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ASTM C1240-20

(Specification)

Standard Specification for Silica Fume Used in Cementitious Mixtures

Standard Specification for Silica Fume Used in Cementitious Mixtures

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The units stated in SI are to be regarded as the standard. No other units of measurement are included in this standard.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 – 19, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
14-Jan-2020
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C09 - Concrete and Concrete Aggregates
Drafting Committee
C09.24 - Supplementary Cementitious Materials
Current Stage
Ref Project

Relations

Refers
ASTM C185-20 - Standard Test Method for Air Content of Hydraulic Cement Mortar
Effective Date
01-Apr-2020
Refers
ASTM C219-20a - Standard Terminology Relating to Hydraulic and Other Inorganic Cements
Effective Date
01-Aug-2020
Refers
ASTM C219-20 - Standard Terminology Relating to Hydraulic and Other Inorganic Cements
Effective Date
01-Apr-2020

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ASTM C1240-20 - Standard Specification for Silica Fume Used in Cementitious MixturesASTM C1240-20 - Standard Specification for Silica Fume Used in Cementitious Mixtures
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REDLINE ASTM C1240-20 - Standard Specification for Silica Fume Used in Cementitious MixturesREDLINE ASTM C1240-20 - Standard Specification for Silica Fume Used in Cementitious Mixtures
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation:C1240 −20
Standard Specification for
1
Silica Fume Used in Cementitious Mixtures
This standard is issued under the fixed designation C1240; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* C114Test Methods for Chemical Analysis of Hydraulic
Cement
1.1 This specification covers silica fume for use in concrete
C125Terminology Relating to Concrete and Concrete Ag-
and other systems containing hydraulic cement.
gregates
1.2 In the cases of slurried or densified silica fume, perform
C135Test Method for True Specific Gravity of Refractory
thetestsontherawsilicafumefromwhichtheseproductshave
Materials by Water Immersion
been made.
C183/C183MPractice for Sampling and the Amount of
Testing of Hydraulic Cement
1.3 TheunitsstatedinSIaretoberegardedasthestandard.
No other units of measurement are included in this standard. C185Test Method for Air Content of Hydraulic Cement
Mortar
1.4 The following safety hazards caveat pertains only to the
C219Terminology Relating to Hydraulic and Other Inor-
test methods portions, Sections10–19, of this specification:
ganic Cements
This standard does not purport to address all of the safety
C311/C311MTest Methods for Sampling and Testing Fly
concerns, if any, associated with its use. It is the responsibility
Ash or Natural Pozzolans for Use in Portland-Cement
of the user of this standard to establish appropriate safety,
Concrete
health, and environmental practices and determine the appli-
C430Test Method for Fineness of Hydraulic Cement by the
cabilityofregulatorylimitationspriortouse.Readthematerial
45-µm (No. 325) Sieve
safety data sheets for materials used.
C441/C441MTestMethodforEffectivenessofPozzolansor
1.5 The text of this standard references notes and footnotes
Ground Blast-Furnace Slag in Preventing Excessive Ex-
that provide explanatory information. These notes and foot-
pansion of Concrete Due to the Alkali-Silica Reaction
notes (excluding those in tables) shall not be considered as
C494/C494MSpecification for Chemical Admixtures for
requirements of this standard.
Concrete
1.6 This international standard was developed in accor-
C604Test Method for True Specific Gravity of Refractory
dance with internationally recognized principles on standard-
Materials by Gas-Comparison Pycnometer
ization established in the Decision on Principles for the
C670Practice for Preparing Precision and Bias Statements
Development of International Standards, Guides and Recom-
for Test Methods for Construction Materials
mendations issued by the World Trade Organization Technical
C1005Specification for Reference Masses and Devices for
Barriers to Trade (TBT) Committee.
Determining Mass and Volume for Use in the Physical
Testing of Hydraulic Cements
2. Referenced Documents
C1012/C1012M Test Method for Length Change of
2
