Foodstuffs - Guidelines for the calibration and quantitative determination of pesticide residues and organic contaminants using chromatographic methods

This Technical Specification describes the execution of calibration and quantitative evaluation of chromatographic procedures for the determination of pesticides and organic contaminants in residue analysis. In addition, the essential requirements for calibration are outlined.
The calibration of analytical procedures and the evaluation of analytical results need to be conducted according to uniform principles in order to allow for a comparison of analytical results (even from different analytical procedures). They constitute the basis of any method validation and of the quality assurance within laboratories [1], [2], [3].
This Technical Specification does not consider issues of identification/qualification and extraction efficiency.

Lebensmittel - Anleitung zur Kalibrierung und quantitativen Bestimmung von Pflanzenschutzmittelrückständen und organischen Kontaminanten mit chromatographischen Verfahren

Diese Technische Spezifikation beschreibt die Durchführung der Kalibrierung und die Auswertung von Analysenergebnissen bei der Anwendung chromatographischer Methoden für die Bestimmung von Pflanzenschutzmittelrückständen und organischen Kontaminanten in Lebensmitteln. Dabei werden auch die wesentlichen Anforderungen an die Kalibrierung erläutert.
Die Kalibrierung von Analysenverfahren und die Auswertung von Analysenergebnissen müssen nach einheitlichen Grundsätzen erfolgen, um Analysenergebnisse (auch aus verschiedenen Analysenverfahren) miteinander vergleichen zu können. Sie sind Grundlage sowohl der Validierung von Methoden als auch der laborinternen Qualitätssicherung [1], [2], [3].
Diese Technische Spezifikation berücksichtigt keine Fragen zur Identifizierung/Qualifizierung von Analyten und zur Extraktionseffizienz.

Produits alimentaires - Lignes directrices pour l’étalonnage et le dosage des résidus de pesticides et contaminants organiques par des méthodes chromatographiques

Živila - Smernice za kalibracijo in kvantitativno določanje ostankov pesticidov in organskih kontaminantov (onesnaževal) z uporabo kromatografske metode

Ta tehnična specifikacija opisuje izvedbo kalibracije in kvantitativnega vrednotenja kromatografskih postopkov za določevanje pesticidov in organskih onesnaževal pri analizi ostankov. Opisane so tudi bistvene zahteve za kalibracijo.
Kalibracijo analitskih postopkov in vrednotenje analitskih rezultatov je treba izvesti v skladu z enotnimi načeli, da se omogoči primerjava analitskih rezultatov (tudi iz različnih analitskih postopkov). Ti tvorijo podlago za vsako vrednotenje metod in zagotavljanje kakovosti v laboratorijih [1], [2], [3].
Ta tehnična specifikacija ne obravnava zadev v zvezi z identifikacijo/kvalifikacijo in učinkovitostjo ekstrakcije.

General Information

Status
Withdrawn
Publication Date
26-Sep-2017
Withdrawal Date
03-Sep-2019
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
04-Sep-2019

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 17061:2017
01-november-2017
äLYLOD6PHUQLFH]DNDOLEUDFLMRLQNYDQWLWDWLYQRGRORþDQMHRVWDQNRYSHVWLFLGRYLQ
RUJDQVNLKNRQWDPLQDQWRY RQHVQDåHYDO ]XSRUDERNURPDWRJUDIVNHPHWRGH
Foodstuffs - Guidelines for the calibration and quantitative determination of pesticide
residues and organic contaminants using chromatographic methods
Lebensmittel - Leitfaden für die Kalibrierung und die Auswertung von
Analysenergebnissen bei der Anwendung chromatographischer Methoden für die
quantitative Bestimmung von Pflanzenschutzmittelrückständen und organischen
Kontaminanten
Produits alimentaires - Lignes directrices pour l’étalonnage et le dosage des résidus de
pesticides et contaminants organiques par des méthodes chromatographiques
Ta slovenski standard je istoveten z: CEN/TS 17061:2017
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
SIST-TS CEN/TS 17061:2017 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST-TS CEN/TS 17061:2017

