CEN/TS 17216:2018
(Main)Construction products - Assessment of release of dangerous substances - Determination of activity concentrations of radium-226, thorium-232 and potassium-40 in construction products using semiconductor gamma-ray spectrometry
Construction products - Assessment of release of dangerous substances - Determination of activity concentrations of radium-226, thorium-232 and potassium-40 in construction products using semiconductor gamma-ray spectrometry
This document describes a test method for the determination of the activity concentrations of the radionuclides radium-226, thorium-232 and potassium-40 in construction products using semiconductor gamma-ray spectrometry.
This document describes sampling from a laboratory sample, sample preparation, and the sample measurement by semiconductor gamma-ray spectrometry. It includes background subtraction, energy and efficiency calibration, analysis of the spectrum, calculation of the activity concentrations with the associated uncertainties, the decision threshold and detection limit, and reporting of the results. The preparation of the laboratory sample from the initial product sample lies outside its scope and is described in product standards.
This document is intended to be non product-specific in scope, however, there are a limited number of product-specific elements such as the preparation of the laboratory sample and drying of the test portion. The method is applicable to samples from products consisting of single or multiple material components.
Bauprodukte - Bewertung der Freisetzung von gefährlichen Stoffen - Messung der spezifischen Aktivität von Radium-226, Thorium-232 und Kalium-40 in Bauprodukten mittels Halbleiter-Gammaspektrometrie
Dieses Dokument beschreibt ein Prüfverfahren zur Bestimmung der spezifischen Aktivitäten der Radionuklide Radium-226, Thorium-232 und Kalium-40 in Bauprodukten durch Halbleiter-Gammaspektrometrie.
Dieses Dokument beschreibt die Probenahme einer Laborprobe, die Probenvorbereitung und die Messung der Probe durch Halbleiter-Gammaspektrometrie. Dazu gehört die Hintergrundsubtraktion, Energie- und Effizienzkalibrierung, Analyse des Spektrums, Berechnung der spezifischen Aktivitäten mit den zugehörigen Unsicherheiten, der Erkennungsgrenze und Nachweisgrenze und Angabe der Prüfergebnisse. Die Vor-bereitung der Laborprobe aus der ursprünglichen Produktprobe liegt außerhalb des Anwendungsbereichs und wird in den Produktnormen beschrieben.
Dieses Dokument soll in ihrem Anwendungsbereich nicht produktspezifisch sein, allerdings gibt es eine begrenzte Anzahl produktspezifischer Elemente, wie die Vorbereitung der Laborprobe und die Trocknung der Prüfmenge. Das Verfahren eignet sich für Produktproben, die aus einzelnen oder multiplen Material-komponenten bestehen.
Produits de construction - Evaluation de l'émission de substances dangereuses - Détermination de l’activité du radium-226, du thorium-232 et du potassium-40 dans les produits de construction par spectrométrie gamma
Gradbeni proizvodi - Ocenjevanje sproščanja nevarnih snovi - Določevanje koncentracije aktivnosti radija Ra-226, torija Th-232 in kalija K-40 v gradbenih proizvodih s polprevodniško gama spektrometrijo
Ta tehnična specifikacija določa metodo za določevanje koncentracije aktivnosti radionuklidov 226Ra, 232Th in 40K v gradbenih proizvodih s polprevodniško gama spektrometrijo. Standard opisuje vzorčenje, pripravo preskusnih vzorcev in izvedbo preskusa. Vključuje odstranjevanje ozadja, umerjanje energije in učinkovitosti, analizo spektra, izračun koncentracije aktivnosti s povezanimi negotovostmi, prag odločanja in omejitev zaznavanja ter objavo rezultatov.
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
01-marec-2019
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NRQFHQWUDFLMHDNWLYQRVWLUDGLMD5DWRULMD7KLQNDOLMD.YJUDGEHQLK
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Construction products - Assessment of release of dangerous substances - Determination
of activity concentrations of radium-226, thorium-232 and potassium-40 in construction
products using semiconductor gamma-ray spectrometry
Bauprodukte - Bewertung der Freisetzung von gefährlichen Stoffen - Messung der
spezifischen Aktivität von Radium-226, Thorium-232 und Kalium-40 in Bauprodukten
mittels Halbleiter-Gammaspektrometrie
Produits de construction - Evaluation de l'émission de substances dangereuses -
Détermination de l’activité du radium-226, du thorium-232 et du potassium-40 dans les
produits de construction par spectrométrie gamma
Ta slovenski standard je istoveten z: CEN/TS 17216:2018
ICS:
13.020.99 Drugi standardi v zvezi z Other standards related to
varstvom okolja environmental protection
17.240 Merjenje sevanja Radiation measurements
91.100.01 Gradbeni materiali na Construction materials in
splošno general
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
CEN/TS 17216
TECHNICAL SPECIFICATION
SPÉCIFICATION TECHNIQUE
October 2018
TECHNISCHE SPEZIFIKATION
ICS 91.100.01
English Version
Construction products - Assessment of release of
dangerous substances - Determination of activity
concentrations of radium-226, thorium-232 and
potassium-40 in construction products using
semiconductor gamma-ray spectrometry
Produits de construction - Evaluation de l'émission de Bauprodukte - Bewertung der Freisetzung von
substances dangereuses - Détermination de l'activité gefährlichen Stoffen - Messung der spezifischen
du radium-226, du thorium-232 et du potassium-40 Aktivität von Radium-226, Thorium-232 und Kalium-
dans les produits de construction par spectrométrie 40 in Bauprodukten mittels Halbleiter-
gamma Gammaspektrometrie
This Technical Specification (CEN/TS) was approved by CEN on 14 May 2018 for provisional application.