2.1 ASTM Standards: Hydraulic-Cement Mortars Exposed to a Sulfate Solution
C109/C109MTest Method for Compressive Strength of
C1069Test Method for Specific SurfaceArea ofAlumina or
Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube Quartz by Nitrogen Adsorption
Specimens)
C1157/C1157MPerformance Specification for Hydraulic
Cement
C1437Test Method for Flow of Hydraulic Cement Mortar
1
This specification is under the jurisdiction of ASTM Committee C09 on
3. Terminology
ConcreteandConcreteAggregates andisthedirectresponsibilityofSubcommittee
C09.24 on Supplementary Cementitious Materials.
3.1 Definitions:
Current edition approved Jan. 15, 2020. Published March 2020. Originally
3.1.1 Fordefinitionsoftermsusedinthisspecification,refer
approved in 1993. Last previous edition approved in 2015 as C1240–15. DOI:
10.1520/C1240-20.
to Terminology C125 and Terminology C219.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
3.2 Definitions of Terms Specific to This Standard:
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3.2.1 silica fume, densified, n—silica fume processed to
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. increase bulk density to facilitate handling and shipping.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1240−20
TABLE 2 Physical Requirements
3.2.2 silica fume, undensified, n—silica fume in its raw, as
produced or as c
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1240 − 15 C1240 − 20
Standard Specification for
1
Silica Fume Used in Cementitious Mixtures
This standard is issued under the fixed designation C1240; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Scope*
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have
been made.
1.3 The units stated in SI are to be regarded as the standard. No other units of measurement are included in this standard.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 – 19, of this specification: This
standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user
of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the applicability
of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes
(excluding those in tables) shall not be considered as requirements of this standard.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C109/C109M Test Method for Compressive Strength of Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube Specimens)
C114 Test Methods for Chemical Analysis of Hydraulic Cement
C125 Terminology Relating to Concrete and Concrete Aggregates
C135 Test Method for True Specific Gravity of Refractory Materials by Water Immersion
C183C183/C183M Practice for Sampling and the Amount of Testing of Hydraulic Cement
C185 Test Method for Air Content of Hydraulic Cement Mortar
C219 Terminology Relating to Hydraulic and Other Inorganic Cements
C311/C311M Test Methods for Sampling and Testing Fly Ash or Natural Pozzolans for Use in Portland-Cement Concrete
C430 Test Method for Fineness of Hydraulic Cement by the 45-μm (No. 325) Sieve
C441/C441M Test Method for Effectiveness of Pozzolans or Ground Blast-Furnace Slag in Preventing Excessive Expansion of
Concrete Due to the Alkali-Silica Reaction
C494/C494M Specification for Chemical Admixtures for Concrete
C604 Test Method for True Specific Gravity of Refractory Materials by Gas-Comparison Pycnometer
C670 Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
C1005 Specification for Reference Masses and Devices for Determining Mass and Volume for Use in the Physical Testing of
Hydraulic Cements
C1012/C1012M Test Method for Length Change of Hydraulic-Cement Mortars Exposed to a Sulfate Solution
C1069 Test Method for Specific Surface Area of Alumina or Quartz by Nitrogen Adsorption
C1157/C1157M Performance Specification for Hydraulic Cement
C1437 Test Method for Flow of Hydraulic Cement Mortar
1
This specification is under the jurisdiction of ASTM Committee C09 on Concrete and Concrete Aggregates and is the direct responsibility of Subcommittee C09.24 on
Supplementary Cementitious Materials.
Current edition approved June 15, 2015Jan. 15, 2020. Published September 2015March 2020. Originally approved in 1993. Last previous edition approved in 20142015
as C1240 – 14.C1240 – 15. DOI: 10.1520/C1240-15.10.1520/C1240-20.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1240 − 20
3. Terminology
3.1 Definitions:
3.1.1 For definitions of terms used in this specification, refer to Terminology C125 and Termi
...