---------------------- Page: 2 ----------------------

SIST-TS CEN/TS 17061:2017


CEN/TS 17061
TECHNICAL SPECIFICATION

SPÉCIFICATION TECHNIQUE

September 2017
TECHNISCHE SPEZIFIKATION
ICS 67.050
English Version

Foodstuffs - Guidelines for the calibration and quantitative
determination of pesticide residues and organic
contaminants using chromatographic methods
Produits alimentaires - Lignes directrices pour Lebensmittel - Leitfaden für die Kalibrierung und die
l'étalonnage et le dosage des résidus de pesticides et Auswertung von Analysenergebnissen bei der
contaminants organiques par des méthodes Anwendung chromatographischer Methoden für die
chromatographiques quantitative Bestimmung von
Pflanzenschutzmittelrückständen und organischen
Kontaminanten
This Technical Specification (CEN/TS) was approved by CEN on 11 May 2017 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17061:2017 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST-TS CEN/TS 17061:2017
CEN/TS 17061:2017 (E)
Contents Page
European foreword . 4
1 Scope . 5
2 Principle . 5
3 General . 5
4 Execution and calculation of calibrations . 6
4.1 General/specifications . 6
4.1.1 Working range. 6
4.1.2 Number of calibration points . 6
4.1.3 Permissible quantities for determination of response (peak areas or peak heights
and peak ratio, respe
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 17061:2017
01-marec-2017
äLYLOD6PHUQLFH]DNDOLEUDFLMRLQNYDQWLWDWLYQRGRORþDQMHRVWDQNRYSHVWLFLGRYLQ
RUJDQVNLKNRQWDPLQDQWRY RQHVQDåHYDO ]XSRUDERNURPDWRJUDIVNHPHWRGH
Foodstuffs - Guidelines for the calibration and quantitative determination of pesticide
residues and organic contaminants using chromatographic methods
Lebensmittel - Leitfaden für die Kalibrierung und die Auswertung von
Analysenergebnissen bei der Anwendung chromatographischer Methoden für die
quantitative Bestimmung von Pflanzenschutzmittelrückständen und organischen
Kontaminanten
Ta slovenski standard je istoveten z: FprCEN/TS 17061
ICS:
67.050 Splošne preskusne in General methods of tests and
analizne metode za živilske analysis for food products
proizvode
kSIST-TS FprCEN/TS 17061:2017 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 17061:2017

---------------------- Page: 2 ----------------------
kSIST-TS FprCEN/TS 17061:2017


FINAL DRAFT
TECHNICAL SPECIFICATION
FprCEN/TS 17061
SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION

January 2017
ICS 67.050
English Version

Foodstuffs - Guidelines for the calibration and quantitative
determination of pesticide residues and organic
contaminants using chromatographic methods
 Lebensmittel - Leitfaden für die Kalibrierung und die
Auswertung von Analysenergebnissen bei der
Anwendung chromatographischer Methoden für die
quantitative Bestimmung von
Pflanzenschutzmittelrückständen und organischen
Kontaminanten


This draft Technical Specification is submitted to CEN members for Vote. It has been drawn up by the Technical Committee
CEN/TC 275.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change
without notice and shall not be referred to as a Technical Specification.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 17061:2017 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 17061:2017
FprCEN/TS 17061:2017 (E)
Contents Page
European foreword . 4
1 Scope . 5
2 Principle . 5
3 General . 5
4 Execution and calculation of calibrations . 6
4.1 General/specifications . 6
4.1.1 Working range. 6
4.1.2 Number of calibration points . 6
4.1.3 Permissible quantities for determination of response (peak areas or peak heights
and peak ratio, respectively) . 7
4.1.4 Stability of calibration functions . 7
4.2 Calibration functions . 8
4.2.1 Selection of appropriate calibration function
...

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