C09.24 - Supplementary Cementitious Materials

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether coal ash or natural pozzolan results in an acceptable level of strength development when used in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the coal ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a coal ash or natural pozzolan in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing coal ash and raw or calcined pozzolans for use in concrete.  
1.2 The procedures appear in the following order:    
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide,
calcium oxide, magnesium oxide, sulfur
trioxide, sodium oxide and potassium
oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21 – 23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index  
27 – 30  
Water requirement  
31  
Effectiveness of Coal Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Coal Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
Note 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal ash and raw or calcined natural pozzolan, for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to coal ash or natural pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a coal ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.    
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SCOPE
1.1 This specification covers ground-glass pozzolans for use in concrete where pozzolanic action is desired. This specification applies to ground glass from sources that consist of container glass, plate glass, or E-glass.  
1.2 The standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. If required results obtained from another standard are not reported in the same system of units as used by this standard, it is permitted to convert those results using the conversion factors found in the SI Quick Reference Guide.2  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
5.1 These test methods are used to assess the chemical (pozzolanic or hydraulic) reactivity of SCMs over a curing time of 7 days. The results of these test methods can be used to estimate the potential contribution of a SCM to the development of strength, or other properties such as lower permeability, when used with portland cement. However, the test results are not a substitute for direct measurement of the same properties of concrete made with that SCM.  
5.2 The calcium hydroxide, calcium carbonate, potassium sulfate, and potassium hydroxide are combined in proportions to provide a paste where the dissolved ions from these components simulate the pore solution in a portland cement system.  
5.3 The pastes are cured at 40 °C to accelerate the rate of reaction of slowly reactive SCMs.  
5.4 These test methods allow for the direct measurement of the hydraulic or pozzolanic reactivity of a potential SCM. These test methods are also suitable for screening purposes in the development and research of SCMs for use in portland cement-based systems. Furthermore, these test methods may be used in manufacturing control of portland cement-based products for assessing the hydraulic or pozzolanic reactivity of a SCM component.  
5.5 These test methods are based on the work by Avet et al.4 and are a result of the work of RILEM Technical Committee 267 – Tests for Reactivity of Supplementary Cementitious Materials.5 The test methods are based on established correlations between strength development and evolution of heat and binding of water for SCMs covered by Specifications C618, C989/C989M, and C1240, and by Guide C1709. For other alternative SCMs, the validity of such correlations has not been established.  
5.6 There is no requirement to use Method A and Method B for a given application. In many instances the choice is based on the user’s determination of available equipment. Method A can also provide an indication of rate of reactivity because measurements are taken con...
SCOPE
1.1 These two alternative test methods are used to assess the chemical reactivity of a supplementary cementitious material (SCM) as determined by measurements of cumulative heat release or bound water content of hydrated pastes composed of the SCM, calcium hydroxide, calcium carbonate, potassium sulfate, and potassium hydroxide cured at 40 °C for 3 and 7 days.  
1.1.1 These two test methods do not distinguish between hydraulic and pozzolanic reactivity.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of the standard refers to notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.)2  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The units stated in SI are to be regarded as the standard. No other units of measurement are included in this standard.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 – 19, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal ash resulting from the combustion of coal, and raw or calcined natural pozzolan, for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to coal ash or natural pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a coal ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.    
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.    
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:    
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide,
calcium oxide, magnesium oxide, sulfur
trioxide, sodium oxide and potassium
oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21 – 23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index with portland cement  
27 – 30  
Water requirement  
31  
Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
Note 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SCOPE
1.1 This specification covers ground-glass pozzolans for use in concrete where pozzolanic action is desired. This specification applies to ground glass from sources that consist of container glass, plate glass, or E-glass.  
1.2 The standard references notes and footnotes that provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. If required results obtained from another standard are not reported in the same system of units as used by this standard, it is permitted to convert those results using the conversion factors found in the SI Quick Reference Guide.2  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.    
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:    
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide,
calcium oxide, magnesium oxide, sulfur
trioxide, sodium oxide and potassium
oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21 – 23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index with portland cement  
27 – 30  
Water requirement  
31  
Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Note 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 Common types of SCM include fly ash, slag cement, calcined clays, and silica fume. The introduction and widespread use of fly ash, slag cement, calcined clay, and silica fume have been characterized and supported by significant research and development programs, preconstruction testing, field testing and long term performance monitoring. As the technical and economic benefits of SCM have been recognized, and as sustainability and environmental awareness resulted in the need to develop new materials and new ways to use materials not previously utilized, new sources of potential SCM are being proposed for use in concrete as ASCM.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This Guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989, and C1240. This Guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989, and C1240. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This guide does not purport to address all environmental and safety concerns, if any, associated with its use. It is the responsibility of the user of this guide to establish the appropriate environmental, health, and safety issues, and identify appropriate risk management procedures.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement. (A) The use of Class F pozzolan containing up to 12.0 % loss on ignition may be approved by the user if either acceptable performance records or laboratory test results are made available.  (A) The strength activity index with portland cement is not to be considered a measure of the compressive strength of concrete containing the fly ash or natural pozzolan. The mass of fly ash or natural pozzolan specified for the test to determine the strength activity index with portland cement is not considered to be the proportion recommended for the concrete to be used in the work. The optimum amount of fly ash or natural pozzolan for any specific project is determined by the required properties of the concrete and other constituents of the concrete and is to be established by testing. Strength  activity index with portland cement is a measure of reactivity with a given cement and is subject to variation depending on the source of both the fly ash or natural pozzolan and the cement.(B) Meeting the 7 day or 28 day strength activity index will indicate specification compliance.(C) If the fly ash or natural pozzolan will constitute more than 20 % by mass of the cementitious material in the project mixture, the test specimens for autoclave expansion shall contain that anticipated percentage. Excessive autoclave expansion is highly significant in cases where water to cementitious material ratios are low, for example, in block or shotcrete mixtures.  (A) Determination of compliance or noncompliance with the requirement relating to increase in drying shrinkage will be made only at the request of the purchaser.(B) Fly ash or natural pozzolan shall be considered effective only when the fly ash or natural pozzolan is used at percentages, by mass, of the total cementitious material within 2 % of those that are successful in the test mixtures or between two percentages that are successful, and when the C3A content of the project cement is less than, or equal to, that which was used in the test mixtures. See Appendix X2 of Test Method C311/C311M.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Tra...

