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ASTM D4809-09ae1

(Test Method)

Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)

Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)

SIGNIFICANCE AND USE
5.1 The heat of combustion is a measure of the energy available from a fuel. A knowledge of this value is essential when considering the thermal efficiency of equipment for producing either power or heat.  
5.2 The mass heat of combustion, that is, the heat of combustion per unit mass of fuel, is measured by this procedure. Its magnitude is particularly important to weight-limited vehicles such as airplanes, surface effect vehicles, and hydrofoils as the distance such craft can travel on a given weight of fuel is a direct function of the fuel's mass heat of combustion and its density.  
5.3 The volumetric heat of combustion, that is, the heat of combustion per unit volume of fuel, can be calculated by multiplying the mass heat of combustion by the density of the fuel (mass per unit volume). The volumetric heat of combustion, rather than the mass heat of combustion, is important to volume-limited craft such as automobiles and ships, as it is directly related to the distance traveled between refuelings.
SCOPE
1.1 This test method covers the determination of the heat of combustion of hydrocarbon fuels. It is designed specifically for use with aviation turbine fuels when the permissible difference between duplicate determinations is of the order of 0.2 %. It can be used for a wide range of volatile and nonvolatile materials where slightly greater differences in precision can be tolerated.  
1.2 In order to attain this precision, strict adherence to all details of the procedure is essential since the error contributed by each individual measurement that affects the precision shall be kept below 0.04 %, insofar as possible.  
1.3 Under normal conditions, the test method is directly applicable to such fuels as gasolines, kerosines, Nos. 1 and 2 fuel oil, Nos. 1-D and 2-D diesel fuel and Nos. 0-GT, 1-GT, and 2-GT gas turbine fuels.  
1.4 Through the improvement of the calorimeter controls and temperature measurements, the precision is improved over that of Test Method D240.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 7, 10.6, A1.7.1 and Annex A3.

General Information

Status
Historical
Publication Date
31-Aug-2009
ICS
75.160.20 - Liquid fuels
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.05 - Properties of Fuels, Petroleum Coke and Carbon Material
Current Stage
Ref Project

Relations

Replaces
ASTM D4809-09a - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
Effective Date
01-Sep-2009
Replaced By
ASTM D4809-13 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
Effective Date
01-May-2013
Referred By
ASTM D7566-22a - Standard Specification for Aviation Turbine Fuel Containing Synthesized Hydrocarbons
Effective Date
01-Sep-2009
Referred By
ASTM D240-19 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
Effective Date
01-Sep-2009
Referred By
ASTM D8434-21 - Standard Specification for Unleaded Aviation Gasoline Test Fuel Containing Organo-metallic Additive
Effective Date
01-Sep-2009
Referred By
ASTM D7719-21a - Standard Specification for High Aromatic Content Unleaded Hydrocarbon Aviation Gasoline Test Fuel
Effective Date
01-Sep-2009
Referred By
ASTM G63-15(2023) - Standard Guide for Evaluating Nonmetallic Materials for Oxygen Service
Effective Date
01-Sep-2009
Referred By
ASTM D910-21 - Standard Specification for Leaded Aviation Gasolines
Effective Date
01-Sep-2009
Referred By
ASTM G114-21 - Standard Practices for Evaluating the Age Resistance of Polymeric Materials Used in Oxygen Service
Effective Date
01-Sep-2009
Referred By
ASTM D3338/D3338M-20a - Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels
Effective Date
01-Sep-2009
Referred By
ASTM D6227-18(2023) - Standard Specification for Unleaded Aviation Gasoline Containing a Non-hydrocarbon Component
Effective Date
01-Sep-2009
Referred By
ASTM D1655-23 - Standard Specification for Aviation Turbine Fuels
Effective Date
01-Sep-2009
Referred By
ASTM D6615-22 - Standard Specification for Jet B Wide-Cut Aviation Turbine Fuel
Effective Date
01-Sep-2009
Referred By
ASTM D8147-17(2023) - Standard Specification for Special-Purpose Test Fuels for Aviation Compression-Ignition Engines
Effective Date
01-Sep-2009
Referred By
ASTM G94-22 - Standard Guide for Evaluating Metals for Oxygen Service
Effective Date
01-Sep-2009

