EN 13649:2001

Stationary source emissions - Determination of the mass concentration of individual gaseous organic compounds - Activated carbon and solvent desorption method

This European Standard specifies procedures for the sampling onto activated carbon, the preparation and the analysis of samples of volatile organic components such as those arising from solvent using processes. It can be used as a reference method.
NOTE   See Council Directive 1999/13/EEC.
The results obtained using this Standard are expressed as the mass concentration (mg/m3) of the individual gaseous organic components. This Standard is suitable for use in the range of about 0,5 mg/m3 to 2000 mg/m3.
For the measurement of the mass concentration of total organic carbon arising from solvent using processes then EN 13526 should be used.

Emissionen aus stationären Quellen - Bestimmung der Massenkonzentration von einzelnen gasförmigen organischen Verbindungen - Aktivkohleadsorptions- und Lösemitteldesorptionsverfahren

Diese Europäische Norm legt Verfahren zur Probenahme von flüchtigen organischen Verbindungen auf Aktivkohle sowie die Aufarbeitung und Analyse der Proben fest. Diese flüchtigen organischen Verbindungen treten zum Beispiel bei Prozessen, in denen Lösemittel eingesetzt werden, auf. Diese Norm kann als Referenzverfahren angewendet werden.
ANMERKUNG   Siehe Richtlinie 1999/13/EG des Rates.
Die unter Verwendung dieser Norm erzielten Ergebnisse werden als Massenkonzentration der einzelnen gasförmigen organischen Verbindungen in Milligramm pro Kubikmeter (mg/m³) angegeben. Diese Norm ist zur Anwendung im Bereich von etwa 0,5 mg/m³ bis 2000 mg/m³ geeignet.
Zur Messung der Massenkonzentration des gesamten organisch gebundenen Kohlenstoffs aus Prozessen, bei denen Lösemittel eingesetzt werden, sollte EN 13526 angewendet werden.

Emissions de sources fixes - Détermination de la concentration massique en composés organiques gazeux individuels - Méthode par charbon actif et description des solvants

La présente Norme européenne spécifie les modes opératoires d'échantillonnage sur du charbon actif, de préparation et d'analyse d'échantillons de composants organiques volatiles, tels que ceux provenant de procédés utilisant des solvants. Elle peut être utilisée comme méthode de référence.
NOTE   Voir la Directive du Conseil 1999/13/EEC.
Les résultats obtenus en utilisant la présente norme sont exprimés en concentration massique (mg/m3) de composants organiques gazeux individuels. La présente norme est utilisable sur une plage de concentration comprise entre 0,5 mg/m3 environ et 2 000 mg/m3.
Pour le mesurage de la concentration massique en carbone organique total provenant de procédés utilisant des solvants, il convient d'utiliser l'EN 13526.

Emisije nepremičnih virov - Določevanje masne koncentracije posameznih organskih spojin v plinasti fazi - Metoda z aktivnim ogljem in desorpcije s topilom

General Information

• Status: Withdrawn
• Publication Date: 13-Nov-2001
• Withdrawal Date: 02-Dec-2014
• ICS: 13.040.40 - Stationary source emissions
• Technical Committee: CEN/TC 264 - Air quality
• Drafting Committee: CEN/TC 264/WG 4 - Total gaseous organic carbon (emissions)
• Current Stage: 9960 - Withdrawal effective - Withdrawal
• Completion Date: 03-Dec-2014
• Directive: 94/67/EC - Incineration of hazardous waste
• Mandate: M/001 - Mandate given to CEN concerning a standard for a reference method allowing the calibration of automated measurement systems for Total gaseous Organic Carbon (TOC) and main performance characteristics for the automated measurement systems
• Ref Project: SIST EN 13649:2002 - Stationary source emissions - Determination of the mass concentration of individual gaseous organic compounds - Activated carbon and solvent desorption method

Relations

• Replaced By: CEN/TS 13649:2014 - Stationary source emissions - Determination of the mass concentration of individual gaseous organic compounds - Sorptive sampling method followed by solvent extraction or thermal desorption
• Effective Date: 10-Dec-2014

Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN 13649:2002
01-maj-2002
(PLVLMHQHSUHPLþQLKYLURY'RORþHYDQMHPDVQHNRQFHQWUDFLMHSRVDPH]QLK
RUJDQVNLKVSRMLQYSOLQDVWLID]L0HWRGD]DNWLYQLPRJOMHPLQGHVRUSFLMHVWRSLORP
Stationary source emissions - Determination of the mass concentration of individual
gaseous organic compounds - Activated carbon and solvent desorption method
Emissionen aus stationären Quellen - Bestimmung der Massenkonzentration von
einzelnen gasförmigen organischen Verbindungen - Aktivkohleadsorptions- und
Lösemitteldesorptionsverfahren
Emissions de sources fixes - Détermination de la concentration massique en composés
organiques gazeux individuels - Méthode par charbon actif et description des solvants
Ta slovenski standard je istoveten z: EN 13649:2001
ICS:
13.040.40 (PLVLMHQHSUHPLþQLKYLURY Stationary source emissions
SIST EN 13649:2002 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN 13649:2002

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SIST EN 13649:2002
EUROPEAN STANDARD
EN 13649
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2001
ICS 13.040.40
English version
Stationary source emissions - Determination of the mass
concentration of individual gaseous organic compounds -
Activated carbon and solvent desorption method
Emissions de sources fixes - Détermination de la Emissionen aus stationären Quellen - Bestimmung der
concentration massique en composés organiques gazeux Massenkonzentration von einzelnen gasförmigen
individuels - Méthode par charbon actif et désorption des organischen Verbindungen - Aktivkohleadsorptions- und
solvants Lösemitteldesorptionsverfahren
This European Standard was approved by CEN on 29 September 2001.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36  B-1050 Brussels
© 2001 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN 13649:2001 E
worldwide for CEN national Members.

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SIST EN 13649:2002
EN 13649:2001 (E)
Contents
page
Foreword 3
1 Scope 3
2 Normative references 3
3 Terms and definitions 4
4 Principle 4
5 Apparatus and materials 5
6 Sampling procedure 9
7 Analytical procedure 11
8 Calculation 13
9 Report 13
Annex A (informative) Measurement uncertainty and associated statistics 15
Annex B (informative) Typical desorption efficiencies of selected organic components on
activated carbon 17
Annex C (informative) Procedure for control of leakage 19
Annex D (informative) Procedure for dilution sampling 20
Annex E (informative) Safety measures 21
2

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SIST EN 13649:2002
EN 13649:2001 (E)
Foreword
This European Standard has been prepared by Technical Committee CEN/TC 264 "Air
Quality", the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication
of an identical text or by endorsement, at the latest by May 2002, and conflicting national
standards shall be withdrawn at the latest by May 2002.
This European Standard has been prepared under a mandate given to CEN by the European
Commission and European Free Trade Association.
The annexes A, B, C, D and E are informative.
According to the CEN/CENELEC Internal Regulations, the national standards organizations
of the following countries are bound to implement this European Standard: Austria, Belgium,
Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy,
Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United
Kingdom.
1Scope
This European Standard specifies procedures for the sampling onto activated carbon, the
preparation and the analysis of samples of volatile organic components such as those arising
from solvent using processes. It can be used as a reference method.
NOTE  See Council Directive 1999/13/EEC.
3
The results obtained using this Standar
...