast irons and blast furnace iron for chemical and spectrochemical determination of composition. This practice is similar to ISO 14284.
1.2 This practice is divided into the following sections. SectionsRequirements for Sampling and Sample Preparation6General6.1Sample6.2Selection of a Sample6.3Preparation of a Sample6.4Liquid Iron for Steelmaking and Pig Iron Production7General7.1Spoon Sampling7.2Probe Sampling7.3Preparation of a Sample for Analysis7.4Liquid Iron for Cast Iron Production8General8.1Spoon Sampling8.2Probe Sampling8.3Preparation of a Sample for Analysis8.4Sampling and Sample Preparation for the Determination ofOxygen and Hydrogen8.5Liquid Steel for Steel Production9General9.1Probe Sampling9.2Spoon Sampling9.3Preparation of a Sample for Analysis8.4Sampling and Sample Preparation for the Determinationof Oxygen9.5Sampling and Sample Preparation for the Determinationof Hydrogen9.6Pig Irons10General10.1Increment Sampling10.2Preparation of a Sample for Analysis10.3Cast Iron Products11General11.1Sampling and Sample Preparation11.2Steel Products12General12.1Selection of a Laboratory Sample or a Sample forAnalysis from a Cast Product12.2Selection of a Laboratory Sample or a Sample forAnalysis from a Wrought Product12.3Preparation of a Sample for Analysis12.4Sampling of Leaded Steel12.5Sampling and Sample Preparation for the Determinationof Oxygen12.6Sampling and Sample Preparation for the Determinationof Hydrogen12.7Keywords13 AnnexesSampling Probes for Use with Liquid Iron and SteelAnnex A1Sampling Probes for Use with Liquid Steel for theAnnex A2Determination of Hydrogen
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.4 For specific precautions, see 6.4.3.5, 9.4.4.3, and 12.5.1.1 as well as Section 5.

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ASTM E1806-96(2001) - Standard Practice for Sampling Steel and Iron for Determination of Chemical Composition
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E 1806 – 96 (Reapproved 2001)
Standard Practice for
Sampling Steel and Iron for Determination of Chemical
1
Composition
This standard is issued under the fixed designation E 1806; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope
Selection of a Laboratory Sample or a Sample for 12.2
Analysis from a Cast Product
1.1 This practice covers the sampling of all grades of steel,
Selection of a Laboratory Sample or a Sample for 12.3
both cast and wrought, and all types (grades) of cast irons and
Analysis from a Wrought Product
Preparation of a Sample forAnalysis 12.4
blast furnace iron for chemical and spectrochemical determi-
Sampling of Leaded Steel 12.5
nation of composition. This practice is similar to ISO 14284.
Sampling and Sample Preparation for the Determination 12.6
1.2 This practice is divided into the following sections.
of Oxygen
Sections
Sampling and Sample Preparation for the Determination 12.7
Requirements for Sampling and Sample Preparation 6
of Hydrogen
General 6.1
Sample 6.2
Keywords 13
Selection of a Sample 6.3
Preparation of a Sample 6.4
Annexes
Sampling Probes for Use with Liquid Iron and Steel AnnexA1
Liquid Iron for Steelmaking and Pig Iron Production 7
Sampling Probes for Use with Liquid Steel for the AnnexA2
General 7.1
Determination of Hydrogen
Spoon Sampling 7.2
Probe Sampling 7.3
1.3 This standard does not purport to address all of the
Preparation of a Sample forAnalysis 7.4
safety concerns, if any, associated with its use. It is the
Liquid Iron for Cast Iron Production 8
responsibility of the user of this standard to establish appro-
General 8.1
priate safety and health practices and determine the applica-
Spoon Sampling 8.2
bility of regulatory limitations prior to use.
Probe Sampling 8.3
Preparation of a Sample forAnalysis 8.4
1.4 For specific precautions, see 6.4.3.5, 9.4.4.3, and
Sampling and Sample Preparation for the Determination of 8.5
12.5.1.1 as well as Section 5.
Oxygen and Hydrogen
2. Referenced Documents
Liquid Steel for Steel Production 9
General 9.1 2
2.1 ASTM Standards:
Probe Sampling 9.2
A 48 Specification for Gray Iron Castings
Spoon Sampling 9.3
Preparation of a Sample forAnalysis 9.4
A 751 Test Methods, Practices, and Definitions for Chemi-
Sampling and Sample Preparation for the Determination 9.5
cal Analysis of Steel Products
of Oxygen
E 135 Terminology Relating to Analytical Chemistry for
Sampling and Sample Preparation for the Determination 9.6
of Hydrogen
Metals, Ores, and Related Materials
E 415 Test Method for Optical Emission Vacuum Spectro-
Pig Irons 10
metric Analysis of Carbon and Low-Alloy Steel
General 10.1
Increment Sampling 10.2
E 1010 Practice for Preparation of Disk Specimens of Steel
Preparation of a Sample forAnalysis 10.3
and Iron for Spectrochemical Analysis by Remelting
E 1087 Practice for Sampling Molten Steel from a Ladle
Cast Iron Products 11
General 11.1
Using an Immersion Sampler to Produce a Sample for
Sampling and Sample Preparation 11.2
3
Spectrochemical Analysis
2.2 ISO Documents:
Steel Products 12
General 12.1
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This practice is under the jurisdiction of ASTM Committee E01 on Analytical contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Chemistry for Metals, Ores, and Related Materials and is the direct responsibility of Standards volume information, refer to the standard’s Document Summary page on
Subcommittee E01.01 on Iron, Steel, and Ferroalloys. the ASTM website.
3
Current edition approved April 10, 1996. Published June 1996. Withdrawn.
Copyright ©ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA19428-2959, United States.
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E 1806 – 96 (2001)
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ISO 9147 Pig irons–Definition and classification 3.2.18 wrought product, n—item of steel which has been
ISO 14284 Steel and iron—Sampling and preparation of subject to deformation by rolling, drawing, forging, or some
4
samples for the determination of chemical composition other method, for example, a bar, billet, plate, strip, tube, or
wire.
3. Terminology
3.1 Definitions—For definitions of terms in this practice, 4. Significance and Use
refer to Terminology E 135.
4.1 This practice covers all aspects of sampling and prepar-
3.2 Definitions of Terms Specific to This Standard:
ing steel and iron for chemical analysis as defined in Test
3.2.1 cast product, n—item of iron or steel which has not
Methods, Practices, and Definitions A 751 and Specification
been subject to deformation, for example, a
...

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