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ASTM D4809-09ae1 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)ASTM D4809-09ae1 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
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ASTM D4809-09ae1 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: D4809 − 09a
StandardTest Method for
Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb
1
Calorimeter (Precision Method)
This standard is issued under the fixed designation D4809; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1
ε NOTE—Corrected footnote reference in 11.4 editorially in November 2012.
1. Scope* 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the determination of the heat of
D129Test Method for Sulfur in Petroleum Products (Gen-
combustionofhydrocarbonfuels.Itisdesignedspecificallyfor
eral High Pressure Decomposition Device Method)
use with aviation turbine fuels when the permissible difference
D240Test Method for Heat of Combustion of Liquid Hy-
between duplicate determinations is of the order of 0.2%. It
drocarbon Fuels by Bomb Calorimeter
can be used for a wide range of volatile and nonvolatile
D1018Test Method for Hydrogen In Petroleum Fractions
materials where slightly greater differences in precision can be
D1193Specification for Reagent Water
tolerated.
D1266TestMethodforSulfurinPetroleumProducts(Lamp
1.2 In order to attain this precision, strict adherence to all
Method)
details of the procedure is essential since the error contributed
D2622Test Method for Sulfur in Petroleum Products by
by each individual measurement that affects the precision shall
Wavelength Dispersive X-ray Fluorescence Spectrometry
be kept below 0.04%, insofar as possible.
D3120Test Method for Trace Quantities of Sulfur in Light
1.3 Under normal conditions, the test method is directly
Liquid Petroleum Hydrocarbons by Oxidative Microcou-
applicable to such fuels as gasolines, kerosines, Nos. 1 and 2
lometry
fuel oil, Nos. 1-D and 2-D diesel fuel and Nos. 0-GT, 1-GT,
D3701Test Method for Hydrogen Content of Aviation
and 2-GT gas turbine fuels.
Turbine Fuels by Low Resolution Nuclear Magnetic
Resonance Spectrometry
1.4 Through the improvement of the calorimeter controls
D4294Test Method for Sulfur in Petroleum and Petroleum
and temperature measurements, the precision is improved over
Products by Energy Dispersive X-ray Fluorescence Spec-
that of Test Method D240.
trometry
1.5 The values stated in SI units are to be regarded as
D5453Test Method for Determination of Total Sulfur in
standard. No other units of measurement are included in this
Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel
standard.
Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
1.6 This standard does not purport to address the safety
E1Specification for ASTM Liquid-in-Glass Thermometers
concerns, if any, associated with its use. It is the responsibility
E144Practice for Safe Use of Oxygen Combustion Bombs
of the user of this standard to establish appropriate safety and
E200Practice for Preparation, Standardization, and Storage
health practices and determine the applicability of regulatory
of Standard and Reagent Solutions for ChemicalAnalysis
limitations prior to use. For specific warning statements, see
3. Terminology
Section 7, 10.6, A1.7.1 and Annex A3.
3.1 Definitions:
3.1.1 gross heat of combustion—expressed as megajoules
perkilogram.Thegrossheatofcombustionatconstantvolume
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
2
D02.05 on Properties of Fuels, Petroleum Coke and Carbon Material. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Sept. 1, 2009. Published November 2009. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1988. Last previous edition approved in 2009 as D4809–09. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D4809-09a. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
´1
D4809 − 09a
of a liquid or solid fuel containing only the elements carbon, 3.2.2 Time is expressed in minutes and decimal fractions
hydrogen, oxygen, nitrogen, and sulfur is the quantity of heat thereof. It can be measured in minutes or seconds, or both.
liberated when a unit mass of the fuel is burned in oxygen in 3.2.3 Masses are measured in grams. No buoyancy correc-
an enclosure of constant volume, the products of combustion tions are applied except to obtain the mas
...

