Sludge, treated biowaste and soil - Determination of linear alkylbenzene sulfonates (LAS) by high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) or mass selective detection (MS)

This Technical Specification specifies a method for the determination of linear alkylbenzene sulfonate (LAS) in sludge, treated biowaste and soil using high-performance liquid chromatography (HPLC) with a fluorescence detector (FLD) or a mass selective detector (MS).
This Technical Specification specifies the determination of the sum of LAS. Under the conditions specified in this Technical Specification, typically a limit of detection of 20 mg/kg (expressed as dry matter) for sludge and of 0,2 mg/kg to 0,5 mg/kg for soil and treated biowaste may be achieved.
Lower limits of detection may be achieved by concentrating the extract by solvent evaporation.
NOTE   The single LAS homologues C10 to C14 can be determined by this Technical Specification.

Schlamm, behandelter Bioabfall und Boden - Bestimmung von linearen Alkylbenzolsulfonaten (LAS) mittels Hochleistungs-Flüssigkeitschromatographie (HPLC) mit Fluoreszenzdetektion (FLD) oder massenselektiver Detektion (MS)

Diese Technische Spezifikation legt ein Verfahren zur Bestimmung der linearen Alkylbenzolsulfonate (LAS) in Schlamm, behandeltem Bioabfall und Boden mittels Hochleistungs Flüssigchromatographie (HPLC) und Detektion durch Fluoreszenz (FLD) oder Massenspektrometrie (MS) fest.
Diese Technische Spezifikation beschreibt die Bestimmung der Summe aller LAS. Unter den in dieser Technischen Spezifikation festgelegten Bedingungen kann in der Regel eine Nachweisgrenze von 20 mg/kg (angegeben als Trockenmasse) für Schlamm und eine Nachweisgrenze von 0,2 mg/kg bis 0,5 mg/kg für Boden und behandelten Bioabfall erreicht werden.
Niedrigere Nachweisgrenzen können erreicht werden, wenn der Extrakt durch Verdampfen des Lösemittels konzentriert wird.
ANMERKUNG   Nach dieser Technischen Spezifikation können die LAS Homologen C10 bis C14 einzeln bestimmt werden.

Boues, biodéchets traités et sols - Détermination des alkylbenzènesulfonates linéaires (LAS) par chromatographie liquide à haute performance (CLHP) avec détection par fluorescence (FLD) ou détection sélective de masse (SM)

La présente Spécification technique spécifie une méthode pour la détermination des alkylbenzènesulfonates linéaires (LAS) dans les boues, les biodéchets traités et les sols par chromatographie liquide à haute performance (CLHP) avec détection par fluorescence (FLD) ou détection par spectrométrie de masse (SM).
La présente Spécification technique spécifie la détermination de la somme des alkylbenzènesulfonates linéaires (LAS). Dans les conditions définies dans la présente Spécification technique, on peut généralement atteindre une limite de détection de 20 mg/kg (exprimée par rapport à la matière sèche) pour les boues et de 0,2 mg/kg à 0,5 mg/kg pour les sols et les biodéchets traités.
Il est possible d'atteindre des limites de détection inférieures en augmentant la concentration de l'extrait par évaporation de solvant.
NOTE   La présente Spécification technique permet de déterminer les homologues individuels C10 à C14 des alkylbenzènesulfonates linéaires (LAS).

Blato, obdelani biološki odpadki in tla - Določevanje linearnih alkilbenzen sulfonatov (LAS) z uporabo tekočinske kromatografije visoke ločljivosti (HPLC) s fluorescenčno detekcijo (FLD) ali masno selektivno detekcijo (MS)

Ta tehnična specifikacija opredeljuje metodo za določevanje linearnih alkilbenzen sulfonatov (LAS) v blatu, obdelanih bioloških odpadkih in tleh z uporabo tekočinske kromatografije visoke ločljivosti (HPLC) s fluorescenčno detekcijo (FLD) ali masno selektivno detekcijo (MS). Ta tehnična specifikacija opredeljuje določevanje vsote linearnih alkilbenzen sulfonatov. Pod pogoji iz te tehnične specifikacije se običajno lahko dosežejo meje detekcije 20 mg/kg (izraženo kot suha snov) za blato in od 0,2 mg/kg do 0,5 mg/kg za tla in obdelane biološke odpadke. Nižje meje detekcije se lahko dosežejo s koncentracijo izvlečka z izhlapevanjem raztopine.

General Information

Status
Published
Publication Date
21-Feb-2012
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Start Date
02-Dec-2020
Completion Date
02-Dec-2020

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST-TS CEN/TS 16189:2012
01-junij-2012
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHOLQHDUQLKDONLOEHQ]HQ
VXOIRQDWRY /$6 ]XSRUDERWHNRþLQVNHNURPDWRJUDILMHYLVRNHORþOMLYRVWL +3/& V
IOXRUHVFHQþQRGHWHNFLMR )/' DOLPDVQRVHOHNWLYQRGHWHNFLMR 06
Sludge, treated biowaste and soil - Determination of linear alkylbenzene sulfonates
(LAS) by high-performance liquid chromatography (HPLC) with fluorescence detection
(FLD) or mass selective detection (MS)
Schlamm, behandelter Bioabfall und Boden - Bestimmung von Linearen
Alkylbenzolsulfonaten (LAS) mittels Hochleistungs-Flüssigkeitschromatographie (HPLC)
mit Fluoroszenzdetektion (FLD) oder massenselektiver Detektion (MS)
Boues, bio-déchets traités et sols - Détermination des alkylbenzènesulfonates linéaires
(LAS) par chromatographie liquide à haute performance (CLHP) avec détection par
fluorescence (FLD) ou détection sélective de masse (SM)
Ta slovenski standard je istoveten z: CEN/TS 16189:2012
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
13.080.10 .HPLMVNH]QDþLOQRVWLWDO Chemical characteristics of
soils
SIST-TS CEN/TS 16189:2012 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------

