Construction products: Assessment of release of dangerous substances - Digestion by aqua regia for subsequent analysis of inorganic substances

This Technical Specification specifies methods for obtaining the aqua regia digestible content of construction products. Solutions produced by this method are for analysis by inductively coupled plasma mass spectrometry (ICP-MS) and inductively coupled spectrometry (ICP-OES) for the following 67 elements:
Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), silver (Ag), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).
Solutions produced by the methods are suitable for analysis by cold vapour atomic absorption or fluorescent spectrometry (CV-AAS, CV-AFS), for mercury (Hg).
The method in this Technical Specification is applicable to construction products.
Digestion with aqua regia will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.
NOTE   Construction products include e.g. mineral-based products (S); bituminous products (B); metals (M); wood-based products (W); plastics and rubbers (P); sealants and adhesives (A); paints and coatings (C), see also CEN/TR 16045.

Bauprodukte - Bewertung der Freisetzung von gefährlichen Stoffen - Königswasser-Aufschluss zur anschließenden Analyse von anorganischen Stoffen

Diese Technische Spezifikation legt Verfahren zur Gewinnung des mit Königswasser aufschließbaren Anteils von Bauprodukten fest. In den Lösungen, die nach diesem Verfahren hergestellt wurden, können mittels Massenspektrometrie mit induktiv gekoppeltem Plasma (ICP-MS) oder mittels optischer Emissionspektrometrie mit induktiv gekoppeltem Plasma (ICP-OES) die folgenden 67 Elemente analysiert werden:
Aluminium (Al), Antimon (Sb), Arsen (As), Barium (Ba), Beryllium (Be), Bismut (Bi), Blei (Pb), Bor (B), Cadmium (Cd), Calcium (Ca), Cäsium (Cs), Cer (Ce), Chrom (Cr), Cobalt (Co), Dysprosium (Dy), Eisen (Fe), Erbium (Er), Europium (Eu), Gadolinium (Gd), Gallium (Ga), Germanium (Ge), Gold (Au), Hafnium (Hf), Holmium (Ho), Indium (In), Iridium (Ir), Kalium (K), Kupfer (Cu), Lanthan (La), Lithium (Li), Lutetium (Lu), Magnesium (Mg), Mangan (Mn), Molybdän (Mo), Natrium (Na), Neodym (Nd), Nickel (Ni), Palladium (Pd), Phosphor (P), Platin (Pt), Praseodym (Pr), Quecksilber (Hg), Rubidium (Rb), Rhenium (Re), Rhodium (Rh), Ruthenium (Ru), Samarium (Sm), Scandium (Sc), Schwefel (S), Selen (Se), Silber (Ag), Silizium (Si), Strontium (Sr), Tellur (Te), Terbium (Tb), Thallium (Tl), Thorium (Th), Thulium (Tm), Titan (Ti), Uran (U), Vanadium (V), Wolfram (W), Ytterbium (Yb), Yttrium (Y), Zink (Zn), Zinn (Sn) und Zirconium (Zr).
Durch die Verfahren erstellte Lösungen sind für die Analyse von Quecksilber (Hg) mittels Kaltdampf-Atomabsorptions- oder Fluoreszenzspektrometrie (CV-AAS, CV-AFS) geeignet.
Die in dieser Technischen Spezifikation beschriebenen Verfahren sind für Bauprodukte geeignet.
Der Aufschluss mit Königswasser wird die Probe nicht unbedingt völlig zersetzen. Die extrahierten Analytkonzentrationen können unter Umständen nicht den Gesamtgehalt in der Probe wiedergeben.
ANMERKUNG   Bauprodukte umfassen z. B. mineralische Produkte (S), bituminöse Produkte (B), Metalle (M), Holzprodukte (W), Kunststoffe und Gummi (P), Dichtstoffe und Kleber (A), Farben und Beschichtungen (C), siehe auch CEN/TR 16045.

Produits de construction - Evaluation de l’émission de substances dangereuses - Digestion par l’eau régale pour une analyse ultérieure de substances inorganiques

Gradbeni proizvodi - Ocenjevanje sproščanja nevarnih snovi - Razklop z zlatotopko za analizo anorganskih snovi

Ta tehnična specifikacija določa metodo za razklop gradbenih proizvodov za analizo vsebnosti anorganskih snovi. Metoda temelji na uporabi zlatotopke. Raztopine, pridobljene s to metodo, so primerne za analizo z npr. masno spektrometrijo z induktivno sklopljeno plazmo (ICP-MS) in emisijsko spektrometrijo z induktivno sklopljeno plazmo (ICP-OES), atomsko absorpcijsko spektrometrijo (CVAAS, CVAFS) za naslednje elemente: aluminij, antimon, arzen, barij, berilij, bizmut, bor, kadmij, kalcij, cerij, krom, kobalt, baker, železo, lantan, svinec, litij, magnezij, mangan, živo srebro, molibden, neodim, nikelj, fosfor, kalij, prazeodim, samarij, skandij, selen, silicij, srebro, natrij, stroncij, žveplo, telurij, talij, torij, kositer, titan, volfram, uran, vanadij, cink in cirkonij. OPOMBA: Gradbeni proizvodi vključujejo npr. mineralne proizvode (S), bitumenske proizvode (B), kovine (M), lesne proizvode (W), plastične mase in gume (P), tesnila in lepila (A), barve in premaze (C), glej tudi CEN/TR 16045.

