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ASTM F677-04(2009)

(Test Method)

Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications

Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications

SIGNIFICANCE AND USE
Fluids and greases in contact with encapsulating compounds may adversely modify the encapsulant properties with resulting damage or loss of protection to components in electronic applications.
This test method provides a means for measuring the effect of fluids and greases on various encapsulants.
This test method is intended for use in research and evaluation.
SCOPE
1.1 This test method determines the resistance of encapsulating compounds to fluids or greases by measuring changes in weight (Note 1) and volume under defined conditions of time and temperature.
Note 1—To provide consistency with the usage in other ASTM test methods concerned with determining the properties of plastic materials, the terms “weight” and “weigh” are used in this test method although the units of measurement are those of mass.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  See 9.1.  
1.3 The values stated in SI units are standard. The values in parentheses are for information only.
Note 2—There is no similar or equivalent IEC standard.

General Information

Status
Historical
Publication Date
30-Sep-2009
ICS
31.020 - Electronic components in general
Technical Committee
D09 - Electrical and Electronic Insulating Materials
Drafting Committee
D09.01 - Electrical Insulating Products
Current Stage
Ref Project

Relations

Replaces
ASTM F677-04 - Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications
Effective Date
01-Oct-2009
Replaced By
ASTM F677-13 - Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications (Withdrawn 2013)
Effective Date
01-Apr-2013

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ASTM F677-04(2009) - Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic ApplicationsASTM F677-04(2009) - Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications
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ASTM F677-04(2009) - Standard Test Method for Fluid and Grease Resistance of Thermoset Encapsulating Compounds Used in Electronic and Microelectronic Applications
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Standards Content (Sample)


NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: F677 − 04(Reapproved 2009) An American National Standard
Standard Test Method for
Fluid and Grease Resistance of Thermoset Encapsulating
Compounds Used in Electronic and Microelectronic
Applications
ThisstandardisissuedunderthefixeddesignationF677;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3.1.1 For the definitions of terms used in this standard, refer
to Terminology D1711.
1.1 This test method determines the resistance of encapsu-
lating compounds to fluids or greases by measuring changes in
4. Summary of Test Method
weight (Note 1) and volume under defined conditions of time
and temperature.
4.1 Specimens of encapsulating compound are immersed in
fluids or greases for specified conditions of temperature and
NOTE 1—To provide consistency with the usage in other ASTM test
time. The weight and volume of each specimen is measured
methods concerned with determining the properties of plastic materials,
the terms “weight” and “weigh” are used in this test method although the before and after immersion and percent change is reported.
units of measurement are those of mass.
4.2 The fluids and greases to be used as test media (8.3) are
1.2 The values stated in SI units are standard. The values in
not specified by the test method and shall be agreed to by the
parentheses are for information only.
parties to the test.
NOTE 2—There is no similar or equivalent IEC standard.
5. Significance and Use
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5.1 Fluids and greases in contact with encapsulating com-
responsibility of the user of this standard to establish appro-
pounds may adversely modify the encapsulant properties with
priate safety and health practices and determine the applica-
resulting damage or loss of protection to components in
bility of regulatory limitations prior to use. See 9.1.
electronic applications.
5.2 This test method provides a means for measuring the
2. Referenced Documents
effect of fluids and greases on various encapsulants.
2.1 ASTM Standards:
5.3 This test method is intended for use in research and
D1193 Specification for Reagent Water
evaluation.
D1711 Terminology Relating to Electrical Insulation
D5423 Specification for Forced-Convection Laboratory Ov-
6. Interferences
ens for Evaluation of Electrical Insulation
D6054 Practice for Conditioning Electrical Insulating Mate- 6.1 Test results obtained with molded or cast specimens of
rials for Testing filled encapsulating compounds will differ from those obtained
with cut or machined specimens (because of exposed fillers in
3. Terminology
the latter).
3.1 Definitions:
6.2 Lack of complete contact between the test medium and
the surfaces of the specimen may seriously affect the results of
the test.
This test method is under the jurisdiction of ASTM Committee D09 on
6.3 Some encapsulants may be affected by the reagents
Electrical and Electronic Insulating Materials and is the direct responsibility of
specified for use in removing the test media from the speci-
Subcommittee D09.01 on Electrical Insulating Varnishes, Powders and Encapsulat-
ing Compounds.
mens.Alternative reagents may be required, as agreed upon by
Current edition approved Oct. 1, 2009. Published February 2010. Originally
the parties to the test.
approved in 1980. Last previous edition approved in 2004 as F677 – 04. DOI:
10.1520/F0677-04R09.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 7. Apparatus
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.1 Analytical Balance, capable of determining weight to
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. the nearest 0.001 g.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
F677 − 04 (2009)
7.2 Oven, forced-convection type meeting the requirements fluid. Repeat this procedure to form a sandwich structure of
of Specification D5423, Type I. alternating filter paper and specimen layers.
13.2.2 For grease test media, omit the filter paper if the
7.3 Glass Dishes, of sufficient diameter for specimens to be
viscosity of the grease at the exposure temperature is sufficient
exposed horizontally, and of sufficient height for specimens to
to prevent specimens from touching. Apply grease to all
becompletelycoveredbythetestmedium.Aloose-fittingglass
exposed surfaces of the specimens and insert coated specimens
cover shall be provided for each dish (see 13.3).
into the dish to form a sandwich structure of alternating grease
and specimen layers.
8. Reagents and Materials
13.3 Covertheassembledtestspecimenswithaloose-fitting
8.1 Use the following materials:
glass cover and expose the assembled test specimens in an
8.1.1 Acetone.
ovenat71 63°C(160 65.4°F)foratotaldurationof14days.
8.1.2 Distilled Water—Type III Reagent Water as defined in
Specification D1193.
13.4 Remove the specimens from the oven for measurement
8.1.3 Isopropyl Alcohol.
andobservationaftercumulativeexposuretimesof24 62h(1
day), 168 6 2 h (7 days), and 336 6 2 h (14 days).
8.2 Filter Paper, medium retention and medium filtering
13.4.1 Remove the assembled test specimens from the oven
speed, free of lint or foreign material.
and allow them to cool to room temperature for 30 to 60 min,
8.3 Test Media—agreed-upon fluids or greases.
before conducting measurements and observations as follows:
13.4.1.1 Remove specimens one at a time from the test
9. Safety Precautions
medium, saving the test medium in the glass dish or other
9.1 Some encapsulating compounds are known to contain
convenient noncontaminating vessel. Remove (and save) high-
toxic components, and special precautions are required in
viscosity fluids and greases from the specimen with a spatula.
...