SIST-TS CEN/TS 16189:2012

---------------------- Page: 2 ----------------------

SIST-TS CEN/TS 16189:2012


TECHNICAL SPECIFICATION
CEN/TS 16189

SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION
February 2012
ICS 13.030.01
English Version
Sludge, treated biowaste and soil - Determination of linear
alkylbenzene sulfonates (LAS) by high-performance liquid
chromatography (HPLC) with fluorescence detection (FLD) or
mass selective detection (MS)
Boues, biodéchets traités et sols - Détermination des
Schlamm, behandelter Bioabfall und Boden - Bestimmung
alkylbenzènesulfonates linéaires (LAS) par von linearen Alkylbenzolsulfonaten (LAS) mittels
chromatographie liquide à haute performance (CLHP) avec Hochleistungs-Flüssigkeitschromatographie (HPLC) mit
détection par fluorescence (FLD) ou détection sélective de Fluoreszenzdetektion (FLD) oder massenselektiver
masse (SM) Detektion (MS)
This Technical Specification (CEN/TS) was approved by CEN on 24 April 2011 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to submit their
comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS available
promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in parallel to the CEN/TS)
until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2012 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 16189:2012: E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------

SIST-TS CEN/TS 16189:2012
CEN/TS 16189:2012 (E)
Contents Page
Foreword .3
Introduction .4
1 Scope .5
2 Normative references .5
3 Terms and definitions .5
4 Principle .5
5 Interferences .6
5.1 Interferences from sampling .
...

SLOVENSKI STANDARD
kSIST-TS FprCEN/TS 16189:2011
01-februar-2011
%ODWRREGHODQLELRORãNLRGSDGNLLQWOD'RORþHYDQMHOLQHDUQLKDONLOEHQ]HQ
VXOIRQDWRY /$6 ]XSRUDERWHNRþLQVNHNURPDWRJUDILMHYLVRNHORþOMLYRVWL +3/& V
IOXRUHVFHQþQRGHWHNFLMR )/' DOLPDVQRVHOHNWLYQRGHWHNFLMR 06
Sludge, treated biowaste and soil - Determination of linear alkylbenzene sulfonates
(LAS) by high-performance liquid chromatography (HPLC) with fluorescence detection
(FLD) or mass selective detection (MS)
Schlamm, behandelter Bioabfall und Boden - Bestimmung von Linearen
Alkylbenzolsulfonaten (LAS) mittels Hochleistungs-Flüssigkeitschromatographie (HPLC)
mit Fluoroszenzdetektion (FLD) oder massenselektiver Detektion (MS)
Boues, bio-déchets traités et sols - Détermination des alkylbenzènesulfonates linéaires
(LAS) par chromatographie liquide à haute performance (CLHP) avec détection par
fluorescence (FLD) ou détection sélective de masse (SM)
Ta slovenski standard je istoveten z: FprCEN/TS 16189
ICS:
13.030.20 7HNRþLRGSDGNL%ODWR Liquid wastes. Sludge
kSIST-TS FprCEN/TS 16189:2011 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

---------------------- Page: 1 ----------------------
kSIST-TS FprCEN/TS 16189:2011

---------------------- Page: 2 ----------------------
kSIST-TS FprCEN/TS 16189:2011


TECHNICAL SPECIFICATION
FINAL DRAFT
FprCEN/TS 16189
SPÉCIFICATION TECHNIQUE

TECHNISCHE SPEZIFIKATION

December 2010
ICS 13.030.01
English Version
Sludge, treated biowaste and soil - Determination of linear
alkylbenzene sulfonates (LAS) by high-performance liquid
chromatography (HPLC) with fluorescence detection (FLD) or
mass selective detection (MS)
Boues, bio-déchets traités et sols - Détermination des Schlamm, behandelter Bioabfall und Boden - Bestimmung
alkylbenzènesulfonates linéaires (LAS) par von Linearen Alkylbenzolsulfonaten (LAS) mittels
chromatographie liquide à haute performance (CLHP) avec Hochleistungs-Flüssigkeitschromatographie (HPLC) mit
détection par fluorescence (FLD) ou détection sélective de Fluoroszenzdetektion (FLD) oder massenselektiver
masse (SM) Detektion (MS)


This draft Technical Specification is submitted to CEN members for Technical Committee Approval. It has been drawn up by the Technical
Committee CEN/TC 400.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland,
Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are aware and to
provide supporting documentation.

Warning : This document is not a Technical Specification. It is distributed for review and comments. It is subject to change without notice
and shall not be referred to as a Technical Specification.


EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2010 CEN All rights of exploitation in any form and by any means reserved Ref. No. FprCEN/TS 16189:2010: E
worldwide for CEN national Members.

---------------------- Page: 3 ----------------------
kSIST-TS FprCEN/TS 16189:2011
FprCEN/TS 16189:2010 (E)
Contents Page
Foreword .4
Introduction .5
1 Scope .6
2 Normative references .6
3 Terms and definitions .6
4 Principle .6
5 Interferences .7
5.1 Interferences from sampling .7
5.2 Interferences by HPLC-FLD and HPLC-MS .7
6 Reagents .
...

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