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ASTM D3701-23(Test Method)
Standard Test Method for Hydrogen Content of Aviation Turbine Fuels by Low Resolution Nuclear Magnetic Resonance Spectrometry

SIGNIFICANCE AND USE
5.1 The combustion quality of aviation turbine fuel has traditionally been controlled in specifications by such tests as smoke point (see Test Method D1322), smoke volatility index, aromatic content of luminometer number (see Test Method D1740). Evidence is accumulating that a better control of the quality may be obtained by limiting the minimum hydrogen content of the fuel.  
5.2 Existing methods allow the hydrogen content to be calculated from other parameters or determined by combustion techniques. The method specified provides a quick, simple, and more precise alternative to these methods.
SCOPE
1.1 This test method covers the determination of the hydrogen content of aviation turbine fuels.  
1.2 Use Test Methods D4808 or D7171 for the determination of hydrogen in other petroleum liquids.  
1.3 The values stated in SI units are to be regarded as standard. The preferred units are mass percent hydrogen.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific warning statement, see 7.1.  
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ASTM D7826-23b(Guide)
Standard Guide for Evaluation of New Aviation Gasolines and New Aviation Gasoline Additives

SIGNIFICANCE AND USE
5.1 This guide is intended for the developers or sponsors of new aviation gasolines or additives to describe the data requirements necessary to support the development of specifications for these new products by ASTM members. The ultimate goal of the data generated in accordance with this guide is to provide an understanding of the performance of the new fuel or additive within the property constraints and compositional bounds of the proposed specification criteria.  
5.2 This guide is not an approval process. It is intended to describe test and analysis requirements necessary to generate data to support specification development. This guide does not address the approval process for ASTM International standards.  
5.3 This guide will reduce the uncertainty and risk to developers or sponsors of new aviation gasolines or additives by describing the test and analysis requirements necessary to proceed with the development of an ASTM International specification for aviation gasoline or specification revision for an aviation gasoline additive. There are certain sections within this guide that do not specify an exact number of data points required. For example, 6.2.4.3 requires viscosity to be measured from freezing point to room temperature; 6.2.4.4, 6.2.4.5, and 6.3.2.3 require measurements over the operating temperature range; 6.3.2.4 and 6.3.2.5 require measurements versus temperature. In these cases, the developers or sponsors of new aviation gasolines or additives should attempt to generate data close to the upper and lower boundaries indicated. If no boundary is specified (for example, generate data versus temperature), then data at the widest practical test limits should be generated. A minimum of three data points is required in all cases (for example, upper, middle, lower), while five or more data points are preferred.  
5.4 This guide does not purport to specify an all-inclusive listing of test and analysis requirements to achieve ASTM International approval ...
SCOPE
1.1 This guide provides procedures to develop data for use in research reports for new aviation gasolines or new aviation gasoline additives.  
1.2 This data is intended to be used by the ASTM subcommittee to make a determination of the suitability of the fuel for use as an aviation fuel in either a fleet-wide or limited capacity, and to make a determination that the proposed properties and criteria in the associated standard specification provide the necessary controls to ensure this fuel maintains this suitability during high-volume production.  
1.3 These research reports are intended to support the development and issuance of new specifications or specification revisions for these products. Guidance to develop ASTM International standard specifications for aviation gasoline is provided in Subcommittee J on Aviation Fuels Operating Procedures, Annex A6, “Guidelines for the Development and Acceptance of a New Aviation Fuel Specification for Spark-Ignition Reciprocating Engines.”  
1.4 The procedures, tests, selection of materials, engines, and aircraft detailed in this guide are based on industry expertise to give appropriate data for review. Because of the diversity of aviation hardware and potential variation in fuel/additive formulations, not every aspect may be encompassed and further work may be required. Therefore, additional data beyond that described in this guide may be requested by the ASTM task force, Subcommittee J, or Committee D02 upon review of the specific composition, performance, or other characteristics of the candidate fuel or additive.  
1.5 While it is beyond the scope of this guide, investigation of the future health and environmental impacts of the new aviation gasoline or new aviation gasoline additive and the requirements of environmental agencies is recommended.  
1.6 The values stated in SI units are to be regarded as standard.  
1.6.1 Exception—Some industry standard methodologies uti...