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement. (A) The use of Class F pozzolan containing up to 12.0 % loss on ignition may be approved by the user if either acceptable performance records or laboratory test results are made available.  (A) The strength activity index with portland cement is not to be considered a measure of the compressive strength of concrete containing the fly ash or natural pozzolan. The mass of fly ash or natural pozzolan specified for the test to determine the strength activity index with portland cement is not considered to be the proportion recommended for the concrete to be used in the work. The optimum amount of fly ash or natural pozzolan for any specific project is determined by the required properties of the concrete and other constituents of the concrete and is to be established by testing. Strength  activity index with portland cement is a measure of reactivity with a given cement and is subject to variation depending on the source of both the fly ash or natural pozzolan and the cement.(B) Meeting the 7 day or 28 day strength activity index will indicate specification compliance.(C) If the fly ash or natural pozzolan will constitute more than 20 % by mass of the cementitious material in the project mixture, the test specimens for autoclave expansion shall contain that anticipated percentage. Excessive autoclave expansion is highly significant in cases where water to cementitious material ratios are low, for example, in block or shotcrete mixtures.  (A) Determination of compliance or noncompliance with the requirement relating to increase in drying shrinkage will be made only at the request of the purchaser.(B) Fly ash or natural pozzolan shall be considered effective only when the fly ash or natural pozzolan is used at percentages, by mass, of the total cementitious material within 2 % of those that are successful in the test mixtures or between two percentages that are successful, and when the C3A content of the project cement is less than, or equal to, that which was used in the test mixtures. See Appendix X2 of Test Method C311/C311M.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Tra...

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:    
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21 – 23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index with portland cement  
27 – 30  
Water requirement  
31  
Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Note 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:    
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21 – 23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index with portland cement  
27 – 30  
Water requirement  
31  
Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
Note 1: Sieve size is identified by its standard designation in Specification E11. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.  
Note 1: Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement. (A) The use of Class F pozzolan containing up to 12.0 % loss on ignition may be approved by the user if either acceptable performance records or laboratory test results are made available.  (A) The strength activity index with portland cement is not to be considered a measure of the compressive strength of concrete containing the fly ash or natural pozzolan. The mass of fly ash or natural pozzolan specified for the test to determine the strength activity index with portland cement is not considered to be the proportion recommended for the concrete to be used in the work. The optimum amount of fly ash or natural pozzolan for any specific project is determined by the required properties of the concrete and other constituents of the concrete and is to be established by testing. Strength  activity index with portland cement is a measure of reactivity with a given cement and is subject to variation depending on the source of both the fly ash or natural pozzolan and the cement.(B) Meeting the 7 day or 28 day strength activity index will indicate specification compliance.(C) If the fly ash or natural pozzolan will constitute more than 20 % by mass of the cementitious material in the project mixture, the test specimens for autoclave expansion shall contain that anticipated percentage. Excessive autoclave expansion is highly significant in cases where water to cementitious material ratios are low, for example, in block or shotcrete mixtures.  (A) Determination of compliance or noncompliance with the requirement relating to increase in drying shrinkage will be made only at the request of the purchaser.(B) Fly ash or natural pozzolans meeting this requirement are considered as effective in controlling alkali silica reactions as the use of the low-alkali control cement used in the evaluation. However, the fly ash or natural pozzolan shall be considered effective only when used at percentages by mass of the total cementitious material equal to or exceeding that used in the tests and when the alkali content of the cement to be used does not exceed that used in the tests by more than 0.05 %. See Appendix XI, Test Methods C311.(C) Fly ash or natural pozzolan shall be considered effective only when the fly ash or natural pozzolan is used at percentages, by mass, of the total cementitious material within 2 % of those that are successful in the test mixtures or between two percentages that are successful, and when the C3A content of the project cement is less than, or equal to, that which was used in the test mixtures. See Appendix X2 of Test Method C311.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement...

