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EN ISO 14596:2007

(Main)

Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:2007)

Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:2007)

ISO 14596:2007 specifies a method for the determination of the sulfur content of liquid petroleum products, additives for petroleum products, and semi-solid and solid petroleum products that are either liquefied by moderate heating or soluble in organic solvents of negligible or accurately known sulfur content. The method is applicable to products or additives having sulfur contents in the range 0,001 % (m/m) to 2,50 % (m/m); higher contents can be determined by appropriate dilution. Other elements do not interfere at concentrations anticipated in the materials subject to this analysis.

Mineralölerzeugnisse - Bestimmung des Schwefelgehaltes - Wellenlängendispersive Röntgenfluoreszenz-Analyse (ISO 14596:2007)

Diese Internationale Norm legt ein Verfahren fest zur Bestimmung des Schwefelgehaltes von flüssigen Mineralölerzeugnissen, Additiven für Mineralölerzeugnisse sowie von halbfesten oder festen Mineralöl¬erzeugnissen, die entweder durch mäßiges Erhitzen verflüssigt werden können oder löslich in organischen Lösemitteln (siehe 4.1) mit vernachlässigbarem oder aber genau bekanntem Schwefelgehalt sind. Das Verfahren ist anwendbar auf Produkte mit einem Schwefelanteil im Bereich von 0,001 % (m/m) bis 2,50 % (m/m) Massenanteil; höhere Gehalte sind durch entsprechende Verdünnung bestimmbar. Andere Elemente stören nicht in den Gehaltsbereichen, die in Materialien für diese Prüfung erwartet werden können.
ANMERKUNG   Für den Zweck dieser Internationalen Norm wird das Symbol „% (m/m)“ für „Massenanteil in %“
verwendet.
Hohe Phosphorgehalte oder Chlorgehalte (typischerweise über 3 % (m/m) können Abweichungen für ein Schwefel-Ergebnis verursachen, da die Zr-L-Linie und die S-K-Linie in unterschiedlichem Ausmaß abgeschwächt werden. In solchen Fällen ist es notwendig, das Ausmaß dieser Störung durch Phosphor genauer zu untersuchen.
Bei höheren Molybdängehalten (üblicherweise 50 mg/kg bis 100 mg/kg) kann es eine angestiegene Hinter¬grundstrahlung sowie spektrale Überlappungen mit dem Schwefelsignal geben. In diesen Fällen ist es notwendig, die relevanten spektralen Bereiche hinsichtlich der Bedeutung potentieller Störungen zu untersuchen.

Produits pétroliers - Détermination de la teneur en soufre - Spectrométrie de fluorescence X dispersive en longueur d'onde (ISO 14596:2007)

L'ISO 14596:2007 spécifie une méthode de détermination de la teneur en soufre dans les produits pétroliers liquides, dans les additifs pour produits pétroliers, et dans les produits pétroliers solides et semi-solides qui sont soit liquéfiés par un chauffage modéré, soit solubles dans des solvants organiques dont la teneur en soufre est négligeable ou connue avec précision. La méthode est applicable à des produits ou à des additifs dont la teneur en soufre est située de 0,001 % (m/m) à 2,50 % (m/m), des teneurs plus élevées pouvant être déterminées par des dilutions appropriées. Les autres éléments n'interfèrent pas dans le domaine de concentration visé pour les produits relevant de cette méthode.

Naftni proizvodi – Določevanje vsebnosti žvepla – Valovno disperzivna rentgenska fluorescenčna spektrometrija (ISO 14596:2007)

General Information

Status
Published
Publication Date
14-Sep-2007
Withdrawal Date
30-Mar-2008
ICS
75.080 - Petroleum products in general
Technical Committee
CEN/TC 19 - Petroleum products, lubricants and related products
Drafting Committee
CEN/TC 19 - Petroleum products, lubricants and related products
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
15-Sep-2007
Due Date
01-Feb-2009
Completion Date
15-Sep-2007
Ref Project
SIST EN ISO 14596:2007 - Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:2007)

Relations

Replaces
EN ISO 14596:1998 - Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:1998)
Effective Date
22-Dec-2008
Replaces
EN ISO 14596:1998/AC:1999 - Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray fluorescence spectrometry (ISO 14596:1998)
Effective Date
22-Dec-2008

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 14596:2007
01-december-2007
1DGRPHãþD
SIST EN ISO 14596:1999
1DIWQLSURL]YRGL±'RORþHYDQMHYVHEQRVWLåYHSOD±9DORYQRGLVSHU]LYQDUHQWJHQVND
IOXRUHVFHQþQDVSHNWURPHWULMD ,62
Petroleum products - Determination of sulfur content - Wavelength-dispersive X-ray
fluorescence spectrometry (ISO 14596:2007)
Mineralölerzeugnisse - Bestimmung des Schwefelgehaltes - Wellenlängendispersive
Röntgenfluoreszenz-Analyse (ISO 14596:2007)
Produits pétroliers - Détermination de la teneur en soufre - Spectrométrie de
fluorescence X dispersive en longueur d'onde (ISO 14596:2007)
Ta slovenski standard je istoveten z: EN ISO 14596:2007
ICS:
75.080 Naftni proizvodi na splošno Petroleum products in
general
SIST EN ISO 14596:2007 en,fr
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

EUROPEAN STANDARD
EN ISO 14596
NORME EUROPÉENNE
EUROPÄISCHE NORM
September 2007
ICS 75.080 Supersedes EN ISO 14596:1998
English Version
Petroleum products - Determination of sulfur content -
Wavelength-dispersive X-ray fluorescence spectrometry (ISO
14596:2007)
Produits pétroliers - Détermination de la teneur en soufre - Mineralölerzeugnisse - Bestimmung des Schwefelgehaltes
Spectrométrie de fluorescence X dispersive en longueur - Wellenlängendispersive Röntgenfluoreszenz-Analyse
d'onde (ISO 14596:2007) (ISO 14596:2007)
This European Standard was approved by CEN on 8 September 2007.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the
official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2007 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 14596:2007: E
worldwide for CEN national Members.

---------------------- Page: 2 ----------------------

EN ISO 14596:2007 (E)
Contents Page
Foreword.3

2

---------------------- Page: 3 ----------------------

EN ISO 14596:2007 (E)
Foreword
This document (EN ISO 14596:2007) has been prepared by Technical Committee ISO/TC 28 "Petroleum
products and lubricants" in collaboration with Technical Committee CEN/TC 19 "Gaseous and liquid fuels,
lubricants and related products of petroleum, synthetic and biological origin", the secretariat of which is held
by NEN.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by March 2008, and conflicting national standards shall be withdrawn at
the latest by March 2008.
This document supersedes EN ISO 14596:1998.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech
Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia,
Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain,
Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 14596:2007 has been approved by CEN as a EN ISO 14596:2007 without any modification.

3

---------------------- Page: 4 ----------------------

INTERNATIONAL ISO
STANDARD 14596
Second edition
2007-09-15

Petroleum products — Determination of
sulfur content — Wavelength-dispersive
X-ray fluorescence spectrometry
Produits pétroliers — Détermination de la teneur en soufre —
Spectrométrie de fluorescence X dispersive en longueur d'onde




Reference number
ISO 14596:2007(E)
©
ISO 2007

---------------------- Page: 5 ----------------------

ISO 14596:2007(E)
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