EN 13926:2003

Surface active agents - Alkoxylated derivatives - Determination of hydroxyl value - N-methyl imidazole method

This draft European Standard specifies a method for the determination of hydroxyl value of aliphatic and alicyclic hydroxyl compounds such as polyols, sorbitan esters, plasticisers and surface active agent alcohols and ethoxylates with hydroxyl values greater than 20 mg/g KOH.

Grenzflächenaktive Stoffe - Alkoxylierte Derivate - Bestimmung der Hydroxylzahl - N-Methylimidazol-Verfahren

Diese Europäische Norm legt ein Verfahren zur Bestimmung der Hydroxylzahl von aliphatischen und alizyklischen Hydroxylbestandteilen wie Polyalkoholen, Sorbitanestern, grenzflächenaktiven Alkoholen und Ethoxylaten mit Hydroxylzahlen größer als 20 mg/g KOH fest.

Agents de surface - Dérivés alkyloxylés - Détermination de l'indice d'hydroxyle - Méthode à la N-méthylimidazole

La présente Norme européenne spécifie une méthode de détermination de l'indice d'hydroxyle de composés hydroxy aliphatiques et alicycliques tels que les polyols, les esters de sorbitan, les plastifiants et les agents de surface sur base alcool et alkyloxylés avec des indices d'hydroxyle supérieurs à 20 mg KOH/g.

Površinsko aktivne snovi - Alkoksilatni derivati - Določevanje hidroksilne vrednosti - Metoda z N-metil imidazolom

General Information

• Status: Published
• Publication Date: 11-Mar-2003
• Withdrawal Date: 29-Sep-2003
• ICS: 71.100.40 - Surface active agents
• Technical Committee: CEN/TC 276 - Surface active agents
• Drafting Committee: CEN/TC 276/WG 1 - Methods of analysis
• Current Stage: 9093 - Decision to confirm - Review Enquiry
• Completion Date: 31-Oct-2024
• Ref Project: SIST EN 13926:2003 - Surface active agents - Alkoxylated derivatives - Determination of hydroxyl value - N-methyl imidazole method

Standards Content (Sample)

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.GURNVLOQHGrenzflächenaktive Stoffe - Alkoxylierte Derivate - Bestimmung der Hydroxylzahl - N-Methylimidazol-VerfahrenAgents de surface - Dérivés alkyloxylés - Détermination de l'indice d'hydroxyle - Méthode a la N-méthylimidazoleSurface active agents - Alkoxylated derivatives - Determination of hydroxyl value - N-methyl imidazole method71.100.40Površinsko aktivna sredstvaSurface active agentsICS:Ta slovenski standard je istoveten z:EN 13926:2003SIST EN 13926:2003en01-maj-2003SIST EN 13926:2003SLOVENSKI
STANDARD
EUROPEAN STANDARDNORME EUROPÉENNEEUROPÄISCHE NORMEN 13926March 2003ICS 71.100.40English versionSurface active agents - Alkoxylated derivatives - Determinationof hydroxyl value - N-methyl imidazole methodAgents de surface - Dérivés alkyloxylés - Détermination del'indice d'hydroxyle - Méthode à la N-méthylimidazoleGrenzflächenaktive Stoffe - Alkoxylierte Derivate -Bestimmung der Hydroxylzahl - N-Methylimidazol-VerfahrenThis European Standard was approved by CEN on 29 November 2002.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,Hungary, Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Slovakia, Spain, Sweden, Switzerland and UnitedKingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMITÉ EUROPÉEN DE NORMALISATIONEUROPÄISCHES KOMITEE FÜR NORMUNGManagement Centre: rue de Stassart, 36
B-1050 Brussels© 2003 CENAll rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 13926:2003 ESIST EN 13926:2003

Results of interlaboratory test.9Annex B (informative)
Example for potentiometric operating parameters.11Annex C (informative)
Example for a typical titration curve and its derivative.12Bibliography.13SIST EN 13926:2003

% dried at (105 ± 1) °C.SIST EN 13926:2003

% (m/m) to the nearest 0,1 g and dissolve it in 250 mlfreshly boiled water. Then transfer the solution into a 2 l volumetric flask and complete to the mark with ethanol(5.6). Allow the solution to stand for 24 h before standardization.5.8Acetylation reagentCarefully mix 92 ml of tetrahydrofuran (5.2) and 8 ml of acetic anhydride (5.3). This solution is stable for up to onemon
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