General Information

Status
Withdrawn
Publication Date
17-Jul-2018
Withdrawal Date
21-Nov-2023
Current Stage

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 17196:2019
01-januar-2019
*UDGEHQLSURL]YRGL2FHQMHYDQMHVSURãþDQMDQHYDUQLKVQRYL5D]NORS]
]ODWRWRSNR]DDQDOL]RDQRUJDQVNLKVQRYL
Construction products - Assessment of release of dangerous substances - Digestion by
aqua regia for subsequent analysis of inorganic substances
Bauprodukte - Bewertung der Freisetzung von gefährlichen Stoffen - Königswasser-
Aufschluss zur anschließenden Analyse von anorganischen Stoffen
Produits de construction - Evaluation de l’émission de substances dangereuses -
Digestion par l’eau régale pour une analyse ultérieure de substances inorganiques
Ta slovenski standard je istoveten z: CEN/TS 17196:2018
ICS:
13.020.99 Drugi standardi v zvezi z Other standards related to
varstvom okolja environmental protection
91.100.01 Gradbeni materiali na Construction materials in
splošno general
SIST-TS CEN/TS 17196:2019 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST-TS CEN/TS 17196:2019

---------------------- Page: 2 ----------------------

SIST-TS CEN/TS 17196:2019


CEN/TS 17196
TECHNICAL SPECIFICATION

SPÉCIFICATION TECHNIQUE

July 2018
TECHNISCHE SPEZIFIKATION
ICS 91.100.01
English Version

Construction products: Assessment of release of
dangerous substances - Digestion by aqua regia for
subsequent analysis of inorganic substances
Produits de construction - Evaluation de l'émission de Bauprodukte - Bewertung der Freisetzung von
substances dangereuses - Digestion par l'eau régale gefährlichen Stoffen - Königswasser-Aufschluss zur
pour une analyse ultérieure de substances anschließenden Analyse von anorganischen Stoffen
inorganiques
This Technical Specification (CEN/TS) was approved by CEN on 9 March 2018 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17196:2018 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST-TS CEN/TS 17196:2019
CEN/TS 17196:2018 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Symbols and abbreviations . 7
5 Principle . 8
6 Interferences and sources of errors . 8
7 Reagents . 8
8 Apparatus .
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 17196:2018
01-januar-2018
*UDGEHQLSURL]YRGL2FHQMHYDQMHVSURãþDQMDQHYDUQLKVQRYL5D]NORS]
]ODWRWRSNR]DDQDOL]RDQRUJDQVNLKVQRYL
Construction products: Assessment of release of dangerous substances - Digestion by
aqua regia for subsequent analysis of inorganic substances
Bauprodukte - Beurteilung der Freisetzung von gefährlichen Stoffen - Königswasser-
Aufschluss von Bauprodukten
Produits de construction - Évaluation des émissions de substances dangereuses -
Digestion à l'eau régale des produits de construction
Ta slovenski standard je istoveten z: FprCEN/TS 17196
ICS:
13.020.99 Drugi standardi v zvezi z Other standards related to
varstvom okolja environmental protection
91.100.01 Gradbeni materiali na Construction materials in
splošno general
kSIST-TS FprCEN/TS 17196:2018 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 17196:2018

---------------------- Page: 2 ----------------------
kSIST-TS FprCEN/TS 17196:2018


FINAL DRAFT
TECHNICAL SPECIFICATION
FprCEN/TS 17196
SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION

November 2017
ICS 91.100.01
English Version

Construction products: Assessment of release of
dangerous substances - Digestion by aqua regia for
subsequent analysis of inorganic substances
Produits de construction - Évaluation des émissions de Bauprodukte - Beurteilung der Freisetzung von
substances dangereuses - Digestion à l'eau régale des gefährlichen Stoffen - Königswasser-Aufschluss von
produits de construction Bauprodukten


This draft Technical Specification is submitted to CEN members for Vote. It has been drawn up by the Technical Committee
CEN/TC 351.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.

Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change
without notice and shall not be referred to as a Technical Specification.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2017 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 17196:2017 E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 17196:2018
FprCEN/TS 17196:2017 (E)
Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 5
3 Terms and definitions . 5
4 Symbols and abbreviations . 7
5 Principle . 8
6 Interferences and sources of errors . 8
7 Reagents . 8
8 Apparatus . 8
9 Procedure. 10
9.1 Sample pre-treatment .
...

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