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The units stated in SI are to be regarded as the standard. No other units of measurement are included in this standard.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 – 19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The units stated in SI are to be regarded as the standard.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 – 19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SIGNIFICANCE AND USE
4.1 These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests—The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:
Sections  
Sampling  
7  
CHEMICAL ANALYSIS  
Reagents and apparatus  
10  
Moisture content  
11 and 12  
Loss on ignition  
13 and 14  
Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide  
15  
Available alkali  
16 and 17  
Ammonia  
18  
PHYSICAL TESTS  
Density  
19  
Fineness  
20  
Increase of drying shrinkage of mortar bars  
21-23  
Soundness  
24  
Air-entrainment of mortar  
25 and 26  
Strength activity index with portland cement  
27-30  
Water requirement  
31  
Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions  
32  
Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance  
34
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.Note 1—Sieve size is identified by its standard designation in Specification D1426. The alternative designation given in parentheses is for information only and does not represent a different standard sieve size.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.TABLE 1 Chemical Requirements    
Class  
N  
F  
C  
Silicon dioxide (SiO2) plus aluminum oxide (Al2O3) plus iron oxide (Fe2O3),
min, %  
70.0  
70.0  
50.0  
Sulfur trioxide (SO3), max, %  
4.0  
5.0  
5.0  
Moisture content, max, %  
3.0  
3.0  
3.0  
Loss on ignition, max, %  
10.0  
6.0A  
6.0 A The use of Class F pozzolan containing up to 12.0 % loss on ignition may be approved by the user if either acceptable performance records or laboratory test results are made available.TABLE 2 Physical Requirements    
Class  
N  
F  
C  
Fineness:  
Amount retained when wet-sieved on 45 μm (No. 325) sieve, max, %  
34  
34  
34  
Strength activity index: A  
With portland cement, at 7 days, min, percent of
control  
75B  
75B  
75B  
With portland cement, at 28 days, min, percent of
control  
75B  
75B  
75B  
Water requirement, max, percent of control  
115  
105  
105  
Soundness: C  
Autoclave expansion or contraction, max, %  
0.8  
0.8  
0.8  
Uniformity requirements:  
The density and fineness of individual samples
shall not vary from the average established by the
ten preceding tests, or by all preceding tests if the
number is less than ten, by more than:  
Density, max variation from average, %  
5  
5  
5  
Percent retained on 45-μm (No. 325), max variation,
percentage points from average  
5  
5  
5 A The strength activity index with portland cement is not to be considered a measure of the compressive strength of concrete containing the fly ash or natural pozzolan. The mass of fly ash or natural pozzolan specified for the test to determine the strength activity index with portland cement is not considered to be the proportion recommended for the concrete to be used in the work. The optimum amount of fly ash or natural pozzolan for any specific project is determined by the required properties of the concrete and other constituents of the concrete and is to be established by testing. Strength  activity index with portland cement is a measure of reactivity with a given cement and is subject to variation depending on the source of both the fly ash or natural pozzolan and the cement.B Meeting the 7 day or 28 day strength activity index will indicate specification compliance.C If the fly ash or natural pozzolan will constitute more than 20 % by mass of the cementitious material in the project mixture, the test specimens for autoclave expansion shall contain that anticipated percentage. Excessive autoclave expansion is highly significant in cases where...

