Alloyed steels - Determination of nickel content - Inductively coupled plasma optical emission spectrometric method

This European Standard specifies an inductively coupled plasma optical emission spectrometric method for the determination of nickel content (mass fraction) between 5,0 % and 25,0 % in alloyed steels.
The method does not apply to alloyed steels having niobium and/or tungsten contents higher than 0,1 %.

Legierte Stähle - Bestimmung des Nickelanteils - Verfahren mittels optischer Emissionsspektrometrie mit induktiv gekoppeltem Plasma

Diese Europäische Norm legt ein Verfahren der optischen Emissionsspektrometrie mit induktiv gekoppeltem Plasma fest, das zur Bestimmung von Nickelanteilen (Massenanteilen) in legierten Stählen zwischen 5,0 % und 25,0 % angewendet wird.
Das Verfahren ist nicht auf legierte Stähle anwendbar, die Niobium  und/oder Wolframanteile von mehr als 0,1 % haben.

Aciers alliés - Détermination du nickel - Méthode par spectrométrie d'émission optique avec source à plasma induit

La présente Norme européenne spécifie une méthode de détermination des teneurs en nickel comprises entre 5,0 % et 25,0 %, dans les aciers alliés, par spectrométrie d’émission optique avec source à plasma induit.  
La méthode ne s’applique pas aux aciers alliés contenant plus de 0,1 % de niobium et/ou de tungstène.

Legirana jekla - Določevanje niklja - Optična emisijska spektrometrija z induktivno sklopljeno plazmo (ICP/OES)

V tem dokumentu je določena metoda optične emisijske spektrometrije z induktivno sklopljeno plazmo za določanje vsebnosti niklja (masni delež) med 5,0 % (m/m) in 25,0 % (m/m) v legiranih jeklih.
Metoda ne velja za legirana jekla z vsebnostjo niobija in/ali volframa, višjo od 0,1 %.

General Information

Status
Published
Publication Date
08-Dec-2015
Current Stage
9093 - Decision to confirm - Review Enquiry
Completion Date
13-Aug-2021

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Stahl - Bestimmung des Nickelgehaltes - Optischer Emissionsspektrometrie mit induktiv gekoppeltem Plasma VerfahrenAciers alliés - Détermination du Nickel - Méthode par spectrométrie d'émission optique avec source à plasma induitAlloyed steels - Determination of Nickel content - Inductively coupled plasma optical emission spectrometric method77.080.20JeklaSteels77.040.30Kemijska analiza kovinChemical analysis of metalsICS:Ta slovenski standard je istoveten z:EN 10361:2015SIST EN 10361:2016en,fr,de01-februar-2016SIST EN 10361:2016SLOVENSKI

STANDARD
SIST EN 10361:2016
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 10361
December
t r s w ICS
y yä r v rä u r English Version

Alloyed steels æ Determination of nickel content æ Inductively coupled plasma optical emission spectrometric method Aciers alliés æ Détermination du nickel æ Méthode par spectrométrie d 5émission optique avec source à plasma induit

Legierte Stähle æ Bestimmung des Nickelanteils æ Verfahren mittels optischer Emissionsspektrometrie mit induktiv gekoppeltem Plasma This European Standard was approved by CEN on

t r June
t r s wä

egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä

translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä

CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä

EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels

t r s w CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN

s r u x sã t r s w ESIST EN 10361:2016

EN 10361:2015 (E) 2 Contents Page European foreword ....................................................................................................................................................... 3 1 Scope .................................................................................................................................................................... 4 2 Normative references .................................................................................................................................... 4 3 Principle ............................................................................................................................................................. 4 4 Reagents ............................................................................................................................................................. 4 5 Apparatus ........................................................................................................................................................... 5 6 Sampling ............................................................................................................................................................. 6 7 Procedure........................................................................................................................................................... 6 8 Determination .................................................................................................................................................. 8 9 Expression of the results .............................................................................................................................. 9 10 Test report ......................................................................................................................................................... 9 Annex A (informative)

Plasma optical emission spectrometer - Suggested performance criteria to be checked ................................................................................................................................. 13 Annex B (informative)

Composition of the samples used for the validation precision test............. 15 Annex C (informative)

Graphical representation of the precision data .................................................. 16 Bibliography ................................................................................................................................................................. 17

SIST EN 10361:2016

EN 10361:2015 (E) 3 European foreword This document (EN 10361:2015) has been prepared by Technical Committee ECISS/TC 102 “Methods of chemical analysis of iron and steel”, the secretariat of which is held by SIS. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2016 and conflicting national standards shall be withdrawn at the latest by June 2016. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 10361:2016

EN 10361:2015 (E) 4 1 Scope This European Standard specifies an inductively coupled plasma optical emission spectrometric method for the determination of nickel content (mass fraction) between 5,0 % and 25,0 % in alloyed steels. The method does not apply to alloyed steels having niobium and/or tungsten contents higher than 0,1 %. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN ISO 648, Laboratory glassware - Single-volume pipettes (ISO 648) EN ISO 1042, Laboratory glassware - One-mark volumetric flasks (ISO 1042) 3 Principle Dissolution of a test portion with hydrochloric and nitric acids. Filtration and ignition of the acid insoluble residue. Removal of silica with hydrofluoric acid. Fusion of the residue with potassium hydrogen sulphate (or with potassium disulphate), dissolution of the melt with acid and addition of this solution to the reserved filtrate. After suitable dilution and, if necessary, addition of an internal reference element,

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