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ASTM D3242-23(Test Method)
Standard Test Method for Acidity in Aviation Turbine Fuel

SIGNIFICANCE AND USE
5.1 Some acids can be present in aviation turbine fuels due either to the acid treatment during the refining process or to naturally occurring organic acids. Significant acid contamination is not likely to be present because of the many check tests made during the various stages of refining. However, trace amounts of acid can be present and are undesirable because of the consequent tendencies of the fuel to corrode metals that it contacts or to impair the water separation characteristics of the aviation turbine fuel.  
5.2 This test method is designed to measure the levels of acidity that can be present in aviation turbine fuel and is not suitable for determining significant acid contamination.
SCOPE
1.1 This test method covers the determination of the acidity in aviation turbine fuel in the range from 0.000 mg/g to 0.100 mg/g KOH.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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5.1 This test method provides a rapid and precise elemental measurement with simple sample preparation. Typical analysis times are approximately 4 min to 5 min per sample with a preparation time of approximately 1 min to 3 min per sample.  
5.2 The quality of crude oil is related to the amount of sulfur present. Knowledge of the vanadium and nickel concentration is necessary for processing purposes as well as contractual agreements.  
5.3 The presence of vanadium and nickel presents significant risks for contamination of the cracking catalysts in the refining process.  
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1.1 This test method covers the quantitative determination of total vanadium and nickel in crude and residual oil in the concentration ranges shown in Table 1 using X-ray fluorescence (XRF) spectrometry.  
1.2 Sulfur is measured for analytical purposes only for the compensation of X-ray absorption matrix effects affecting the vanadium and nickel X-rays. For measurement of sulfur by standard test method use Test Methods D4294, D2622 or other suitable standard test method for sulfur in crude and residual oils.  
1.3 This test method is limited to the use of X-ray fluorescence (XRF) spectrometers employing an X-ray tube for excitation in conjunction with wavelength dispersive detection system or energy dispersive high resolution semiconductor detector with the ability to separate signals of adjacent and near-adjacent elements.  
1.4 This test method uses inter-element correction factors calculated from XRF theory, the fundamental parameters (FP) approach, or best fit regression.  
1.5 Samples containing higher concentrations than shown in Table 1 must be diluted to bring the elemental concentration of the diluted material within the scope of this test method.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6.1 The preferred concentrations units are mg/kg for vanadium and nickel.  
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5.1 The analysis of trace oxygenates in automotive spark-ignition engine fuel has become routine in certain areas to ensure compliance whenever oxygenated fuels are used. In addition, test methods to measure trace levels of oxygenates in automotive spark-ignition fuel are necessary to assess product quality.
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1.1 This test method covers the determination of trace oxygenates in automotive spark-ignition engine fuel. The method used is a multidimensional gas chromatographic method using 1,2-dimethoxy ethane as the internal standard. The oxygenates that are analyzed are: methyl-tertiary butyl ether (MTBE), ethyl-tertiary butyl ether (ETBE), diisopropyl ether (DIPE), methanol, tertiary-amyl methyl ether (TAME), n-propanol, i-propanol, n-butanol, i-butanol, tert-butyl alcohol, sec-butyl alcohol, and tert-pentanol. Ethanol is usually not measured as a trace oxygenate since ethanol can be used as the main oxygenate compound in finished automotive spark-ignition fuels such as reformulated automotive spark-ignition fuels. The concentration range of the oxygenates covered in the ILS study was from 10 mg/kg to 2000 mg/kg. In addition this method is also suitable for the measurement of the C5 isomeric alcohols (2-methyl-1-butanol, 2-methyl-2-butanol) present from the fermentation of ethanol.  
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Standard Test Methods for Hydrogen Content of Light Distillates, Middle Distillates, Gas Oils, and Residua by Low-Resolution Nuclear Magnetic Resonance Spectroscopy

