EN 13399:2017
(Main)Bitumen and bituminous binders - Determination of storage stability of modified bitumen
General Information
- Abstract
This European Standard specifies a method for measuring the storage stability at high temperatures.
NOTE Modified bitumen and, in particular, polymer-modified bitumen, which consist of mainly bitumen and at least one additional agent, are known to display phase separation under certain conditions.
WARNING - The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
- Status
- Published
- Publication Date
- 05-Dec-2017
- Withdrawal Date
- 29-Jun-2018
- Technical Committee
- CEN/TC 336 - Bituminous binders
- Drafting Committee
- CEN/TC 336/WG 1 - Bituminous binders for paving
- Current Stage
- 9093 - Decision to confirm - Review Enquiry
- Start Date
- 30-Nov-2023
- Completion Date
- 17-Sep-2026
Overview
EN 13399:2017 is the CEN European standard that specifies a laboratory method for determining the storage stability of modified bitumen (including polymer‑modified bitumen) at high temperatures. The method evaluates the tendency of modified bituminous binders to undergo phase separation during prolonged thermal storage by conditioning a representative sample in a vertical aluminium tube and comparing the properties of the top and bottom fractions after a specified ageing period.
Key topics and requirements
- Scope: Measurement of storage stability of modified bitumen at high temperature (default test temperature 180 °C ± 5 °C, or producer‑specified temperature ± 5 °C).
- Principle: Keep a homogeneous sample in a vertical vessel for (72 ± 1) h, cool, cut into three equal parts and analyse the top and bottom parts for differences.
- Apparatus highlights:
- Thin unvarnished aluminium tube (closed at one end; height ≥ 160 mm; diameter 25–40 mm - typically “toothpaste tube”).
- Oven capable of maintaining ± 5 °C accuracy at test temperature.
- Forceps/pliers for closing the tube, cutting tool and heating tool for recovery.
- Sample preparation & filling:
- Ensure representative, homogeneous laboratory sample in accordance with EN 58 and prepare test sample per EN 12594.
- Fill tube to a marked level (100–120 mm), remove air, squeeze tube to allow thermal expansion and tightly seal (folded and crimped using forceps).
- Test conditions:
- Place the filled tube vertically in the preheated oven within 1 hour of filling and maintain for 72 hours.
- Cool in vertical position, then recover the sample by cutting or peeling the foil; discard the middle section and combine/analyse top and bottom parts.
- Reporting: Include sample ID, reference to EN 13399, measured values for top and bottom (and difference/ratio), storage temperature if different, deviations, and test date.
- Safety note: The standard warns that hazardous materials and operations may be involved; users must implement appropriate safety and regulatory controls.
Applications and users
EN 13399:2017 is used for:
- Quality control and production monitoring by bitumen and polymer-modified bitumen manufacturers.
- Acceptance testing for paving contractors, road authorities and material procurement.
- R&D labs assessing additive compatibility and formulation stability.
- Certification bodies and laboratories performing compliance testing for product specifications.
Keywords: EN 13399, storage stability of modified bitumen, polymer‑modified bitumen storage test, bitumen testing, CEN standard.
Related standards
- EN 58 - Sampling of bituminous binders
- EN 12594 - Preparation of test samples
- EN 1427 - Softening point (Ring and Ball)
- EN 1426 - Needle penetration
- EN 14770 - DSR (complex shear modulus)
- EN 13398 - Elastic recovery of modified bitumen
This standard helps detect phase separation tendencies and supports reliable specification, production control and in-service performance of modified bituminous binders.
Relations
- Effective Date
- 13-Dec-2017
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
- Effective Date
- 28-Jan-2026
Get Certified
Connect with accredited certification bodies for this standard
DIBt (Deutsches Institut für Bautechnik)
German Institute for Building Technology.
DIN CERTCO
DIN Group product certification.
Element Materials Technology
Materials testing and product certification.
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Frequently Asked Questions
EN 13399:2017 is a standard published by the European Committee for Standardization (CEN). Its full title is "Bitumen and bituminous binders - Determination of storage stability of modified bitumen". This standard covers: This European Standard specifies a method for measuring the storage stability at high temperatures. NOTE Modified bitumen and, in particular, polymer-modified bitumen, which consist of mainly bitumen and at least one additional agent, are known to display phase separation under certain conditions. WARNING - The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
This European Standard specifies a method for measuring the storage stability at high temperatures. NOTE Modified bitumen and, in particular, polymer-modified bitumen, which consist of mainly bitumen and at least one additional agent, are known to display phase separation under certain conditions. WARNING - The use of this European Standard can involve hazardous materials, operations and equipment. This European Standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this European Standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
EN 13399:2017 is classified under the following ICS (International Classification for Standards) categories: 75.140 - Waxes, bituminous materials and other petroleum products; 91.100.50 - Binders. Sealing materials. The ICS classification helps identify the subject area and facilitates finding related standards.
EN 13399:2017 has the following relationships with other standards: It is inter standard links to EN 13399:2010, EN 58:2012, EN 12594:2024, EN 14023:2010. Understanding these relationships helps ensure you are using the most current and applicable version of the standard.
EN 13399:2017 is associated with the following European legislation: EU Directives/Regulations: 305/2011; Standardization Mandates: M/124. When a standard is cited in the Official Journal of the European Union, products manufactured in conformity with it benefit from a presumption of conformity with the essential requirements of the corresponding EU directive or regulation.
EN 13399:2017 is available in PDF format for immediate download after purchase. The document can be added to your cart and obtained through the secure checkout process. Digital delivery ensures instant access to the complete standard document.
Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.VNODGLãþHQMXBitumen und bitumenhaltige Bindemittel - Bestimmung der Lagerbeständigkeit von modifiziertem BitumenBitumes et liants bitumineux - Détermination de la stabilité au stockage des bitumes modifiésBitumen and bituminous binders - Determination of storage stability of modified bitumen91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 13399:2017SIST EN 13399:2018en,fr,de01-februar-2018SIST EN 13399:2018SLOVENSKI
STANDARDSIST EN 13399:20101DGRPHãþD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 13399
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Bitumen and bituminous binders æ Determination of storage stability of modified bitumen Bitumes et liants bitumineux æ Détermination de la stabilité au stockage des bitumes modifiés
Bitumen und bitumenhaltige Bindemittel æ Bestimmung der Lagerbeständigkeit von modifiziertem Bitumen This European Standard was approved by CEN on
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egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Rue de la Science 23,
B-1040 Brussels
t r s y CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s u u { {ã t r s y ESIST EN 13399:2018
European foreword . 3 1 Scope . 4 2 Normative references . 4 3 Principle . 4 4 Apparatus . 4 5 Procedure. 5 5.1 General . 5 5.2 Filling of the tube . 5 5.3 Closing of the tube . 5 5.4 Test conditions . 5 5.5 Recovery of the sample . 5 6 Test report . 6 Bibliography . 7
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