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4.1 This test method is intended to provide a means of assessing the ability of a hydraulic-cement grout to retain a stable volume during the stipulated testing period of 28 days, provided that the tendency to change height does not include the effects of drying caused by evaporation, uptake of moisture, carbonation, or exposure to temperatures outside the range 23.0 °C ± 2.0 °C [73 °F ± 3.5 °F] (Note 2). An exception is made when the options described in the section on test conditions are exercised.  
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SIGNIFICANCE AND USE
4.1 This test method provides a means for comparing the relative shrinkage or expansion of cementitious mixtures. It is particularly applicable to grouting, patching, and form-filling operations where the objective is to completely fill a cavity or other defined space with a freshly mixed cementitious mixture that will continue to fill the same space at time of hardening. It would be appropriate to use this test method as a basis for prescribing mixtures having restricted or specified volume change before the mixture becomes hard.  
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1.1 This test method covers the determination of change in height of cylindrical specimens from the time of molding until the mixture is hard.  
1.2 This test method covers height change measurements at early ages for cementitious mixtures of paste, grout, mortar, and concrete.  
1.3 This test method is intended for determination of changes in height that occur from the time of placement until the specimen is fully hard. These include shrinkage or expansion due to hydration, settlement, evaporation, and other physical and chemical effects.  
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5.1 This test method is of significance in making a final determination of the acceptability of fine aggregates with respect to the requirements of Specification C33/C33M concerning organic impurities.  
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ABSTRACT
This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and mortars. Concrete mixtures covered by this specification includes high-early strength concrete, normal strength concrete, normal weight concrete, high-strength mortar, and mortars for unit masonry. The purchaser shall specify the material desired as concrete, high strength mortar, or mortar for use with unit masonry, and the respective physical requirements. Materials used as ingredients in packaged, dry, combined materials for mortar and concrete shall be composed of aggregates, air-entraining admixtures, blended cement, chemical admixtures, fly ash, ground granulated blast-furnace slag, hydrated lime, latex and powder polymer modifiers, masonry cement, mortar cement, Portland cement, and silica fume. All aggregates shall be dried, without disintegration, to specific moisture content The proportions of cementitious material and aggregate shall be such that the strength requirements will be met. Packaged, dry, combined materials for concrete, high strength mortar and mortar for use with unit masonry shall conform to the respective compressive strength requirements. Scales conforming to the standards will be used for sampling concretes from a single batch using a sufficient quantity. A slump test will be performed to check if additional water is required. In sampling mortar, the contents of an entire package of dry, combined material for mortar for unit masonry or for concrete mortar shall be used. Mortar mixing equipment, which must be provided with a bowl positioning adapter, shall be used to ensure clearance for the largest size aggregate in the mix being tested. The specification includes the following testing methods for mortar: compressive strength, density and yield, air content, and water retention.
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1.1 This guide provides information on how to compare the relative performance and potential incompatibility of combinations of concrete-making materials. Performance tests on fresh and early-age properties of mortar mixtures can be useful indicators of concrete performance using similar materials. The performance tests described in this guide include mortar-slump, mortar spread, mortar-workability retention, early stiffening of mortar, time of setting, air entrainment, and hydration kinetics.  
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1.1 This practice describes the apparatus and procedure for measuring relative differences in hydration kinetics of hydraulic cementitious mixtures, either in paste or mortar (see Note 1), including those containing admixtures, various supplementary cementitious materials (SCM), and other fine materials by measuring the thermal power using an isothermal calorimeter.
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ASTM C1260-22(Test Method)
Standard Test Method for Potential Alkali Reactivity of Aggregates (Mortar-Bar Method)

SIGNIFICANCE AND USE
4.1 This test method provides a means of detecting the potential of an aggregate intended for use in concrete for undergoing alkali-silica reaction resulting in potentially deleterious internal expansion. It is based on the NBRI Accelerated Test Method (1-4).3 It is especially useful for aggregates that react slowly or produce expansion late in the reaction. However, it does not evaluate combinations of aggregates with cementitious materials nor are the test conditions representative of those encountered by concrete in service.  
4.2 Because the specimens are exposed to a NaOH solution, the alkali content of the cement is not a significant factor in affecting expansions.  
4.3 Results of tests conducted on an aggregate as described herein should form a part of the basis for a decision as to whether precautions should be taken against excessive expansion due to alkali-silica reaction. Refer to Guide C1778 for the interpretation of the test results from Test Method C1260.
SCOPE
1.1 This test method permits detection, within 16 days, of the potential for deleterious alkali-silica reaction of aggregate in mortar bars.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. When this test method refers to combined-unit standards, the selection of the measurement systems is at the user’s discretion.  
1.3 The text of this test method refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this test method.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. A specific precautionary statement is given in the section on Reagents.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1709-22(Guide)
Standard Guide for Evaluation of Alternative Supplementary Cementitious Materials (ASCM) for Use in Concrete

SIGNIFICANCE AND USE
4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
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1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1753/C1753M-21a(Practice)
Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
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1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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ASTM
ASTM C1697-21(Specification)
Standard Specification for Blended Supplementary Cementitious Materials

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1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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