SIGNIFICANCE AND USE
5.1 The hydrogen content represents a fundamental quality of a petroleum product that has been correlated with many of the performance characteristics of that product.  
5.2 This test method provides a simple and more precise alternative to existing test methods, specifically combustion techniques (Test Methods D5291) for determining the hydrogen content on a range of petroleum products.
SCOPE
1.1 These test methods cover the determination of the hydrogen content of petroleum products ranging from atmospheric distillates to vacuum residua using a continuous wave, low-resolution nuclear magnetic resonance spectrometer. (Test Method D3701 is the preferred method for determining the hydrogen content of aviation turbine fuels using nuclear magnetic resonance spectroscopy.)  
1.2 Three test methods are included here that account for the special characteristics of different petroleum products and apply to the following distillation ranges:    
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A  
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B  
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200–370 (400–700)  
Gas Oils  
370–510 (700–950)  
C  
Residua  
510+ (950+ )  
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Standard Test Method for Vapor-Liquid Ratio Temperature Determination of Fuels (Evacuated Chamber and Piston Based Method)

SIGNIFICANCE AND USE
5.1 The tendency of a fuel to vaporize in automotive engine fuel systems is indicated by the vapor-liquid ratio of the fuel.  
5.2 Automotive fuel specifications generally include
T(V/L = 20) limits to ensure products of suitable volatility performance. For high ambient temperatures, a fuel with a high value of T(V/L = 20), indicating a fuel with a low tendency to vaporize, is generally specified; conversely for low ambient temperatures, a fuel with a low value of T(V/L = 20) is specified.
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1.1 This test method covers the determination of the temperature at which the vapor formed from a selected volume of volatile petroleum product saturated with air at 0 °C to 1 °C (32 °F to 34 °F) produces a pressure of 101.3 kPa (one atmosphere) against vacuum. This test method is applicable to samples for which the determined temperature is between 36 °C and 80 °C (97 °F and 176 °F) and the vapor-liquid ratio is between 8 to 1 and 75 to 1.
Note 1: When the vapor-liquid ratio is 20:1, the result is intended to be comparable to the results determined by Test Method D2533.
Note 2: This test method may also be applicable at pressures other than one atmosphere, but the stated precision may not apply.  
1.2 This test method is applicable to both gasoline and gasoline-oxygenate blends.  
1.2.1 Some gasoline-oxygenate blends may show a haze when cooled to 0 °C to 1 °C. If a haze is observed in 12.5, it shall be indicated in the reporting of results. The precision and bias statements for hazy samples have not been determined (see Note 12).  
1.3 The values stated in SI units are to be regarded as standard.  
1.3.1 Exception—The values given in parentheses are provided for information only.  
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ASTM D5001-23(Test Method)
Standard Test Method for Measurement of Lubricity of Aviation Turbine Fuels by the Ball-on-Cylinder Lubricity Evaluator (BOCLE)