The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.
CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17216:2018 E
worldwide for CEN national Members.
Contents Page
European foreword . 4
Introduction . 5
1 Scope . 6
2 Normative references . 6
3 Terms and definitions . 6
4 Symbols and abbreviations . 8
5 Principles of the test method . 11
6 Sampling and sample preparation . 11
6.1 Sampling hierarchy . 11
6.2 Sampling and sub-sampling . 14
6.3 Test specimen/test portion preparation . 14
7 Test procedure . 18
7.1 General . 18
7.2 Measurement . 18
8 Processing the test data . 21
8.1 General . 21
8.2 Analysis of counting spectrum . 22
8.3 Calculating activity concentration . 22
8.4 Standard uncertainty . 24
8.5 Decision threshold . 27
8.6 Detection limit . 27
9 Test report . 29
Annex A (normative) Method for the determination of the radon-tightness of a test
specimen container . 31
A.1 Principle . 31
A.2 Apparatus, equipment and reagents . 31
A.3 Test . 31
A.4 Processing experimental data . 32
Annex B (normative) Preparation of standardized calibration sources . 35
B.1 Principle . 35
B.2 Apparatus, equipment and reagents . 35
B.3 Test . 35
Annex C (normative) Method for the determination of the activity concentration in a
composite product . 39
Annex D (informative) Complementary photopeaks to verify the activity concentration in
the test specimen . 40
Annex E (informative) Method for the determination of the corrected number of pulses in a
photopeak (only to be used for completely stand-alone single peaks) . 41
Bibliography . 42
European foreword
This document (CEN/TS 17216:2018) has been prepared by Technical Committee CEN/TC 351
“Construction products - Assessment of release of dangerous substances”, the secretariat of which is
held by NEN.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document has been prepared under a mandate given to CEN by the European Commission and the
European Free Trade Association.
According to the CEN/CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Introduction
This document is a Technical Specification developed under Mandate M/366 issued by the European
Commission in the framework of the “Construction Products Directive” 89/106/EEC. This document
addresses the part of Mandate M/366 which provides for the preparation of horizontal
measurement/test methods for the determination of the activity concentrations of the radionuclides
radium-226, thorium-232 and potassium-40 in construction products using gamma-ray spectrometry.
Mandate M/366 is a complement to the product mandates issued by the European Commission to CEN
under the Construction Products Directive (CPD). The harmonized product standards (hEN) developed
in CEN under mandates (and ETAs developed in EOTA for products or kits) specify construction
product(s) as placed on the market and address their intended conditions of use.
The information produced by applying this Technical Specification can be used for purposes of CE
marking and evaluation/attestation of conformity. Product specification, standardization of
representative sampling and procedures for any product-specific laboratory sample preparation are the
responsibility of product TCs and are not covered in this Technical Specification.
This Technical Specification supports existing regulations and standardized practices, and is based on
methods described in standards, such as ISO 10703 [1], ISO 18589-2 [2], ISO 18589-3 [3] and NEN 5697
[4]. In summary, the Technical Specification describes the following:
— sampling, sub-sampling and test specimen preparation;
— measurement using gamma-ray spectrometry;
— background subtraction, energy and efficiency calibration, analysis of the spectrum;
— calculation of activity concentrations with associated uncertainties;
— reporting of test results.
Determination of the activity concentration is based on the principles of gamma-spectrometry, and
procedures for all stages of the testing are provided in this document. Although the tested material
sample rarely reflects a product’s form under its intended conditions of use, the measured activity
concentration is an intrinsic property of the material, which does not vary with the construction
product’s form. Consequently, the test results reflect the radiation behaviour of the product under its
intended use. In addition, the Technical Specification is intended to be non product-specific in scope,
with only a limited number of product-specific elements.
1 Scope
This document describes a test method for the determination of the activity concentrations of the
radionuclides radium-226, thorium-232 and potassium-40 in construction products using
semiconductor gamma-ray spectrometry.
This document describes sampling from a laboratory sample, sample preparation, and the sample
measurement by semiconductor gamma-ray spectrometry. It includes background subtraction, energy
and efficiency calibration, analysis of the spectrum, calculation of the activity concentrations with the
associated uncertainties, the decision threshold and detection limit, and reporting of the results. The
preparation of the laboratory sample from the initial product sample lies outside its scope and is
described in product standards.
This document is intended to be non product-specific in scope, however, there are a limited number of
product-specific elements such as the preparation of the laboratory sample and drying of the test
portion. The method is applicable to samples from products consisting of single or multiple material
components.
2 Normative references
The following documents are referred to in the tex
...
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