EN 13075-2:2016
(Main)Bitumen and bituminous binders - Determination of breaking behaviour - Part 2: Determination of fines mixing time of cationic bituminous emulsions
General Information
- Abstract
This European Standard specifies a method for the determination of the fines mixing time of diluted cationic bituminous emulsions, under standardized conditions.
WARNING — The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Status
- Published
- Publication Date
- 08-Nov-2016
- Withdrawal Date
- 30-May-2017
- Technical Committee
- CEN/TC 336 - Bituminous binders
- Drafting Committee
- CEN/TC 336/WG 2 - Emulsions and fluxed bitumens
- Current Stage
- 9092 - Decision on results of review/2YR ENQ - revise - Review Enquiry
- Start Date
- 07-Dec-2022
- Completion Date
- 23-Sep-2026
Overview
EN 13075-2:2016 - Bitumen and bituminous binders: Determination of breaking behaviour - Part 2 specifies a laboratory method to determine the fines mixing time of diluted cationic bituminous emulsions under standardized conditions. The test measures how long a diluted cationic emulsion remains mixable when a defined quantity of mineral filler is added, recording the time to a noticeable breaking/pasty state. This metric helps assess emulsion–filler compatibility and breaking behaviour for quality control and formulation development.
WARNING: The standard notes the use of hazardous materials and equipment. Users must establish safe laboratory practices and comply with regulatory limits.
Key topics and technical requirements
- Scope: Method for diluted cationic emulsions to determine fines mixing time (mixability until breaking).
- Principle: Add filler gradually to diluted emulsion while stirring; the end point is when the mixture becomes pasty, forms non-adherent lumps and stirring power increases.
- Sample preparation and conditioning: Emulsion and water are conditioned at (25 ± 1) °C; fillers are dried at (110 ± 5) °C to constant mass.
- Quantities and procedure details: Typical test portions stated in the standard include transferring (100.0 ± 0.5) g emulsion, adding (50.0 ± 0.5) g water, and adding (150 ± 1) g filler in portions (10 g every 5 s) while stirring at 1 r/s. Timing is stopped when breaking occurs.
- Reference fillers: Three allowed reference fillers - Forshammer, Sikaisol, and Caolin Q92 - with specified compositional and particle-size envelopes (see Annex A).
- Result expression: Individual mixing times (seconds) to nearest integer; report the arithmetic mean of two tests. If no break within 300 s, report “> 300 s” (or “> 300 s – formation of lumps” if lumps form but full break does not occur).
- Precision: No European round-robin precision data provided in this edition.
Applications and users
This standard is relevant for:
- Quality control laboratories in bitumen/emulsion production
- Asphalt technologists and pavement material researchers
- Emulsion formulators assessing filler compatibility and breaking characteristics
- Contracting firms and materials certification bodies that require standardized test data
Practical uses include batch acceptance, troubleshooting breaking problems, comparing emulsion grades, and supporting specification compliance for cationic bituminous emulsions used in cold mixes, surface treatments, or other pavement applications.
Related standards
- EN 13075-1 (breaking value by mineral filler method)
- EN 58 (sampling bituminous binders)
- EN 12594 (preparation of test samples)
- EN ISO 3696 (laboratory water quality)
- EN 933-10, EN 933-1 (filler/aggregate particle size methods)
Keywords: EN 13075-2:2016, fines mixing time, cationic bituminous emulsions, breaking behaviour, bitumen tests, reference fillers, Forshammer, Caolin Q92, laboratory method.
Relations
- Effective Date
- 27-Jun-2012
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 18-Jan-2023
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DIBt (Deutsches Institut für Bautechnik)
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Element Materials Technology
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Frequently Asked Questions
EN 13075-2:2016 is a standard published by the European Committee for Standardization (CEN). Its full title is "Bitumen and bituminous binders - Determination of breaking behaviour - Part 2: Determination of fines mixing time of cationic bituminous emulsions". This standard covers: This European Standard specifies a method for the determination of the fines mixing time of diluted cationic bituminous emulsions, under standardized conditions. WARNING — The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
This European Standard specifies a method for the determination of the fines mixing time of diluted cationic bituminous emulsions, under standardized conditions. WARNING — The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
EN 13075-2:2016 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.
EN 13075-2:2016 has the following relationships with other standards: It is inter standard links to EN 13075-2:2009, EN 58:2012, EN ISO 3696:1995, EN 12594:2024, EN 13808:2005, EN 13108-31:2019, EN 14733:2005+A1:2010, FprEN 13075-2. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
EN 13075-2:2016 is associated with the following European legislation: Standardization Mandates: M/124. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.
EN 13075-2:2016 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.PXO]LMDKBitumen und bitumenhaltige Bindemittel - Bestimmung des Brechverhaltens - Teil 2: Bestimmung der Mischzeit von Feinanteilen in kationischen BitumenemulsionenBitumes et liants bitumineux - Détermination du comportement à la rupture - Partie 2 : Détermination de la durée de miscibilité des fines dans les émulsions cationiques de bitumeBitumen and bituminous binders - Determination of breaking behaviour - Part 2: Determination of fines mixing time of cationic bituminous emulsions91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13075-2:2016SIST EN 13075-2:2017en,fr,de01-januar-2017SIST EN 13075-2:2017SLOVENSKI
STANDARDSIST EN 13075-2:20091DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13075-2
November
t r s x ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s u r y wæ tã t r r {English Version
Bitumen and bituminous binders æ Determination of breaking behaviour æ Part
tã Determination of fines mixing time of cationic bituminous emulsions Bitumes et liants bitumineux æ Détermination du comportement à la rupture æ Partie
t ã Détermination de la durée de miscibilité des fines dans les émulsions cationiques de bitume
Bitumen und bitumenhaltige Bindemittel æ Bestimmung des Brechverhaltens æ Teil
tã Bestimmung der Mischzeit von Feinanteilen in kationischen Bitumenemulsionen This European Standard was approved by CEN on
t y August
t r s xä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey andUnited Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels
t r s x CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s u r y wæ tã t r s x ESIST EN 13075-2:2017
Characteristics of the reference fillers . 7 A.1 Characteristics of the Forshammer filler . 7 A.2 Characteristics of the Sikaisol filler . 8 A.3 Characteristics of the Caolin Q92 filler . 9 Bibliography . 11
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