Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small-Scale Closed Cup Tester

SIGNIFICANCE AND USE
5.1 This procedure is intended to be used to evaluate the ignitability of liquid wastes.  
5.2 Flash point measures the response of the subsample to heat and an ignition source under controlled laboratory conditions. It is only one of a number of properties that shall be considered in assessing the overall flammability hazard of a liquid waste material.  
5.3 Flash point can indicate the possible presence of highly volatile and flammable materials in a relatively nonvolatile or nonflammable material.  
5.4 This test method uses a small sample volume (2 mL) and short test time (1 min).
SCOPE
1.1 This test method covers the procedure for a flash point test, within the range of –20 to 70 °C, of liquid wastes using a small-scale closed cup tester.
Note 1: Some apparatus are not designed for subambient temperature tests, so the testing range would be between 20 °C and 70 °C.
Note 2: This test method is not applicable for liquid waste that forms a surface film (see Test Method D8175 for Finite Flash Point Determination of Wastes by Pensky-Martens Closed Cup Tester).  
1.2 Units—The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 This standard measures the ignitability properties of liquid wastes (which may be any discarded material), which may include secondary materials, off-specification products, and materials containing free liquids recovered during emergency response actions. Results from this test method may be used as part of a fire risk assessment of the material, but it is the responsibility of the user to perform any additional characterization needed for determination of storage, transport, treatment, or disposal per current regulations.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Warning statements appear throughout. See applicable Safety Data Sheets (SDS) for information about certified reference materials (CRMs) or secondary working standards (SWSs) that may be used in this test method. SDS may also be useful if some components of the waste sample are known.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Publication Date
14-Mar-2018
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ASTM D8174-18 - Standard Test Method for Finite Flash Point Determination of Liquid Wastes by Small-Scale Closed Cup Tester
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8174 − 18
Standard Test Method for
Finite Flash Point Determination of Liquid Wastes by Small-
1
Scale Closed Cup Tester
This standard is issued under the fixed designation D8174; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Flash point values are a function of the apparatus design, the condition of the apparatus used, and
theoperationalprocedurecarriedout.Flashpointcan,therefore,onlybedefinedintermsofastandard
test method, and no general valid correlation can be guaranteed between results obtained by different
test methods or with different test apparatus.
This test method, and Test Method D8175, are used to determine the flash point of liquid wastes.
This procedure is primarily derived from Method B of Test Methods D3828 (EN ISO 3679 and IP
523) and is informally known in federal and other regulations as the Setaflash method.
1. Scope Warning statements appear throughout. See applicable Safety
Data Sheets (SDS) for information about certified reference
1.1 This test method covers the procedure for a flash point
materials(CRMs)orsecondaryworkingstandards(SWSs)that
test, within the range of –20 to 70°C, of liquid wastes using a
may be used in this test method. SDS may also be useful if
small-scale closed cup tester.
some components of the waste sample are known.
NOTE 1—Some apparatus are not designed for subambient temperature
1.5 This international standard was developed in accor-
tests, so the testing range would be between 20°C and 70°C.
dance with internationally recognized principles on standard-
NOTE 2—This test method is not applicable for liquid waste that forms
ization established in the Decision on Principles for the
a surface film (see Test Method D8175 for Finite Flash Point Determina-
Development of International Standards, Guides and Recom-
tion of Wastes by Pensky-Martens Closed Cup Tester).
mendations issued by the World Trade Organization Technical
1.2 Units—The values stated in SI units are to be regarded
Barriers to Trade (TBT) Committee.
as the standard. No other units of measurement are included in
this standard.
2. Referenced Documents
1.3 This standard measures the ignitability properties of 2
2.1 ASTM Standards:
liquid wastes (which may be any discarded material), which
D3828Test Methods for Flash Point by Small Scale Closed
may include secondary materials, off-specification products,
Cup Tester
and materials containing free liquids recovered during emer-
D6299Practice for Applying Statistical Quality Assurance
gency response actions. Results from this test method may be
and Control Charting Techniques to Evaluate Analytical
usedaspartofafireriskassessmentofthematerial,butitisthe
Measurement System Performance
responsibility of the user to perform any additional character-
D7236Test Method for Flash Point by Small Scale Closed
ization needed for determination of storage, transport,
Cup Tester (Ramp Method)
treatment, or disposal per current regulations.
D8175Test Method For Finite Flash Point Determination of
1.4 This standard does not purport to address all of the
Liquid Wastes by Pensky-Martens Closed Cup Tester
safety concerns, if any, associated with its use. It is the
E502Test Method for Selection and Use of ASTM Stan-
responsibility of the user of this standard to establish appro-
dards for the Determination of Flash Point of Chemicals
priate safety, health, and environmental practices and deter-
by Closed Cup Methods
mine the applicability of regulatory limitations prior to use.
E1137/E1137MSpecification for Industrial Platinum Resis-
tance Thermometers
1
This test method is under the jurisdiction ofASTM Committee D34 on Waste
2
Management and is the direct responsibility of Subcommittee D34.01.06 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Analytical Methods. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved March 15, 2018. Published March 2018. Originally Standards volume information, refer to the standard’s Document Summary page on
approved in 2018. DOI: 10.1520/D8174-18. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D8174 − 18
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2.2 ISO Standards: ignition source applied at intervals to establish an estimate of
ISO 17034General Requirements for the Competence of the fl
...

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