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1.1 This specification (see Note 1) covers grades of fuel oil intended for use in various types of fuel-oil-burning equipment under various climatic and operating conditions. These grades are described as follows:  
1.1.1 Grades No. 1 S5000, No. 1 S500, No. 1 S15, No. 2 S5000, No. 2 S500, and No. 2 S15 are middle distillate fuels for use in domestic and small industrial burners. Grades No. 1 S5000, No. 1 S500, and No. 1 S15 are particularly adapted to vaporizing type burners or where storage conditions require low pour point fuel.  
1.1.2 Grades B6–B20 S5000, B6–B20 S500, and B6–B20 S15 are middle distillate fuel/biodiesel blends for use in domestic and small industrial burners.  
1.1.3 Grades No. 4 (Light) and No. 4 are heavy distillate fuels or middle distillate/residual fuel blends used in commercial/industrial burners equipped for this viscosity range.  
1.1.4 Grades No. 5 (Light), No. 5 (Heavy), and No. 6 are residual fuels of increasing viscosity and boiling range, used in industrial burners. Preheating is usually required for handling and proper atomization.  
Note 1: For information on the significance of the terminology and test methods used in this specification, see Appendix X1.
Note 2: A more detailed description of the grades of fuel oils is given in X1.3.  
1.2 This specification is for the use of purchasing agencies in formulating specifications to be included in contracts for purchases of fuel oils and for the guidance of consumers of fuel oils in the selection of the grades most suitable for their needs.  
1.3 Nothing in this specification shall preclude observance of federal, state, or local regulations which can be more restrictive.  
1.4 The values stated in SI units are to be regarded as standard.  
1.4.1 Non-SI units are provided in Table 1 and Table 2 and in 7.1.2.1/7.1.2.2 because these are common units used in the industry.
Note 3: The generation and dissipation of static electricity can create problems in the handling of distillate burner fuel oils. For more information on the subject, see Guide D4865.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8165-24(Test Method)
Standard Test Method for Evaluation of Load-Carrying Capacity of Lubricants Used in Hypoid Final-Drive Axles Operated under Low-Speed and High-Torque Conditions

SIGNIFICANCE AND USE
5.1 This test method measures a lubricant's ability to protect hypoid final drive axles from abrasive wear, adhesive wear, plastic deformation, and surface fatigue when subjected to low-speed, high-torque conditions. Lack of protection can lead to premature gear or bearing failure, or both.  
5.2 This test method is used, or referred to, in specifications and classifications of rear-axle gear lubricants such as:  
5.2.1 Specification D7450.  
5.2.2 American Petroleum Institute (API) Publication 1560.  
5.2.3 SAE J308.  
5.2.4 SAE J2360.
SCOPE
1.1 This test method, commonly referred to as the L-37-1 test, describes a test procedure for evaluating the load-carrying capacity, wear performance, and extreme pressure properties of a gear lubricant in a hypoid axle under conditions of low-speed, high-torque operation.3  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exceptions—Where there is no direct SI equivalent such as National Pipe threads/diameters, tubing size, or where there is a sole source supply equipment specification.
1.2.1.1 The drawing in Annex A6 is in inch-pound units.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific warning statements are provided in 7.2 and 10.1.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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