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.
TABLE 1 Chemical Requirements    Class NFC Silicon dioxide (SiO2) plus aluminum oxide (Al2O3) plus iron oxide (Fe2O3),
min, %70.070.050.0 Sulfur trioxide (SO3), max, %4.05.05.0 Moisture content, max, %3.03.03.0 Loss on ignition, max, %10.06.0A6.0
A The use of Class F pozzolan containing up to 12.0 % loss on ignition may be approved by the user if either acceptable performance records or laboratory test results are made available.
TABLE 2 Physical Requirements    Class NFC Fineness:  Amount retained when wet-sieved on 45 μm (No. 325) sieve, max, %343434 Strength activity index: A  With portland cement, at 7 days, min, percent of
control75B75B75B  With portland cement, at 28 days, min, percent of
control75B75B75B Water requirement, max, percent of control115105105 Soundness: C Autoclave expansion or contraction, max, %0.80.80.8 Uniformity requirements:  The density and fineness of individual samples
shall not vary from the average established by the
ten preceding tests, or by all preceding tests if the
number is less than ten, by more than:  Density, max variation from average, %555  Percent retained on 45-μm (No. 325), max variation,
percentage points from average555
A The strength activity index with portland cement is not to be considered a measure of the compressive strength of concrete containing the fly ash or natural pozzolan. The mass of fly ash or natural pozzolan specified for the test to determine the strength activity index with portland cement is not considered to be the proportion recommended for the concrete to be used in the work. The optimum amount of fly ash or natural pozzolan for any specific project is determined by the required properties of the concrete and other constituents of the concrete and is to be established by testing. Strength activity index with portland cement is a measure of reactivity with a given cement and is subject to variation depending on the source of both the fly ash or natural pozzolan and the cement.
B Meeting the 7 day or 28 day strength activity index will indicate specification compliance.
C If the fly ash or natural pozzolan will constitute more than 20 % by mass of the cementitious material in the project mixture, the test specimens for autoclave expansion shall contain that anticipated percentage. Excessive a...

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C618 or Specification C1697. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
Chemical Tests— The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:
  Sections Sampling7  CHEMICAL ANALYSIS Reagents and apparatus10 Moisture content11 and 12 Loss on ignition13 and 14 Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide15 Available alkali16 and 17 Ammonia18  PHYSICAL TESTS Density19 Fineness20 Increase of drying shrinkage of mortar bars21-23 Soundness24 Air-entrainment of mortar25 and 26 Strength activity index with portland cement27-30 Water requirement31 Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions32 Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance34
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SIGNIFICANCE AND USE
Common types of SCM include fly ash, slag cement, calcined clays, and silica fume. The introduction and widespread use of fly ash, slag cement, calcined clay, and silica fume have been characterized and supported by significant research and development programs, preconstruction testing, field testing and long term performance monitoring. As the technical and economic benefits of SCM have been recognized, and as sustainability and environmental awareness resulted in the need to develop new materials and new ways to use materials not previously utilized, new sources of potential SCM are being proposed for use in concrete as ASCM.
If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.
In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This Guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989, and C1240. This Guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989, and C1240. These materials should not be represented as such and each specific source is to be evaluated separately.
1.4 This guide does not purport to address all environmental and safety concerns, if any, associated with its use. It is the responsibility of the user of this guide to establish the appropriate environmental, health, and safety issues, and identify appropriate risk management procedures.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C618. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
Chemical Tests— The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:
  Sections Sampling7  CHEMICAL ANALYSIS Reagents and apparatus10 Moisture content11 and 12 Loss on ignition13 and 14 Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide15 Available alkali16 and 17 Ammonia18  PHYSICAL TESTS Density19 Fineness20 Increase of drying shrinkage of mortar bars21-23 Soundness24 Air-entrainment of mortar25 and 26 Strength activity index with portland cement27-30 Water requirement31 Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions32 Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance34
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C618. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
Chemical Tests— The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:
  Sections Sampling7  CHEMICAL ANALYSIS Reagents and apparatus10 Moisture content11 and 12 Loss on ignition13 and 14 Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide15 Available alkali16 and 17 Ammonia18  PHYSICAL TESTS Density19 Fineness20 Increase of drying shrinkage of mortar bars21-23 Soundness24 Air-entrainment of mortar25 and 26 Strength activity index with portland cement27-30 Water requirement31 Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions32 Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance34
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.  
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1—The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice for information and guidelines. Specific reference is made to: ACI 232.1RUse of Natural Pozzolans in Concrete ACI 232.2RUse of Fly Ash in Concrete ACI 233RSlag Cement in Concrete and Mortar ACI 234RGuide for the Use of Silica Fume in Concrete
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