SIGNIFICANCE AND USE
5.1 Wear due to excessive friction resulting in shortened life of engine components such as fuel pumps and fuel controls has sometimes been ascribed to lack of lubricity in an aviation fuel.  
5.2 The relationship of test results to aviation fuel system component distress due to wear has been demonstrated for some fuel/hardware combinations where boundary lubrication is a factor in the operation of the component.  
5.3 The wear scar generated in the ball-on-cylinder lubricity evaluator (BOCLE) test is sensitive to contamination of the fluids and test materials, the presence of oxygen and water in the atmosphere, and the temperature of the test. Lubricity measurements are also sensitive to trace materials acquired during sampling and storage. Containers specified in Practice D4306 shall be used.  
5.4 The BOCLE test method may not directly reflect operating conditions of engine hardware. For example, some fuels that contain a high content of certain sulfur compounds can give anomalous test results.
SCOPE
1.1 This test method covers assessment of the wear aspects of the boundary lubrication properties of aviation turbine fuels on rubbing steel surfaces.  
1.1.1 This test method incorporates two procedures, one using a semi-automated instrument and the second a fully automated instrument. Either of the two instruments may be used to carry out the test.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7398-23(Test Method)
Standard Test Method for Boiling Range Distribution of Fatty Acid Methyl Esters (FAME) in the Boiling Range from 100 °C to 615 °C by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of FAMES provides an insight into the composition of product related to the transesterification process. This gas chromatographic determination of boiling range can be used to replace conventional distillation methods for product specification testing with the mutual agreement of interested parties.  
5.2 Biodiesel (FAMES) exhibits a boiling point rather than a distillation curve. The fatty acid chains in the raw oils and fats from which biodiesel is produced are mainly comprised of straight chain hydrocarbons with 16 to 18 carbons that have similar boiling temperatures. The atmospheric boiling point of biodiesel generally ranges from 330 °C to 357 °C. The Specification D6751 value of 360 °C max at 90 % off by Test Method D1160 was incorporated as a precaution to ensure the fuel has not been adulterated with high boiling contaminants.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of fatty acid methyl esters (FAME). This test method is applicable to FAMES (biodiesel, B100) having an initial boiling point greater than 100 °C and a final boiling point less than 615 °C at atmospheric pressure as measured by this test method.  
1.2 The test method can also be applicable to blends of diesel and biodiesel (B1 through B100), however precision for these samples types has not been evaluated.  
1.3 The test method is not applicable for analysis of petroleum containing low molecular weight components (for example naphthas, reformates, gasolines, crude oils).  
1.4 Boiling range distributions obtained by this test method are not equivalent to results from low efficiency distillation such as those obtained with Test Method D86 or D1160, especially the initial and final boiling points.  
1.5 This test method uses the principles of simulated distillation methodology. See Test Methods D2887, D6352, and D7213.  
1.6 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D7484-23a(Test Method)
Standard Test Method for Evaluation of Automotive Engine Oils for Valve-Train Wear Performance in Cummins ISB Medium-Duty Diesel Engine

SIGNIFICANCE AND USE
5.1 This test method was developed to assess the performance of a heavy-duty engine oil in controlling engine wear under operating conditions selected to accelerate soot production and valve-train wear in a turbocharged and aftercooled four-cycle diesel engine with sliding tappet followers equipped with exhaust gas recirculation hardware.  
5.2 The design of the engine used in this test method is representative of many, but not all, modern diesel engines. This factor, along with the accelerated operating conditions, shall be considered when extrapolating test results.
SCOPE
1.1 This test method, commonly referred to as the Cummins ISB Test, covers the utilization of a modern, 5.9 L, diesel engine equipped with exhaust gas recirculation and is used to evaluate oil performance with regard to valve-train wear.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exceptions—SI units are provided for all parameters except where there is no direct equivalent such as the units for screw threads, National Pipe Threads/diameters, tubing size, or where there is a sole source of supply equipment specification.  
1.2.2 See also A7.1 for clarification; it does not supersede 1.2 and 1.2.1.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Annex A1 for general safety precautions.  
1.4 Table of Contents:    
Section  
Scope  
1  
Referenced Documents  
2  
Terminology  
3  
Summary of Test Method  
4  
Significance and Use  
5  
Apparatus  
6  
Engine Fluids and Cleaning Solvents  
7  
Preparation of Apparatus  
8  
Engine/Stand Calibration and Non-Reference Oil Tests  
9  
Test Procedure  
10  
Calculations, Ratings, and Test Validity  
11  
Report  
12  
Precision and Bias  
13  
Annexes  
Safety Precautions  
Annex A1  
Intake Air Aftercooler  
Annex A2  
The Cummins ISB Engine Build Parts Kit  
Annex A3  
Sensor Locations and Special Hardware  
Annex A4  
External Oil System  
Annex A5  
Cummins Service Publications  
Annex A6  
Specified Units and Formats  
Annex A7  
Oil Analyses  
Annex A8  
Alternate Fuel Approval Process  
Annex A9  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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