ABSTRACT
This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved. Fly ash and natural pozzolans shall conform to the prescribed chemical composition requirements and physical requirements. The materials shall be tested for fineness, strength activity index, water requirement, soundness, and autoclave expansion or contraction.
SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.  
1.2 The values stated in SI units are to be regarded as the standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C 618. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
Chemical Tests— The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.  
1.2 The procedures appear in the following order:
  Sections Sampling7  CHEMICAL ANALYSIS Reagents and apparatus10 Moisture content11 and 12 Loss on ignition13 and 14 Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide
and potassium oxide15 Available alkali16 and 17 Ammonia18  PHYSICAL TESTS Density19 Fineness20 Increase of drying shrinkage of mortar bars21-23 Soundness24 Air-entrainment of mortar25 and 26 Strength activity index with portland cement27-30 Water requirement31 Effectiveness of Fly Ash or Natural Pozzolan in
Controlling Alkali-Silica Reactions32 Effectiveness of Fly Ash or Natural Pozzolan in
Contributing to Sulfate Resistance34
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SIGNIFICANCE AND USE
These test methods are used to develop data for comparison with the requirements of Specification C 618. These test methods are based on standardized testing in the laboratory and are not intended to simulate job conditions.  
4.1.1 Strength Activity Index—The test for strength activity index is used to determine whether fly ash or natural pozzolan results in an acceptable level of strength development when used with hydraulic cement in concrete. Since the test is performed with mortar, the results may not provide a direct correlation of how the fly ash or natural pozzolan will contribute to strength in concrete.  
4.1.2 Chemical Tests— The chemical component determinations and the limits placed on each do not predict the performance of a fly ash or natural pozzolan with hydraulic cement in concrete, but collectively help describe composition and uniformity of the material.
SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.
1.2 The procedures appear in the following order:
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.4 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

ABSTRACT
This specification covers silica fume for use in concrete and other systems containing hydraulic cement. The material shall composed of silica fume, mostly of amorphous silica. Test methods for chemical analysis, moisture content and loss on ignition, bulk density, specific surface, air entrainment of mortar, strength acitivity index, reactivity with cement alkalis, and sulfate resistance of silica fume shall conform to this specification. Physical tests shall include determining the specimen's density and the specific surface by utilizing the BET, nitrogen adsorption method. Silica fume shall be stored in such a manner as to permit easy access for the proper inspection and identification of each shipment.
SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 These test methods cover procedures for sampling and testing fly ash and raw or calcined pozzolans for use in portland-cement concrete.
1.2 The procedures appear in the following order:  SectionsSampling7 CHEMICAL ANALYSISReagents and apparatus10Moisture content11 and 12Loss on ignition13 and 14Silicon dioxide, aluminum oxide, iron oxide, calcium oxide, magnesium oxide, sulfur trioxide, sodium oxide and potassium oxide15Available alkali16 and 17 PHYSICAL TESTSDensity18Fineness19Increase of drying shrinkage of mortar bars20 to 22Soundness23Air-entrainment of mortar24 and 25Strength activity index with portland cement26 to 29Water requirement30Effectiveness of Fly Ash or Natural Pozzolan in Controlling Alkali-Silica Reactions31Effectiveness of Fly Ash or Natural Pozzolan in Contributing to Sulfate Resistance33
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are provided for information purposes only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections , of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10-19, of this specification:  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to fly ash or pozzolans may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a fly ash or natural pozzolan is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

SCOPE
1.1 This specification covers coal fly ash and raw or calcined natural pozzolan for use as a mineral admixture in concrete where cementitious or pozzolanic action, or both, is desired, or where other properties normally attributed to finely divided mineral admixtures may be desired, or where both objectives are to be achieved.
Note 1—Finely divided materials may tend to reduce the entrained air content of concrete. Hence, if a mineral admixture is added to any concrete for which entrainment of air is specified, provision should be made to ensure that the specified air content is maintained by air content tests and by use of additional air-entraining admixture or use of an air-entraining admixture in combination with air-entraining hydraulic cement.
1.2 The values stated in SI units are to be regarded as the standard.
1.3 The text of this standard references notes and footnotes, which provide explanatory information. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.

SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 through 19, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.

SCOPE
1.1 This specification covers silica fume for use in concrete and other systems containing hydraulic cement.
1.2 In the cases of slurried or densified silica fume, perform the tests on the raw silica fume from which these products have been made.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 The following safety hazards caveat pertains only to the test methods portions, Sections 10 through 19, of this specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Read the material safety data sheets for materials used.
1.5 The text of this standard references notes and footnotes that provide explanatory information. These notes and footnotes (excluding those in tables) shall not be considered as requirements of this standard.